22463 results about "Ingot" patented technology

A method of manufacturing a single crystal ingot, and a single crystal ingot and a wafer manufactured thereby are provided. The method of manufacturing a single crystal ingot according to an embodiment includes forming a silicon melt in a crucible inside a chamber, preparing a seed crystal on the silicon melt, and growing a single crystal ingot from the silicon melt, and pressure of the chamber may be controlled in a range of 90 Torr to 500 Torr.

GaN single crystal substrates are produced by slicing a GaN single crystal ingot in the planes parallel to the growing direction. Penetration dislocations which have been generated in the growing direction extend mainly in the bulk of the GaN substrate. A few of the threading dislocations appear on the surface of the GaN substrate. GaN substrates of low-dislocation density are obtained.

The invention relates to a high-conductivity aluminum alloy material for a cable and a preparation method thereof. The aluminum alloy material comprises the following components in percentage by weight: 0.25-0.80 percent of iron element, 0.02-0.15 percent of boron element, 0.1-1.5 percent of rare earth element and the balance of aluminum and inevitable impurities. The aluminum alloy is formed by adding an aluminum alloy intermediate alloy, an aluminum-boron alloy and an aluminum-rare earth intermediate alloy into an aluminum ingot of which the purity is more than 99.80 percent by weight and carrying out a casting process and annealing treatment on the mixture. Compared with a common electric aluminum conductor, the prepared aluminum alloy conductor has more excellent conductive performance and the conductivity reaching or exceeding 62.5 percent IACS (International Annealed Copper Standard); the aluminum alloy conductor treated by using a special process has excellent flexibility and creep resistance; and compared with a common electric aluminum conductor, the prepared aluminum alloy material used as a cable extrusion insulating lead core is more energy-saving and safer.

The invention relates to a high-entropy alloy material and a method for preparing the same. The component of the high-entropy alloy material is AlCoCrFeNiTix, wherein x represents a molar ratio, and the value range is between 0.1-0.4. The method for preparing the material comprises: preparing raw materials, adopting the alloy smelting raw materials including Al, Co, Cr, Fe, Ni and Ti, and accurately weighing and proportioning according to the molar ratio; then, purifying oxide on a metal surface; putting the prepared raw materials into a tank in a water-cooling copper-formed mold smelting pool, vacuumizing, filling argon, controlling smelting current to be at about 250 ampere and smelting time for 30-60 seconds, turning an alloy block after alloys are fully mixed, putting an alloy ingot into a tank of a water-cooling copper-formed mold, regulating the smelting current, opening a suction casting air suction valve after the alloys are uniformly smelted, utilizing the negative pressure in a pump for suction casting, and taking out the alloy ingot after an alloy mould is cooled. Compared with the conventional crystalline state alloy, the high-entropy alloy material has relative high thermal stability, hardness, yield strength, breaking tenacity, plastic deformation and work hardening capacity.

The invention relates to an austenitic stainless steel, a steel tube thereof and a manufacturing method thereof, wherein the austenitic stainless steel and the stainless steel tube comprise the components by mass percent: 0.060-0.14% of C, more than 0 and less than or equal to 0.50% of Si, more than 0 and less than or equal to 1.00% of Mn, less than 0.040% of P, less than 0.015% of S, 17.00-20.00% of Cr, 8.00-11.00% of Ni, 2.50-4.00% of Cu, 0.30-0.60% of Nb, 0.15-0.50% of Mo, 0.15-0.50% of Co, 0.05-0.14% of N, 0.001-0.01% of B, the rest of Fe and unavoidable impurity. The manufacturing method of the steel tube comprises: smelting and pouring to form steel ingots or continuously cast bloom, processing bar material, preparing tubular billet and further processing the steel tube; the method comprises the steps: the heating temperature of processing the bar material is 1250-1270 DEG C, heating temperature of preparing the tubular billet is 1100-1220 DEG C, and the finished product solid solution temperature is 1120-1190 DEG C. The austenitic stainless steel tube has high temperature creep strength and corrosion resisting performance at the high temperature.

