401 results about "Liquid interface" patented technology

The present application provides a method for generating a micro-scale columnar high-speed acoustic beam in a liquid environment, comprising: a liquid environment; a high-frequency resonator, which generates 0.5-30 GHz ultrasonic waves to act on the liquid environment during operation, generating a directional fluid motion along the direction of propagation of the sound wave in the liquid at the solid-liquid interface, i.e., a columnar focused acoustic beam; the high-frequency resonator is driven to operate in at least one driving cycle with a first power, each driving cycle including a first stage and a second stage, the first stage driving the high-frequency resonator to operate, and the second stage stopping the driving; the magnitude of the first power causes the high-frequency resonator to generate an acoustic beam in the first stage; and the duration of the first stage at the first power is less than the second threshold or the duty cycle of the first stage in one driving cycle is less than the first threshold. Corresponding applications are also provided, such as a method for directional transport of liquids or particles in liquids, and a method for processing target objects.

The invention relates to the technical field of chemical automation control, and discloses an intelligent closed-loop control system for producing p-dichlorobenzene by a biomass method, which comprises a signal acquisition module, a residence time reconstruction module, a thermal coupling analysis module, a parameter self-adaptive scheduling module and an execution control module. The rheological characteristics of raw materials are monitored by collecting the current of a stirring motor, the liquid level is dynamically increased through a retention time reconstruction module to prolong the retention time of the materials, and a liquid level periodic migration strategy is introduced to prevent scaling of a gas-liquid interface; the thermal coupling analysis module and the parameter self-adaptive scheduling module are used for calculating thermal retardation post factors, temperature control parameters are corrected in real time, the upper limit of cooling output is limited, inner wall supercooling crystallization is prevented, and the problems that the conversion rate is reduced, the heat transfer efficiency is reduced and equipment is hung on the wall due to viscosity fluctuation of biomass raw materials are effectively solved. And the self-adaptive stable control of the reaction process is realized.

The invention discloses a liquid hydrogen container heat leakage prediction and boost characteristic detection method and system. The method comprises the following steps: establishing a three-dimensional heat flow field model of a liquid hydrogen container; calculating the heat flow density of a gas-liquid interface based on the three-dimensional heat flow field model so as to adjust the liquid hydrogen evaporation capacity; total heat leakage is obtained through finite element simulation and experimental data collaborative calibration; calculating a static evaporation rate according to the total heat leakage; establishing a nonlinear mapping model of the static evaporation rate and the boost rate through a response surface regression method; the wall temperature distribution of the liquid hydrogen container is monitored in real time, thermophysical parameters are calibrated through the LSTM neural network by adopting a dynamic calibration algorithm, and the output result of the three-dimensional heat flow field model is corrected. By establishing a three-dimensional heat flow field model of the liquid hydrogen container, determining a nonlinear response relationship between the evaporation rate and the pressure rising rate of the liquid hydrogen container, and constructing a cloud-edge collaborative detection system, the heat leakage performance of the liquid hydrogen container is accurately predicted, and efficient pressure rising rate detection is realized.

The invention relates to a preparation method of a silicon single crystal rod and a silicon wafer. Comprising a melting stage, a temperature adjusting stage, a welding stage, a seeding stage, a shouldering stage, an equal-diameter stage, an ending stage and a breaking stage which are carried out in sequence, in the equal-diameter stage, the pulling speed is controlled to be within a first pulling speed range, and the solid-liquid interface temperature gradient is controlled to be within a first gradient range; wherein the range of the first pulling speed ranges from 0.5 mm / min to 1.1 mm / min; the first gradient range is 3 DEG C / cm to 5 DEG C / cm. By reducing the temperature gradient of a solid-liquid interface and lowering the crystal pulling rate, the stability of a thermal field is enhanced, and sufficient conditions are provided for the composite reaction of Sii and V, so that the impurity capturing efficiency is improved, the internal purity of the crystal is improved, and the impurities are effectively removed.

