4173 results about "Metal powder" patented technology

The invention relates to the technical field of image data processing, and discloses a fine metal powder defect detection method and system based on image recognition, and the method comprises the steps: illuminating a metal powder region through a non-polarized light source, and collecting two images in an orthogonal polarization state through imaging equipment with a linear polarizer, according to the method, the defect morphological fingerprints are constructed through the polarization information entropy, the three-dimensional structure information is converted into light field order degree change for detection, the dimension limitation of traditional two-dimensional imaging is broken through, and the detection accuracy is improved. Hidden defects such as internal pores and aggregates can be accurately identified, and meanwhile, stable detection and material defect cross discrimination under a dynamic working condition are realized in combination with motion compensation and multiband entropy ratio verification.

The invention relates to the technical field of rocket engine thrust chamber additive manufacturing, and discloses a metal powder recovery system for rocket engine thrust chamber additive manufacturing. Comprising a powder collection module, a screening classification module, a purification treatment module, a particle size adjustment module and an intelligent control module. The powder collecting module captures residual metal powder and collects data to generate a data set; the screening and grading module performs particle size separation by using a joint algorithm; the purification treatment module is used for constructing a multi-stage purification model to remove an oxide layer and decompose organic matters; the particle size adjustment module designs a composite regulation strategy to adjust particle size distribution; and the intelligent control module establishes an optimization model to generate a parameter adjustment instruction. In addition, the system is further provided with a powder characteristic analysis module, a circulation monitoring module and an exception handling module. The system can efficiently recover the metal powder, improve the quality and reutilization value of the metal powder, reduce the cost and guarantee the quality of additive manufacturing products, and is suitable for metal powder recovery treatment in the field of additive manufacturing of rocket engine thrust chambers.

The invention discloses an intelligent management system based on metal powder production, and relates to the technical field of industrial automation intelligent management. Sensor arrays are deployed in an ultrasonic atomizer and a vacuum drying furnace, the dust concentration, the vibration frequency, the pressure, the humidity, the temperature and the oxygen concentration are measured in real time, and the current stage is obtained through a production plan; dynamically and finely adjusting the weight matrix according to the sensor parameters corresponding to different stages, generating a weighted comprehensive index, calculating theoretical control parameters based on a physical model, correcting the theoretical control parameters through an LSTM neural network in combination with real-time environmental data, outputting an equipment control instruction, and extracting the sphericity and the moisture residue of the metal powder after the production of the metal powder is completed, so as to obtain the spherical degree of the metal powder. And the production quality is judged, and different responses are adopted according to the judgment result. The multi-parameter cooperative control precision is further improved, and the system stability is enhanced.

The invention belongs to the field of metal powder hot isostatic pressing and additive manufacturing near-net forming, and discloses a hot isostatic pressing forming method for preparing a substrate for additive manufacturing by mixing SS-PREP and EIGA Ti6Al4V ELI spherical powder, which comprises the following steps of: 1, mixing Ti6Al4V ELI powder prepared by SS-PREP and Ti6Al4V ELI powder prepared by EIGA according to a proportion under atmosphere protection; 2, in vacuum vibration powder loading equipment, the mixed powder is loaded into a steel sheath, and degassing seal welding is carried out; step 3, placing the seal-welded sheath in hot isostatic pressing equipment, carrying out heat preservation and pressure maintaining sintering forming, and then carrying out gradient cooling; and 4, after cooling, the steel sheath is removed through machining, and the large-size substrate for additive manufacturing is obtained. The prepared substrate has excellent comprehensive mechanical properties which are higher than the level of traditional forgings, and the application requirements of additive manufacturing are met.

The invention discloses a formula, a coating and a method of a dual in-situ precipitation reinforced FeCoNiCr-based high-entropy alloy composite material with a low corrosion-wear synergistic effect. The Al-Co-Cr alloy material comprises the following components in atomic percent: 15 to 30 at% of Al, 10 to 25 at% of Co, 10 to 25 at% of Cr, 10 to 25 at% of Fe, 10 to 25 at% of Ni, 20 to 35 at% of Ti and 5 to 15 at% of C, the preparation method comprises the following steps: filling all metal powder and graphene powder into a ball-milling tank, adding grinding balls, filling argon, sealing, and ball-milling, so as to obtain mixed powder in which the surfaces of metal powder particles are uniformly coated with graphene. The high-entropy alloy composite material with high hardness, high wear resistance and high corrosion resistance is obtained by utilizing the solid solution strengthening effect and the multiple in-situ precipitation strengthening effect of micron-scale TiC and nano-scale precipitation B2. The prepared coating is uniform and compact in structure, is metallurgically bonded with a base material, and has excellent corrosion and friction resistance and low corrosion-wear synergistic effect.