A silicon casting apparatus for producing polycrystal silicon ingot by heating a silicon melt (8) held in a mold (4) from above by a heater (3) and cooling it from below while changing the heat exchange area of a heat exchange region (HE), defined between a pedestal (5) having the mold (4) placed thereon and a bottom cooling member (6), in such a manner as to keep pace with the rise of the solid-liquid interface of the silicon melt (8), thereby causing unidirectional solidification upward along the mold (4); and a method of producing polycrystal silicon ingot using such apparatus. According to this production method, the temperature gradient given to the silicon melt (8) can be maintained at constant by adjusting the heat exchange area, so that polycrystal silicon ingot having good characteristics can be produced with good reproducibility.

A method of creating thin wafers of single crystal silicon wherein an ingot of single-crystal silicon with a (111) axis is flattened and polished at one end normal to the axis, and a notch with a vertex in the (111) plane is produced on a side or edge of the ingot, such that the distance between this vertex and said end is the desired thickness of a wafer to be cleaved from the ingot and such this vertex is in the desired plane of cleavage. Light of a wavelength able to penetrate into the silicon crystal without significant absorption, when the intensity of the beam is low, but is efficiently absorbed and converted to heat when the intensity of the beam is high, is focused to an elongated volume with an axis of elongation in the desired cleavage plane, parallel to and a short distance from said notch edge. Heating and the resulting transient local expansion of the silicon in this illuminated volume causes tensile stress at the vertex of said notch, substantially normal to the desired cleavage plane, thereby causing fracture of the crystal in the chosen cleavage plane. Movement of the illuminated volume relative to the ingot allows the fracture to propagate across the desired cleavage plane, thereby completely severing the wafer from the rest of the ingot.

The invention relates to a tin-base leadless solder without silver, and relative production. Wherein, it comprises Bi at 7.5-60% (without 7.5%), Cu at 0.1-3.0%, and the left is tin; and it also can contain Zn, Ni, P, Ge, Ga, In, Al, La, Ce, Sb, Cr, Fe, Mn, or Co while the total amount of micro alloy element is not higher than 1.0%. And the production comprises that in protective gas or vacuum, smelting middle alloy Sn-Cu10; then smelting into leadless solder alloy ingot which can be used as solder directly or be made into bar band, wire plate or powder. The inventive solder has low cost while its fusion point can be controlled between 140 and 230Deg. C. And it has strong anti-oxidization and anti-corrosion properties.

This invention discloses a method for increasing sintered Nd FeB coercive force by adding nm oxide in grain-boundary phase including the following steps: 1,applying casting technology to produce NdFeB ingot alloy or applying rapid hardening film technology to produce NdFeB rapid hardening film of with host phase alloy, applying casting technology to produce ingot alloy or rapid hardening film technology to get rapid hardening film or rapid quench technology to manufacture a rapid quench strip with the grain boundary phase alloy, 2, processing powder with the two alloys, 3, adding a nm oxide to the grain boundary phase alloy powder, 4, pressing the mixed powder into formation, 5, producing sintered magnetic body in a vacuum sintering oven.

The invention discloses a processing method for a TC4 titanium alloy large-sized bar. The method comprises the following steps of: cogging and forging TC4 titanium alloy ingots for 2 to 3 heating times to obtain forging billets; 2, upsetting the forging billets repeatedly and performing drawing-out forging for 2 to 3 heating times; 3, upsetting the forging billets subjected to forging repeatedly and performing drawing-out forging for 3 to 5 heating times; and 4, performing chamfering round forging on the forging billets subjected to forging for 2 heating times to obtain the TC4 titanium alloy large-sized bar with the diameter of 200 to 400 mm and length of not less than 2,500 mm. The TC4 titanium alloy bar processed by the method has uniform and fine grains, few internal defects and high safety and accords with the domestic advanced level of the like products. In the processed TC4 titanium alloy bar, the room-temperature tensile strength is 920 to 960 MPa; the yield strength is 830 to 870 MPa; the elongation percentage is not less than 12 percent; the contraction ratio of the cross section is not less than 36 percent; flaw detection clutter reflects small signals; and the flaw detection level is high.

