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850 results about "Hydrogen flow" patented technology

Method for improving catalyst reacting activity in the propylene producing through propane dehydrogenation

A method to promote the activity of a catalyst for dehydrogenation of propane to propylene is as follows: (1) an inorganic oxide bonding agent, a promoter and an acid solvent are added into a heat-resistant oxide; then after the oxide bonding agent, the promoter, the acid solvent and the oxide are kneaded evenly, the oxide is molded by rolling or band-extruding; (2) the catalyst carrier prepared is dried for 2 to 10 hours under the temperature of 60 centigrade degrees, and calcined under the temperature of 400 to 800 degrees; (3) the calcined carrier is immersed in a rare earth metal water solution under the temperature of 60 to 100 centigrade degrees for 2 to 10 hours; (4) the catalyst carrier modified by the rare earth is immersed in a water solution comprising platinum metal elementsand the fourteenth metal elements under the temperature of 400 to 600 centigrade degrees for 2 to 10 hours, and then the carrier is filtered, washed with distilled water, dried under the temperature of 60 to 180 centigrade degrees for 2 to 10 hours, and calcined under the temperature of 400 to 600 centigrade degrees for 2 to 10 hours; (5) the catalyst prepared is activated in the air under the temperature of 400 to 600 centigrade degrees for 3 to 10 hours, and reduced in a hydrogen flow under the temperature of 400 to 600 centigrade degrees for 2 to 10 hours; the reduced catalyst is used for catalytic reaction for dehydrogenation of propane to propylene.
Owner:SOUTHEAST UNIV

Technological process for continuously producing succinic anhydride and co-producing succinic acid through maleic anhydride hydrogenation

The invention discloses a technological process for continuously producing succinic anhydride and co-producing succinic acid through maleic anhydride catalytic hydrogenation. The whole process comprises three steps, namely, reaction, rectification and hydrolysis, wherein two stages of hydrogenation reactors are used for reaction, a primary hydrogenation reactor is a fixed bed reactor with hydrogen entering from the lower part and reaction liquid exiting from the upper part, and a secondary hydrogenation reactor is a trickle bed reactor with hydrogen and reaction liquid entering from the upper part and exiting from the lower part. The technological process adopts an external circulating heat radiation manner, and reaction heat is uniformly removed, so that the average operation temperature of the whole reactor is effectively controlled, and the reaction temperature in the whole main reactor is balanced. Furthermore, the primary hydrogenation reactor adopts the manner that both the maleic anhydride solution and hydrogen flow upward simultaneously, so that the reaction temperature of the whole reactor is controlled to be balanced, local hot spot temperature is effectively controlled and lowered, and the reactants are prevented from polymerizing and depositing carbon or coking.
Owner:SHANXI UNIV

Method for preparing iron-based prealloy powder

ActiveCN103658668AGood cold forming abilityEvenly distributedReduction treatmentEvaporation
The invention discloses a method for preparing iron-based prealloy powder. The method includes the steps that (1) iron-based bulk metal is prepared, the content of Fe is 30wt%-90wt%, the content of Cu is 10wt%-70wt%, and the melting point is no more than 1,800 DEG C; (2) smelting water atomization powder process treatment is conducted on the metal, so that the iron-based prealloy powder is obtained; (3) the treated powder is dried; (4) after drying of the atomization powder is completed, low-melting metal simple substance powder is added, the melting point is no more than 500 DEG C, and the content is no more than 15wt%; (5) the low-melting metal powder and the dried powder are evenly mixed; (6) reduction treatment is carried out on the mixed powder through a reduction furnace, hydrogen flow is controlled to be 20m<3>/h-30m<3>/h, and reduction time is no less than 2h; (7) large particles are sieved and removed to obtain the iron-based prealloy powder. The method is easy to implement and simple and convenient to operate, by the aid of a high-temperature diffusion and evaporation cohesion principle in the reduction process, the content of produced Zn is 2-15% that of the iron-based prealloy powder, and the iron-based prealloy powder has the advantages of being low in oxygen content, simple in preparation mode and good in cold pressing formability.
Owner:HUBEI EXIN DIAMOND TECH

Integrated metal-graphite composite bipolar plate fuel cell light electric stack and manufacturing method thereof

The invention relates to an integrated metal-graphite composite bipolar plate fuel cell light electric stack. An integrated metal-graphite composite bipolar plate is used for the integrated metal-graphite composite bipolar plate fuel cell light electric stack, the integrated metal-graphite composite bipolar plate comprises a metal corrugated plate and a graphite plate, the metal corrugated plate is a negative pole plate, a raised ridge inner chamber is an oxygen flow field, and meanwhile a raised ridge takes a heat-radiating rib into consideration; the graphite plate is a positive pole plate, the surface of one side of the graphite plate body is provided with a hydrogen flow field, the edge of the surface of one side of the graphite plate body is provided with a sealing groove, and the other side of the graphite plate body is provided with a graphite plate corrugated structure; and the graphite plate is embedded into the metal corrugated plate by the graphite plate corrugated structure, and the graphite plate and the metal corrugated plate are connected as a whole. The performance and the stability of the electric stack are remarkably improved. Because a negative temperature coefficient thermistor material is added in the graphite plate material, the cold starting time can be remarkably reduced, and the electric stack can be used normally at a higher temperature above 60 DEG C.
Owner:TSINGHUA UNIV
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