The invention relates to the technical field of image data processing, and discloses a method for detecting impurities in metal powder based on image recognition, which comprises the following steps of: irradiating the metal powder by using polarized light, synchronously acquiring an orthogonal polarization component image of the reflected light, and realizing impurity detection by calculating a differential image. Qualified powder spontaneously forms a uniform dark field in a differential image by utilizing the essential difference of response of metal powder and impurities to polarized light, and the impurities generate remarkable signals due to optical anisotropy, so that the detection blind area of the traditional method on the microscopic impurities is broken through, the method further performs time sequence analysis by multiplexing total luminous flux data, and the detection accuracy is improved. Synchronous identification of impurity morphological characteristics is realized, component and morphological two-dimensional detection capability is formed, the system realizes adaptive threshold adjustment based on statistical characteristics of differential images, and long-term operation stability is ensured.

The invention provides a high-precision laser additive manufacturing method and device based on metal powder melting, and relates to the technical field of metal additive manufacturing, and the high-precision laser additive manufacturing device comprises a multi-element powder supply and electrification unit which is used for carrying out independent metering supply and airflow dispersion mixing on various metal powder in an inert atmosphere environment and enabling powder particles to obtain controllable charges; the electromagnetic field cooperative control unit is used for actively regulating and controlling the falling speed and the transverse track of the powder particles through the cooperative effect of a longitudinal magnetic field and a transverse electric field when the powder particles are in a charged state; the invention provides a metal powder forming technology path based on particle size active conveying and spatial positioning, and active conveying and accurate positioning of the metal powder particles in the flying process are realized by performing electrified regulation and control on single or small-scale metal powder particles and utilizing the action of an electromagnetic field. Therefore, layer-by-layer stacking forming is completed under the condition of not depending on the whole powder laying layer.

The invention discloses a method for measuring the particle size of metal powder by using a scanning electron microscope, which comprises the following steps: step 1, sample treatment: adhering a small conductive adhesive tape on a sample table, sprinkling metal powder on the adhered conductive adhesive tape, and purging to obtain the conductive adhesive tape adhered with the metal powder; step 2, parameter setting: setting acceleration voltage, working distance, diaphragm, image contrast, brightness, magnification times and scanning speed of a scanning electron microscope to observe the conductive adhesive tape adhered with the metal powder obtained in the step 1 to obtain an electronic image of metal powder particles; and processing and calculating the electronic image of the metal powder particles by using software to obtain the average particle size of the metal powder particles. According to the method disclosed by the invention, a solvent is not needed to disperse the sample, pollution of the solvent to the sample is effectively avoided, and the result is more accurate than that of directly measuring the particle size by using length software.

The invention discloses a flux-cored wire for extra-thick marine steel high heat input EGW and a preparation method of the flux-cored wire, and relates to the technical field of metal welding, the flux-cored wire comprises an outer skin of a double-layer alloy steel strip and powder filled in the outer skin, the filling rate of the powder is 20 + / -5%, and the powder comprises Fe, Mn, Si, Cr, Ni, Mo, V, B, S, Al, MgAl2O4, MgO-TiO2, ReOx and a slag former. According to the preparation method, the metal powder is positively charged, the rare earth nanoparticles are negatively charged through an electrostatic self-assembly technology, the metal powder and the rare earth nanoparticles are mixed with a slag former after being mixed, filtered and freeze-dried, an alloy steel strip is filled with the powder, and then rolling and drawing forming is conducted. In the welding process, the composite inclusions form a core-shell structure, a weld metal structure is regulated and controlled, acicular ferrite nucleation is promoted, and grains are refined, so that the low-temperature toughness and crack arrest performance of a weld are remarkably improved, the rare earth elements are beneficial for changing irregular inclusions into spheres, nucleation sites are increased, interface energy is reduced, and the nucleation rate of acicular ferrite is increased.