The invention provides a gas-liquid interface identification and ship sloshing liquid level correction method and system, and the method comprises the steps: extracting image edge and gray texture features, achieving the state identification of a liquid-gas interface through a lightweight convolutional neural network model, and dynamically generating a collection strategy according to the state identification; then collecting original liquid level signals and synchronously obtaining IMU data, extracting a multi-mode component through signal decomposition, constructing a disturbance recognition model by combining an IMU, filtering disturbance related components and reconstructing a stable liquid level; and further modeling the disturbance component into a residual sequence, realizing disturbance trend prediction and liquid level dynamic correction by using a time sequence prediction model, and outputting more stable and reliable liquid level data. The problem that liquid level measurement is unstable in the LNG ship sloshing environment can be effectively solved, image recognition and IMU data are fused, liquid level disturbance suppression and dynamic correction are achieved, and the method has the advantages of being self-adaptive, resistant to interference, stable in measurement and the like and is suitable for high-precision liquid level monitoring under the complex working condition.

The invention provides a horizontal coalescence phase splitter suitable for phase-change absorbent lean and rich liquid phase splitting. The horizontal coalescence phase splitter sequentially comprises a section I phase splitting buffer area, a section II coalescence phase splitting area and a section III gravity phase splitting area in the fluid flowing direction. The I-section split-phase buffer area is provided with a tangential feeding hole and a flow guide baffle plate; the section II coalescence split-phase area is filled with stainless steel mesh coalescence filler subjected to composite modification of AP adhesive and nano Al2O3; and a heavy phase outlet and a light phase outlet are formed in the section III gravity phase-splitting area. According to the horizontal phase splitter, the gas-liquid interface area is large, the gas-liquid movement directions are perpendicular to each other, gas-liquid phase balance is facilitated, and the separation effect is better; in addition, the liquid level is stable, when the incoming liquid flow changes, the liquid level change of the horizontal separator is small, the buffering capacity is high, and stable flow can be provided for downstream equipment; in addition, by adding the composite modified stainless steel mesh coalescence filler into the phase splitter, tiny liquid drops can be effectively captured and coalesced, the separation effect is further improved, and comprehensive liquid-liquid separation is achieved.

The invention provides a single crystal furnace crystal pulling ending parameter control method and system based on adaptive regulation, and the method comprises the steps: collecting production data and parameter data of an ending starting point through a distributed sensor network and a processing equipment interface, and processing the data to obtain current state data of a crystal; and performing similarity comparison on the current state data of the crystal to obtain initial process parameters of the ending stage, and deducing and predicting state expectation evolution data of the crystal in the ending process based on the current state data of the crystal and the initial process parameters. According to the method, through the synergistic effect of full-state perception, foresight deduction, risk quantification and self-adaptive regulation and control, the bubble capture risk index is stably controlled to be 0.5 or below, the stability of a solid-liquid interface in the ending stage is improved, the technological process is not affected by the experience level of operators, and the optical uniformity consistency between batches is greatly improved.

A crystal pulling method and system for fabricating a large-diameter silicon single crystal, and a silicon single crystal and a medium. The method can comprise: performing global two-dimensional simulation on a crystal pulling process, and acquiring a global temperature distribution, a velocity field distribution and an initial solid-liquid interface value during the crystal pulling process under a preset crystal pulling apparatus and a preset crystal pulling parameter; on the basis of the global temperature distribution and the velocity field distribution, determining a boundary condition, and on the basis of the boundary condition, performing local three-dimensional simulation on the crystal pulling process to determine a target solid-liquid interface value; adjusting the preset crystal pulling parameter until the initial solid-liquid interface value is equal to the target solid-liquid interface value within a threshold range, and using the adjusted preset crystal pulling parameter as a reference crystal pulling parameter; on the basis of the reference crystal pulling parameter, simulating and calculating a simulated defect during the crystal pulling process; on the basis of the simulated defect, iteratively optimizing the reference crystal pulling parameter until the simulated defect meets a preset condition, and using the optimized reference crystal pulling parameter as a target crystal pulling parameter; and fabricating a defect-free silicon single crystal.