The invention discloses an ultrahigh-strength Al-Zn-Mg-Cu system aluminum alloy large-size flat cast ingot and a making method thereof, and belongs to the aluminum alloy making field. The flat cast ingot comprises, by mass, 2.0-2.4% of Cu, 1.95-2.5% of Mg, 5.5-9.0% of Zn, 0.08-0.15% of Zr, 0.0003-0.0015% of Be, below 0.06% of Ti, below 0.04% of Cr, below 0.10% of Mn, 0.085% or less of Si, 0.14% or less of Fe, and the balance Al and inevitable elements, wherein the content of each of the inevitable elements is lower than 0.05%, the total amount of the inevitable elements is lower than 0.15%, and a content ratio of Fe to Si is not less than 1.6. The making method disclosed in the invention improves traditional making methods, and does not need pure aluminum bottoming, and the flat cast ingot made in the invention has the advantages of large size, high strength, no cracks, and high casting success rate.

The invention relates to the production of bulky monocrystalline metal or semi-metal bodies, in particular of a monocrystalline Si ingot, using the vertical gradient freeze (VGF) method by directional solidification of a melt in a melting crucible having a polygonal basic shape.

According to the invention, the entire bottom of the melting crucible is completely covered with a thin seed crystal plate made of the monocrystalline semi-metal or metal. Throughout the procedure, the bottom of the melting crucible is kept below the melting temperature of the semi-metal or metal in order to prevent melting of the seed crystal plate.

Monocrystalline ingots produced in this way are distinguished by a low average dislocation density of for example less than 10⁵ cm⁻², allowing the production of very efficient monocrystalline Si solar cells.

The invention relates to high-performance marine mooring chain steel and a manufacturing method thereof. The method comprises the following steps: a. tapping compositions comprise the following by weight percentage: C: 0.16 to 0.27, Mn: 0.40 to 1.45, Si: 0.15 to 0.50, Cr: 1.25 to 2.50, Ni: larger than 0 and less than 1.20, Mo: 0.20 to 0.60, Al: 0.01 to 0.06, N: 0.004 to 0.015, S: not larger than 0.005, P: not larger than 0.015, Cu: larger than 0 and less than 0.50, and the balance of Fe; b. a steel ingot or a continuous casting billet is casted after the steps of primary smelting in an electric stove or a converter, external refining and vacuum degassing; c. the charging temperature of a heating oven is not larger than 900 DEG C, the heating rate is not larger than 150 DEG C/h; when being raised to 1100 to 1300 DEG C, the temperature is kept for more than 40 minutes, cogging bloom or rolling by a finisher is carried out, and the finishing temperature is not larger than 1050 DEG C; and d. after heated at the temperature of 1000 to 1250 DEG C, the cogged ingot is hot-rolled or forged into round steel, the finishing temperature is not larger than 1050 DEG C, and after rolling, the steel is air-cooled, slow cooled or softening heat-treated at the temperature of not less than 600 DEG C. The performance of finished products achieves or exceeds the requirement of level 4.5 and level 5 of mooring chain steel.

A method for spalling a layer from an ingot of a semiconductor substrate includes forming a metal layer on the ingot of the semiconductor substrate, wherein a tensile stress in the metal layer is configured to cause a fracture in the ingot; and removing the layer from the ingot at the fracture. A system for spalling a layer from an ingot of a semiconductor substrate includes a metal layer formed on the ingot of the semiconductor substrate, wherein a tensile stress in the metal layer is configured to cause a fracture in the ingot, and wherein the layer is configured to be removed from the ingot at the fracture.

A method of fabricating substrates while minimizing loss of starting material of an ingot, wherein a layer is transferred onto a support. The technique includes forming a flat front face on a raw ingot of material, implanting atomic species through the front face to a controlled mean implantation depth to create a zone of weakness that defines a top layer of the ingot, bonding a support to the front face of the ingot, wherein the support has a surface area that is smaller than a surface area of the front face of the ingot, and detaching from the ingot at the zone of weakness that portion of the top layer that is bonded to the support to form the substrate.