The invention discloses a multi-component composite oxide dispersion strengthening molybdenum alloy and a preparation method thereof, and relates to the technical field of refractory metal powder metallurgy preparation. The molybdenum alloy comprises a molybdenum matrix and a Y-X-O composite oxide nano precipitated phase dispersed and distributed in the molybdenum matrix. The molybdenum alloy comprises the following components in percentage by mass: 1%-2% of Y2O3, 0.3%-1.2% of an active element X, 96.5%-98.7% of molybdenum and inevitable impurities, wherein X is selected from one of Ti, Zr and Hf; the Y-X-O composite oxide nano precipitated phase and the molybdenum matrix form a coherent or semi-coherent interface, and the interface mismatch degree is less than or equal to 5%. The molybdenum alloy has excellent high-temperature strength and creep resistance, and can be applied to the high-temperature fields of nuclear industry, aerospace and the like.

The invention relates to a method for preparing bimetallic core-shell structure composite powder based on an acoustic resonance technology, and belongs to the technical field of powder metallurgy. Adding the micron matrix metal powder and the nano coating layer metal powder into a mixing tank, replacing air in the mixing tank with protective gas or active gas, and setting the pressure of the gas in the tank and the temperature of the tank body; and then three-section acoustic resonance coating powder preparation is carried out, and the bimetal core-shell structure composite powder is obtained. According to the method, different metal powder is driven by acoustic resonance to do violent disordered movement, the outer layer of micron metal powder is evenly and tightly coated with nano metal powder under the combined action of electrostatic force and other physical force, and finally the core-shell structure bimetal coated powder is obtained. The method is simple, the preparation efficiency is high, the applicability is wide, the thickness adjustable range of the coating layer of the obtained bimetallic coated powder is wide, the obtained bimetallic coated powder is uniform and compact, the powder particle morphology can be effectively maintained, and pollution of other elements is avoided.

An additive manufacturing method based on micro-selective laser melting technology. By using a spot size of 30 μm or less, a metal powder layer thickness of 10 μm or less and ultrafine metal powders having a D90 particle size of 30 μm or less, and in combination with the control of a scanning laser power, a scanning rate, a linear energy density and a volumetric energy density within specific ranges, the method can print complex-structured metal parts having extremely high resolutions and surface smoothness, and can obtain a high-density internal structure of a component even under a relatively low energy density or power condition, thereby effectively protecting an optical system. Moreover, a printed component exhibits a defect-free microstructure, and has excellent electrical properties, thermal properties and mechanical properties. Particularly, ultrafine grains and a high dislocation density provide superior mechanical properties compared to conventional manufacturing materials. An infrared laser device can be used, thereby achieving low costs.

The invention belongs to the technical field of cable processing, and relates to a preparation method and application of a flexible superconducting coaxial cable outer conductor. The preparation method comprises the following steps: mixing Nb powder and Ti powder by adopting a vibrating ball mill to prepare NbTi composite powder; a substrate of laser powder bed melting equipment is preheated, the NbTi composite powder is spread on the substrate of the laser powder bed melting equipment, a melting powder layer is scanned through the laser powder bed melting technology, a three-dimensional communicated grid structure is formed through interlayer staggered scanning, finally, the NbTi net-shaped alloy pipe is placed in a strong acid solution to be soaked for a short time, redundant metal powder is removed, and the NbTi net-shaped alloy pipe is obtained. And finally, the preparation of the flexible superconducting coaxial cable outer conductor for the quantum computer is realized.

The invention provides MAB-phase ceramic powder as well as a preparation method and application thereof, and belongs to the technical field of ceramic materials. Firstly, elementary substance M powder and boron powder serve as raw materials, and MB powder is prepared through ball milling treatment, tabletting, heat treatment and grinding; the simple substance M powder is selected from transition metal powder; the preparation method comprises the following steps: by taking MB powder and aluminum powder as raw materials, carrying out wet ball-milling treatment, compression molding, packaging and sintering treatment to prepare MAB-phase ceramic powder; the packaging is carried out by adopting potassium bromide powder. According to the invention, an MS3-fused salt shielding synthesis / sintering method is adopted, salt is used as a reaction medium and a salt bed, the exterior of a sample is packaged with salt, so that a synthetic product is prevented from being oxidized during high-temperature synthesis in the air, and the preparation method has the characteristics of rapidness, high efficiency, energy conservation, environmental protection, low cost and the like, and is simple, convenient and feasible in the aspect of promotion of large-scale production.

