The invention discloses a preparation method of homogeneous high-purity
scandium-aluminum
alloy powder, and belongs to the technical field of
alloy material preparation. The method comprises the following steps that
metal scandium and
aluminum metal ingots are prepared according to the
atomic ratio of
scandium to aluminum being 1: 3-3: 1 and then placed into a
smelting furnace, and
smelting and heat preservation are conducted under the
argon atmosphere; the
alloy solution is poured into a rotary water-cooling
copper roller with the linear speed of 2-5 m / s to achieve rapid hardening, and a scandium-aluminum alloy sheet is prepared; the scandium-aluminum alloy sheet is activated and then subjected to hydrogenation-
dehydrogenation treatment; and finally,
xenon is used as working gas for
airflow pulverization, and scandium-aluminum alloy
powder of 10-75 microns is obtained through
airflow separation. According to the method, the polycrystalline alloy sheet with fine grains is prepared through rapid hardening,
hydrogen decrepitation is promoted through the
grain boundary,
pollution of a ball milling medium is avoided, the problems that in the prior art, alloy
powder is low in purity, uneven in grain size and low in crushing yield are solved, and the prepared alloy powder is homogeneous, high in purity and suitable for preparation of high-end products such as target materials.