The invention discloses a multi-scale research method for improving the separation efficiency of impurities in an ultra-pure metal system. The multi-scale research method comprises the following steps that tellurium crystals are prepared through a zone melting method, and purity and crystal face orientation analysis is conducted; simulation analysis is carried out in combination with experimental data, firstly, phase field simulation is used for analyzing conversion of an interface structure and grain competition-driven orientation in the solidification process, then the density functional theory is used for calculating and analyzing adsorption energy of solid phases on different crystal faces at the solid-liquid interface to impurity atoms, and the structure-activity relationship between crystal face orientation and impurity separation efficiency is obtained. Finally, the crystal face and the preferred orientation degree of the tellurium crystal are regulated and controlled through a Bridgman method, and the impurity separation efficiency is improved. By means of the mode, the key factors influencing trace impurity atom separation can be obtained, the universal method for improving the impurity separation efficiency in the ultra-pure metal system is obtained, and development of the non-ferrous metal metallurgy field is promoted.

The invention discloses an oxygen-enriched destressing crystal growth method and a crystal growth furnace, and relates to the technical field of crystal growth, and the oxygen-enriched destressing crystal growth method comprises the following steps: step 1, pre-treating a PMNT polycrystal material, and putting the pretreated PMNT polycrystal material into a crucible; 2, pre-flushing the growth furnace and creating an oxygen partial pressure environment; 3, raising the temperature in the growth furnace to melt and homogenize the PMNT polycrystal material in the crucible; step 4, the crucible moves downwards for directional solidification of the crystal, a solid-liquid interface is formed and stably moves upwards, and in the process, a dynamic regulation and control strategy is adopted in the growth furnace to control an oxygen-enriched environment to promote crystal growth, so that the crystal digests growth stress in the growth process, and formation of oxygen vacancies is inhibited; and step 5, after crystal growth is finished, gradient cooling is performed to room temperature in an oxygen-enriched environment, and a crystal ingot is obtained. Oxygen is used as a regulation and control tool, the stress problem caused by oxygen vacancy is physically solved, the color center and performance problems caused by oxygen vacancy are chemically solved, and the crystal growth quality is improved.

The invention provides a thermal response hydrogel construction method based on solid-liquid interface repulsive force and water content, which comprises the following steps: establishing a coarse graining model of a thermal response polymer network and a water molecule system, and constructing a three-dimensional polymer gel network by adjusting the number of polymer chain monomers and the proportion of a cross-linking agent; constructing a simulation box according to the network geometric dimension and filling the simulation box with water beads; defining interaction parameters among beads under the dissipative particle dynamics model, performing molecular dynamics simulation, counting the mass center of a polymer skeleton and the number of water beads adjacent to an interface, and calculating the equilibrium moisture content; establishing a solid-liquid interface model, and calculating an equilibrium distance and interaction energy between a water bead plane and a polymer skeleton plane at the adsorption temperature; the network polymerization degree is optimized by adjusting the number of polymer chain monomers, and the optimal design of the thermal response desorption performance is achieved. The method provided by the invention is suitable for macroscopic hydrogel structure evaluation, can quickly obtain equilibrium moisture content and interfacial interaction energy, and guides reasonable proportioning and preparation of the hydrogel.