The invention discloses a production process of rare earth microalloying low-cost 550MPa-grade weathering steel based on a CSP production line, and belongs to the technical field of steel and iron material preparation. According to the process, the composition proportion is optimized, La / Ce composite microalloying is adopted, and the CSP short-process continuous casting and rolling technology is combined, so that low-cost production of the high-performance weathering resistant steel is achieved. The method specifically comprises the key procedures of molten steel component design, whole-course protective pouring, homogenizing annealing at the temperature of 1100-1300 DEG C, six-rack controlled rolling, layered cooling and the like. The thickness of the obtained steel plate is 1-5 mm, the yield strength is larger than or equal to 550 MPa, the tensile strength is 620-780 MPa, the percentage elongation after fracture is larger than or equal to 16%, and the weight loss ratio is reduced by 15% or above compared with that of rare earth-free steel after the steel plate is immersed and corroded by 3.5% NaCl for 72 h. Through rare earth purification of molten steel, grain refinement and improvement of rust layer compactness, the corrosion resistance is remarkably improved while the use amount of Ni / Cu is reduced, the technical problem that nodulation is prone to occurring when rare earth is added in a CSP production line is solved, and the rare earth metal powder has the comprehensive advantages of being high in production efficiency, low in cost and stable in product performance and is suitable for weather-proof structural parts such as buildings and bridges.

The invention discloses a metal powder packaging quality detection system based on machine vision, and relates to the technical field of visual inspection, the system comprises a visual acquisition module, an image processing module and a central processing module, the visual acquisition module is used for acquiring at least one group of detection images of each metal powder packaging bag; the visual acquisition module transmits the detection image module to the image processing module; after the image processing module receives the detection image, the detection image is matched with the corresponding technical powder packaging bag, and the image processing module preprocesses the detection image; and after receiving the preprocessed detection image, the central processing module performs visual identification on the detection image to obtain use quality data of the packaging bag. Through combination of the visual sensor module and the image processing module, accurate detection of the quality of the packaging bag is realized, and the packaging bag can be monitored in real time.

The invention relates to the technical field of metal powder processing, and discloses a high-performance dissimilar metal powder precision forming process which comprises the following steps: filling powder into a mold cavity, applying vibration disturbance, monitoring the change rate of a phase lag angle, judging that the powder is dense when the change rate is lower than an offset threshold value, outputting a pressing mode switching signal, an induction heating device is used for applying transient thermal load to induce cracks of an oxide film on the surfaces of particles, the pressure load is applied, the side wall is adjusted to generate shear displacement to peel off the oxide film, and metallurgical bonding is achieved through fresh metal surface contact. An interface is activated through thermal expansion mismatch and mechanical friction synergistically, a high-density uniform green body is obtained at low temperature, generation of brittle intermetallic compounds is inhibited, and the fatigue resistance of a formed part is enhanced.

The invention relates to a stainless steel flux-cored wire and a preparation method thereof, and relates to the technical field of flux-cored wires. The stainless steel flux-cored wire comprises a stainless steel strip and a double-layer flux core, the stainless steel strip is filled with the double-layer flux core, and the filling amount of the double-layer flux core accounts for 20-25% of the total mass of the stainless steel flux-cored wire; the double-layer flux core comprises a rapid reaction layer and an alloy transition layer, the rapid reaction layer comprises an oil stain oxidizing agent, the oil stain oxidizing agent comprises a high-temperature decomposition type organic matter and an inorganic composition, and the inorganic composition comprises copper oxide and ferric oxide with the mass ratio being (1-1.5): 1. The high-temperature decomposition type organic matter comprises polytetrafluoroethylene micro powder and trisodium citrate according to the mass ratio of 1: (3-5), and the alloy transition layer comprises 316L stainless steel powder, metal powder, silicon powder, niobium carbide and rare earth oxide. The invention can effectively avoid hydrogen embrittlement caused by diffusible hydrogen easily formed by compounds in anti-rust oil remaining on the surface of the welding wire during welding and entering a welding seam.