A method of preparing a polycrystalline silicon for solar batteries adopts combined means of silicon monoxide disproportionation, acid dipping separation and vacuum melting and processes by the following procedures: (1) the silicon monoxide is made from chemical pure industrial silicon and high purity sand quartz. (2) the high purity silicon is obtained by disproportionation of the silicon monoxide. (3)impurities boron and phosphorus in the silicon are removed by soaking with aquafortis. (4) the high purity silicon is further purified by melting of a vacuum electro beam furnace, and parts with impurities heavily gathered in a cast ingot are cut. (5) nitrogen or nitrogen plus hydrogen is fed into a plasma furnace for melting, so as to further remove the rest boron, phosphorus and other impurities, and conduct directional solidification. (6)the outer skin and parts with impurities heavily gathered of the cast ingot are cut, and finally the high purity silicon which is above 6N pure and applicable to solar batteries is obtained. The invention rejects the technical route of the Siemens method, prevents environment pollution, improves safety of production, and is good for promotion and application in China.

The invention discloses a method for recovering polysilicon ingots, carborundum powder and polyethylene glycol from cutting waste mortar. The recovering method comprises the following steps shown as an attached diagram, wherein the high temperature purification comprises the following steps of: mixing the prepared silicon micro powder with a fluxing agent according to the weight ratio of 1: 0.5-5 into lumps, carrying out high temperature treatment in a high temperature vacuum furnace with the treatment temperature range of 1450-1800 DEG C and the treatment time range of 1-10h; and then carrying out directional solidification on melting-state high purity silicon subjected to the high temperature treatment to obtain the polysilicon ingots; wherein the fluxing agent is selected from one or any mixture of silica, alumina, calcium oxide, magnesium oxide, potassium oxide, sodium oxide, calcium fluoride, magnesium fluoride, sodium fluoride, sodium chloride, potassium chloride and calcium chloride. The invention has the advantages that: the yields of carborundum and polyethylene glycol are high and can reach more than 70-80 percent; and the recovered polysilicon ingots reach the purity of 6-7N and completely satisfy of the requirement for preparing silicon slices of silicon solar cell.

The invention relates to a method for producing a wind-power mainshaft by local continuous upsetting and all-fibre upset forging. The method comprises the following: step one, the heating of steel ingot; step two, forging; step three, first heat processing; step four, rough machining and ultrasonic inspection; step five, quenching and tempering and heat processing; step six, fine machining, wherein, during the step two, the forging comprises that: (1) a first fire, during which, a steel ingot is subject to upset forging at a forging temperature of between 1250 and 900 DEG C; firstly, the bottom of the steel ingot is sawed off, and the steel ingot is subject to capping and upset forging; (2) a second fire, during which, the steel ingot is stretched towards various directions, marked and subject to intermediate billet cogging; after a pole part is molded, scrap on a T end is chopped and removed; after the forging is finished, the steel ingot returns to a heating furnace for being reheated; (3) a third fire, during which, the steel ingot is subject to local continuous upsetting and all-fibre upset forging; (4) a fourth fire, during which, the steel ingot is subject to rolling and leveling; the pole part is stretched; the disc edge of a hub end on the head part of an intermediate billet material after the local continuous upsetting and all-fibre upset forging is subject to rolling operation; after the rolling, the intermediate billet material is inserted into a leaking disc component again; the end face of the disc is pressed and leveled; after the shaping of the disc end is completed, a manipulator clamps the disc and stretches the pole part of the intermediate billet material to a dimension of a forgeable piece; thus, the mainshaft forging is completed. The method can improve the fatigue resisting strength of a wind-power mainshaft forging piece.

A kind of alloy, which is anti-squirming, and the components of it and the weight percent of them is: 1.5-10%Y, 0.15-2.0%Zr, 0.3-2.0%Nd, 2.5-8%Gd, and one kind or several kinds of components among Sm, Dy, Tb, Ho, Er, Tm and Eu is also contained, the other is Mg. the following steps are contained in the method: (1) To prepare material (2) To improve the temperature of warm-up stove and melting stove (3) To warm up the material (4) To melt the purified magnesium ingots in batches (5) To melt the other materials, which has been warmed up, in the Mg solution. (6) To distribute equably the alloy components in the Mg solution. (7) To make into casting ingot, cast, billet, board material, pipe material, model material, stick material, line material and all kinds of forged piece. The Mg alloy can fulfill the need owing a higher mechanics performance and anti-squirming performance under high temperate, and the anti-causticity performance is higher than the Mg in existence.