The invention discloses a
copper-
tungsten alloy waste cleaning and recycling method based on
hydrogen reduction, belongs to the technical field of non-
ferrous metal waste cleaning
metallurgy and resource circulation, and aims at solving the problems that a traditional recycling method is high in
energy consumption, complex in process, heavy in secondary
pollution, difficult to consider both the
metal recycling rate and the
metal purity, large in high-temperature
operation safety risk and the like. According to the method, the
tungsten-
copper alloy waste is sequentially subjected to primary crushing, oxidation, primary reduction, separation, secondary reduction, screening,
tertiary reduction, secondary crushing,
airflow pulverization, acid
pickling and
impurity removal and other procedures, cooperative operation is carried out in cooperation with special equipment such as an oxidation reaction tank and a reduction reaction kettle, and meanwhile mixture separation and a
hydrogen internal circulation
system are integrated; efficient cleaning, separation and extraction of
tungsten and
copper are achieved, and the energy utilization and resource circulation level is improved.
Tungsten and copper are separated thoroughly, the product purity is high,
energy consumption is low, the metal
recovery rate is high, no three wastes are discharged in the whole process, the green low-carbon
circular economy concept is met, the
recovery rate of the obtained tungsten
powder and copper
powder is larger than or equal to 99%, the
oxygen content is smaller than 0.05 wt%, and the particle size uniformity is excellent.