The utility model relates to the technical field of powder injection, and discloses a device for solving air trapping caused by non-injection of metal powder, which comprises a lower die, an upper die is clamped at the top of the lower die, a connecting seat is fixedly connected with the top of the upper die, and first injection pipes are communicated with two ends of the connecting seat. A first injection pipe is fixedly installed in the upper mold, a second injection pipe is fixedly installed in the upper mold, the first injection pipe communicates with the second injection pipe, a fixing base is arranged in the second injection pipe, a stirring helical ribbon is fixedly connected to the top of the fixing base, and a pressing plate is fixedly connected to the top of the stirring helical ribbon; and the top of the pressing plate is rotationally connected with the top of the inner wall of the second injection pipe, and a driving mechanism is embedded into the connecting base. According to the device for solving the problem of air trapping during non-injection of the metal powder, the injected flowing metal powder is stirred to be more uniformly distributed in the second injection pipe and the mold, gaps and bubbles among powder particles are reduced, and the air trapping phenomenon is prevented.

The invention relates to the technical field of nano metal production, and particularly discloses a crucible liquid level height measuring method and a crucible liquid level height measuring device.The crucible liquid level height measuring method comprises the following steps that a cooling jacket is arranged outside a crucible, cooling water is introduced, after the water amount is stable, the crucible and the cooling jacket are weighed through a sensor, and the crucible liquid level height is measured; obtaining a weight value a; equipment works, evaporation of the metal raw materials is reduced, and a real-time weight value c is obtained; and according to the formula, the liquid level remaining height = ((c-a) / liquid metal density) / crucible bottom area, the liquid level remaining height in the crucible is calculated, and the feeding time is judged according to the liquid level remaining height. The crucible liquid level height measuring device comprises a vacuum container, a crucible and a weighing sensor are arranged in the vacuum container, and the crucible is placed above the weighing sensor. The metal powder manufacturing device has the effect of accurately judging the feeding time when metal powder is manufactured.

The invention discloses a metal crack repairing method and device based on an ultrasonic technology. The method comprises the steps that metal powder is selected as brazing filler metal and pretreated; cleaning cracks in the metal base material and spraying a boron nitride coating; mixing an ethanol solution with brazing filler metal powder according to a preset proportion, stirring to form a uniform suspension, injecting the suspension into the crack filling area through a needle tube in a vacuum negative pressure environment, preheating to accelerate solvent volatilization, and only leaving and compacting the brazing filler metal powder; clamping and fixing the base material and putting the base material into a vacuum chamber; electron beam melting is started, snakelike scanning is conducted in the length direction of the crack, and meanwhile ultrasonic vibration is conducted on the crack; and after fusion is completed, ultrasonic vibration is continuously carried out to restrain grain coarsening. Aiming at crack repair of a high-temperature metal part, through the coupling effect of electron beam melting and ultrasonic vibration, the limitation of a single technology is broken through, and a complete and synergistic repair system is formed.

The invention relates to the technical field of metal powder manufacturing products, in particular to an automatic ring part production line and a process control method.Bar heating furnaces of the production line are arranged on the inner side and the outer side of a guide rail in two rows and multiple sets, a transfer manipulator is arranged on the guide rail, a ring forging press machine is arranged at the front end of the guide rail, and a movable workbench is arranged at the ring forging press machine; the ring rolling machine is arranged in front of the ring forging press machine, the center line of the ring rolling machine and the center line of the ring forging press machine are obliquely arranged, a carrying mechanical arm is arranged between the ring rolling machine and the ring forging press machine, the conveying roller way is arranged in front of the ring rolling machine, and the center line of the conveying roller way and the center line of the ring rolling machine are obliquely arranged. The center line of the conveying roller way is parallel to the center line of the ring forging press, and the swing manipulator is arranged in an included angle formed by the ring rolling machine and the conveying roller way. According to the production line and the control method, the production process is optimized, the production efficiency is improved, and the production cost is reduced.