The invention discloses a control method for optimizing a solid / liquid interface of a solution in indium Czochralski purification based on numerical simulation, belongs to the technical field of preparation of high-purity metal materials, and obtains a process regulation and control scheme for stabilizing the solid / liquid interface of the solution through an external magnetic field and establishment of a mapping relation of process parameters-interface data-impurity concentration based on multi-physics field numerical simulation. The method comprises the following steps: acquiring original physical property data of the czochralski furnace and indium, calculating a geometric model, performing mesh generation, and establishing a mathematical model; based on historical experimental data, boundary conditions are set, and the key processes of indium czochralski purification seeding, shouldering and equal diameter are simulated; coupling multiple physical fields, and analyzing the change of a solid / liquid interface of the solution in the direct pulling process; and on the basis of a numerical simulation result, a deep reinforcement learning model is constructed, a mapping relation among process parameters, interface data and impurity concentration is established, 'prediction-verification-optimization 'closed-loop iteration of the process is realized, and collaborative regulation process parameters for stably preparing 8N high-purity indium are obtained.

The embodiment of the invention provides a crystal pulling heating power regulation and control method, device and equipment and a storage medium, and belongs to the technical field of monocrystalline silicon material production. The method comprises the steps that real-time crystal pulling parameters are obtained, wherein the real-time crystal pulling parameters comprise the real-time residual material weight and the real-time crystal pulling speed; based on the real-time residual material weight, the real-time crystal pulling speed and a pre-constructed mapping table, the current heating compensation power is determined, the current crystal pulling heating power is regulated and controlled through the heating compensation power, and the mapping table comprises the mapping relation of the residual material weight, the crystal pulling speed and the compensation power. According to the invention, based on the real-time crystal pulling parameters, the proper current heating compensation power can be rapidly determined by using the pre-constructed mapping table, so that the crystal pulling heating power is regulated and controlled to maintain the solid-liquid interface temperature of the silicon material in the crucible, the stability of the crystal pulling process is improved, and the occurrence of abnormal crystal pulling is reduced.

The present invention discloses a bionic regulation method for a number of bounces of a droplet on a metal surface based on acoustic in-situ monitoring, which comprises the following steps: obtaining dynamic contact characteristics and acoustic properties of a solid-liquid interface of metal superhydrophobic surfaces with different surface information in the droplet bounce process based on an optical-acoustic synchronous in-situ testing system for droplet bounces; and obtaining a correlation among the metal superhydrophobic surface, the acoustic response and the droplet bounce behavior based on the dynamic contact characteristics and the acoustic properties of the solid-liquid interface, and machining and modifying a micro-nano structure of the metal surface by combining a coupled bionic concept according to the correlation. A scientific basis and a novel design method are provided for the bionic regulation of the number of droplet bounces over the metal surface.

The invention relates to the technical field of solid-liquid interfaces and liquid drop movement and control, in particular to a method and device for achieving left-right controllable spontaneous rotation of liquid drops based on light induction, and the method comprises the following steps that acid liquid drops containing photoacid are dropwise added to the surface of liquid metal; a light source system is adopted to irradiate liquid drops on one side of the liquid drops, the liquid drops are induced to locally release non-uniform H < + > ions, and interface chemistry is initiated to generate gradient change distribution; the light intensity generated by the light source system promotes the formation of asymmetric tension distribution on the liquid drop and liquid metal interface, and drives the liquid drop to rotate along a preset direction; and by changing the irradiation position, the liquid drops can be switched between left rotation and right rotation. According to the present invention, by using the mechanism of combining the interface Marangoni effect and the light-induced acidity regulation and control, the stable and rapid spinning behavior of the liquid drop can be represented by adjusting the position, the irradiation time and the irradiation intensity of the illumination region, and the rotation direction can be reversibly switched between the left rotation and the right rotation.

The invention provides a multifunctional experimental system for simulating migration and transformation of micro-plastics in a landfill environment, comprising: a columnar migration device filled with a landfill soil medium, the bottom of which is provided with a liquid inlet interface and a gas-liquid interface, and the top of which is provided with a liquid outlet; the liquid inlet system is connected to the liquid inlet connector through a first peristaltic pump; the temperature control module comprises a flexible heating film arranged around the outer wall of the columnar migration device and a temperature controller, and the flexible heating film is connected with the temperature controller through a temperature control connector, an integrated heating element and a wire; the micro-nano bubble generating device comprises a CH4 gas cylinder, a pressure reducing valve and a micro-nano bubble generator which are connected in sequence, a micro-bubble aeration head is arranged on the micro-nano bubble generator, the micro-bubble aeration head is partially and directly immersed in a preset water body, a high-dispersity bubble water solution is generated under a gas-liquid interface, and the CH4 gas cylinder is used for generating CH4 gas. The gas is quantitatively conveyed to the bottom of the columnar migration device through a second peristaltic pump connected to the downstream, and the dissolution of the landfill gas in the pore water and the gas-liquid interface action are simulated.