The invention discloses a grain boundary diffusion method of a sintered neodymium-iron-boron magnet. The grain boundary diffusion method comprises the following steps: providing a magnet to be diffused; coating the surface of the magnet to be diffused with coating slurry containing heavy rare earth metal powder, and performing grain boundary diffusion after vacuum heat preservation and dehydrogenation; the vacuum heat preservation dehydrogenation process comprises the steps that under the vacuum condition, the temperature is increased to 220-250 DEG C from the normal temperature after 1-1.5 h, heat preservation is conducted for 2-3 h, then the temperature is increased to 520-560 DEG C after 1-2 h, and heat preservation is conducted for 1-2 h; the grain boundary diffusion process comprises the following steps: heating to 650-750 DEG C after 1-1.5 hours, and preserving heat for 24-30 hours for permeation; and finally, the temperature is increased to 970-1000 DEG C after 1-1.5 h, and heat preservation is conducted for 2-3 h. According to the grain boundary diffusion method, the coercive force of the center part of the sintered neodymium-iron-boron magnet with the high permeation thickness can be remarkably improved, and the intrinsic coercive force gradient difference of the surface layer and the center part of the magnet is reduced.

The invention discloses a nuclear radiation resistant heat-insulating protective coating for steam pipelines and a preparation method thereof. The coating comprises a surface layer and a bottom layer; the surface layer comprises 30 to 50 parts of a surface layer base, 10 to 30 parts of pigments and fillers, 5-10 parts of metal powder, 18 to 20 parts of a curing agent and 18 to 20 parts of a diluent; the bottom layer comprises 10 to 30 parts of a bottom layer base, 30 to 50 parts of pigments and fillers, 5-10 parts of metal powder, 18 to 20 parts of a curing agent and 18 to 20 parts of a diluent; wherein the surface layer base comprises acrylic modified organic silicon resin; the bottom layer base comprises water glass; the pigments and fillers comprise enamel powder, ceramics and auxiliary fillers; the auxiliary fillers comprise one or more of mica, iron oxide, zinc titanate, fluoropolymer and borosilicate; the coating of the invention can effectively insulate and protect the steam pipeline in a high temperature and nuclear radiation environment, thereby extending the service life of the steam pipeline and improving the safety and reliability of the nuclear power plant.

The platform stabilizing device for laser 3D printing comprises a machine box and a box door rotationally connected to the outer side of the machine box through a hinge, a supporting device is fixedly connected to the inner side of the machine box, a guide limiting frame is fixedly connected to the top of the supporting device, and conveying rollers are rotationally connected to the two sides of the top of the guide limiting frame; and the outer side of the conveying roller is sleeved with a conveying belt, and the outer side of the guide limiting frame is slidably connected with a scraping device. According to the device, the three-slot platform lifting frame is arranged, and grooves in the two sides of the three-slot platform lifting frame are used for storing metal powder. When the printing platform descends, the main telescopic rod synchronously descends along with the hydraulic telescopic rod, at the moment, hydraulic oil in the main telescopic rod enters the auxiliary telescopic rod through the liquid guide assembly, meanwhile, the auxiliary telescopic rod pushes the push plate to slide upwards in the grooves in the two sides, metal powder is pushed upwards, and sufficient materials are provided for subsequent printing.

The invention provides high-filling silver powder and a preparation method thereof, and belongs to the field of metal powder.The preparation method comprises the steps that a nano-silver solution is prepared, a dispersing agent and a first reducing agent are mixed to obtain a mixed solution, the nano-silver solution and the mixed solution are mixed in a constant-temperature stirring state to obtain a base solution, a second reducing agent solution and a silver nitrate solution are prepared respectively, and the high-filling silver powder is prepared. And under the constant-temperature stirring state, the second reducing agent solution and the silver nitrate solution are synchronously added into the base solution, a silver powder solution is obtained through reaction, the silver powder solution is subjected to washing, solid-liquid separation, drying and depolymerization shaping treatment, and the high-filling silver powder is obtained. Controllable preparation of the large-size sphericity silver powder is achieved by controlling the particle size and the adding amount of the nano-silver, regulating and controlling heterogeneous nucleation and growth sites of silver ions and inhibiting formation of multistage dendritic crystals, surface charges and steric hindrance effects of silver particles are optimized through the surface adsorption effect of the dispersing agent, the agglomeration phenomenon of the silver powder in the growth process is reduced, and the silver powder is prepared. And meanwhile, the silver powder is endowed with excellent flowability.