The utility model discloses a device for eliminating fine crystals in a sodium sulfate cooling crystallization process, which is characterized in that a #-shaped partition plate is arranged below a top cover of a crystallizer, a cross-shaped flow channel formed in an inner baffle of the partition plate comprises radial branches, each radial branch is provided with a fine crystal liquid interface, a hot material liquid backflow interface and a circulating liquid interface, each fine crystal liquid interface is close to the center of the top cover, and each hot material liquid interface is close to the center of the top cover. A hot material liquid backflow connector is arranged on the outer side of the crystallizer and is close to the inner wall of the crystallizer; each fine crystal liquid interface is connected with an inlet pipeline of the fine crystal circulating pump, an outlet of the fine crystal circulating pump is connected with a tube pass inlet of the heat exchanger, and a tube pass outlet of the heat exchanger is connected with the hot material liquid backflow interface; each circulating liquid interface is connected with a suction port pipeline of a feed liquid circulating pump, an outlet of the feed liquid circulating pump is connected with a tube pass inlet of an external cooler, a tube pass outlet of the external cooler and a sodium sulfate solution feeding pipe are jointly connected with a feeding port of a crystallizer, and a crystal mush outlet is formed in the lower part of the side wall of the crystallizer. The device can improve the particle size of product cooling crystallization and prolong the cleaning period of the external cooler.

The invention discloses an indium phosphide single crystal growth dynamic thermal field control method based on AI calibration of multiple temperature zones, and relates to the technical field of semiconductor material preparation and artificial intelligence control. According to the method, a multi-temperature-zone thermal field digital twin model is constructed, multi-channel temperature data, heating power data and crystal growth image data in an indium phosphide single crystal growth furnace are collected, and real-time three-dimensional reconstruction of thermal field distribution in the furnace is carried out; with the crystal growth rate, the solid-liquid interface shape and the thermal stress distribution as optimization targets, power adjustment instructions of heaters in all temperature zones are output; an AI calibration module is introduced to correct thermophysical parameters of the digital twin model; deducing a thermal field state at a future moment, compensating a thermal hysteresis effect in advance, and realizing accurate closed-loop control of an indium phosphide single crystal growth process; according to the invention, the problem that the traditional PID control is difficult to cope with nonlinear, strong-coupling and large-lag thermal field change in large-size crystal growth is solved, and the single crystal yield and the lattice quality are remarkably improved.

According to the invention, heavy arsenic doping 1t is reduced; 111gt, 111gt; the invention relates to a crystal pulling method based on crystal orientation monocrystalline silicon section defect density and a monocrystalline silicon rod, and belongs to the technical field of monocrystalline silicon pulling. In the equal-diameter process, the liquid opening distance is constant, the pulling speed of the crystal bar is gradually reduced according to the length of the crystal bar, and the ratio (CR / SR) of crystal rotation / pot rotation is adjusted, so that heat conduction is uniformly transmitted in the radial direction of the crystal bar by controlling the growth rate of crystals, the temperature gradient of a solid-liquid interface and precipitation of oxides, and the heat conduction efficiency is improved. And in the crystal growth process, point defects such as interstitial atoms and vacancies have more opportunities to diffuse outwards, so that the generation of the point defects and impurity decorations is inhibited, the defect density of the section of the single crystal silicon rod is reduced, and the quality of the heavily arsenic-doped crystal rod is improved.