The present application relates to a kind of method and device for judging the trend of concrete oblique crack tip, fill metal powder in the crack to be measured;Determine the beginning and end point of crack trend according to the opening trend of crack surface to be measured, draw the center line of the connecting line of beginning and end point as the first measuring line, respectively from the two end points of the first measuring line along the first measuring line to crack opening position detection using electromagnetic wave radar detector, record the position and depth of the first fluctuation point on radar development map;With the first measuring line as reference line, rotate to make several new measuring lines, obtain the position and depth of the first fluctuation point of each new measuring line;Fluctuation point is sorted according to measuring line sequence, draw the connecting line diagram, i.e. the trend curve of oblique crack tip.The present application is based on the essential characteristics such as the height and form of oblique crack tip position, combined with the measurement mode from far to near, multi-angle, multiple measuring points and the reflection law of radar wave by metal powder, the position and depth of multiple points of concrete oblique crack tip are measured, and then the trend of crack tip is effectively judged.

The invention belongs to the technical field of TG-DSC testing of metal powder materials, and particularly relates to an anti-oxidation high-precision TG-DSC testing method of high-temperature alloy powder, which comprises the following steps: placing the high-temperature alloy powder in a furnace body of a TG-DSC instrument, carrying out high-purity argon replacement on the atmosphere in the furnace body by taking high-purity argon as furnace body purging gas, and carrying out high-purity argon replacement on the atmosphere in the furnace body; the initial oxygen content in the furnace body is reduced to 0.1 ppm or below; continuously introducing hydrogen-argon mixed gas as flowing gas into the furnace body, controlling the temperature of the furnace body to be increased to a target temperature, and ending the test to obtain a TG curve and a DSC curve of the to-be-tested high-temperature alloy powder; according to the invention, through physical cleaning of oxygen in the furnace body by circulating vacuumizing before testing and chemical cleaning of oxygen permeating into the furnace body by hydrogen-argon mixed gas in the whole process in the testing process, a dual anti-oxidation barrier is constructed, so that oxidation weight increment and oxidation heat release interference of a powder sample are eliminated fundamentally; therefore, the real mass change and the heat flow signal change of the alloy powder sample in the temperature programming process can be accurately measured.

The invention relates to the field of metal powder processing, in particular to a sintering process intelligent control method and system based on a powder metallurgy metal material, and the method comprises the steps: obtaining a temperature curve of a powder metallurgy sintering process, determining the offset of each curve through a cross-correlation function, and carrying out the alignment; the method comprises the following steps: determining a segmentation length according to segmentation adaptability of a local area, analyzing an abnormal reference degree based on correlation between a mahalanobis distance of each segment and sintering quality, obtaining an overall abnormal degree of each curve through normalization processing and weighted calculation, and judging whether an abnormal temperature curve exists according to the overall abnormal degree and a preset abnormal degree threshold value. And if the abnormal degree exceeds the preset abnormal degree threshold value, early warning that the sintering process is abnormal, and prompting adjustment control. According to the invention, local abnormity is accurately detected, temperature control is optimized, the production cost is reduced, and the product quality and the production efficiency are improved.

The invention provides a vibration screening device for metal powder, and belongs to the technical field of metal powder screening, the vibration screening device comprises a screening shell and a sealing cover mounted at the upper end of the screening shell, a mounting frame is arranged in the screening shell and is in a step shape, a first annular screen is arranged in the center of the interior of the mounting frame, and a second annular screen is arranged in the middle of the first annular screen. A second annular screen is arranged at the inner edge of the mounting frame, a first gear ring is rotationally connected to the inner center of the mounting frame, a first vortex-shaped piece used for cleaning the surface of the first annular screen is arranged on the outer side face of the first gear ring, and a second gear ring is rotationally connected to the inner edge of the mounting frame; a second vortex-shaped piece used for cleaning the surface of the second annular screen is arranged on the outer side face of the second gear ring. A driving part used for driving the first gear ring and the second gear ring to rotate is arranged in the mounting frame. According to the screening device, materials can be effectively dispersed while screening is conducted, and the probability that the screen is blocked is reduced.