The invention discloses a low-temperature liquid storage tank pressure prediction method based on a non-thermal equilibrium state model, and aims to improve the calculation speed of a pressure evolution law so as to reduce the time required for predicting the pressure of a storage tank. The method comprises the steps that firstly, a pressure sensor, a temperature sensor and a liquid level meter are used for collecting the temperature of a current gas phase and liquid phase area of the low-temperature liquid storage tank, the pressure in the storage tank, the vacuum degree of a heat insulation layer and the real-time liquid level; secondly, transmitting signal data obtained by monitoring of the sensor to a processor, and checking the density, phase change latent heat and thermodynamic energy of gas and liquid phases in the storage tank through REFPROP software; then establishing a three-dimensional model and a heat and mass transfer relationship of the storage tank, and performing heat transfer analysis on gas-phase and liquid-phase media in the storage tank; secondly, performing energy analysis on a gas phase region, a liquid phase region and a gas-liquid interface in the storage tank according to the established three-dimensional model and a heat transfer analysis result, and selecting a proper time step to perform iterative calculation so as to ensure the calculation precision of each step; storing the calculation result of the previous step, and searching and taking thermodynamic parameters of the next time step through REFPROP software according to the parameters obtained through calculation; finally, the safe storage time of the storage tank under the current liquid filling volume and the heat insulation performance is calculated, and safe work of the storage tank is guaranteed.

The invention belongs to the technical field of reactor thermal hydraulic tests, and particularly relates to a device for measuring steam-water direct contact condensation. The device comprises an upper cylinder body, a lower cylinder body, an upper sealing head and a lower sealing head, the upper sealing head, the upper cylinder body, the lower cylinder body and the lower sealing head are connected from top to bottom to form a sealed cylinder body structure; a visual mirror is arranged on the lower cylinder body, and the axial height of the visual mirror covering the lower cylinder body is more than 1 / 2; an electrode wire measuring structure is arranged at the joint of the upper cylinder and the lower cylinder and is used for capturing the vapor-liquid interface contact area; a through hole is formed in the upper sealing head, a steam outlet of the steam inlet connecting pipe is connected into the barrel structure through the through hole, and the steam outlet is connected with a steam diffuser. The vapor-liquid interface contact area can be obtained directly through visual shooting and later graphic processing, the vapor-liquid effective contact area can be quantitatively measured through the electrode wire, and therefore the vapor-water direct contact condensation heat transmission intensity is quantified.

The utility model discloses a solid-liquid interface detection device and crystal growth equipment, the solid-liquid interface detection device comprises a fixed ring, a distance measuring assembly and a connecting frame, the fixed ring is suitable for sleeving outside a crystal bar and is fixed with the crystal bar, the distance measuring assembly and the fixed ring are arranged at an interval along the axial direction of the fixed ring, and the distance measuring assembly is connected with the connecting frame. The distance measuring assembly is suitable for being arranged at an interval with the growth interface of the crystal bar, the distance measuring assembly comprises a mounting frame and distance measuring units, the distance measuring units are used for acquiring the distance between the distance measuring units and the growth interface, the connecting frame is connected with the fixing ring and the mounting frame, and the multiple distance measuring units are arranged on the mounting frame at intervals in the direction perpendicular to the axial direction of the fixing ring. Therefore, the solid-liquid interface detection device can more conveniently and accurately measure the morphology of the growth interface of the crystal bar, so that process parameters can be better configured, and crystals with better quality can be obtained in the crystal production process.

This invention relates to the technical field of surface lubrication and friction measurement of machinery, and provides an apparatus and method for measuring the energy barrier at the surface solid-liquid interface of a microstructure. [Solution] The apparatus includes a micro-pump, a fixed elbow, a capillary tube, an upper contact surface, a lower contact surface, a droplet, a micro-movement stage, and a high-speed microscope camera. In this method, the micro-pump transports liquid to form a droplet between the upper and lower contact surfaces, the micro-movement stage is used to drag the lower contact surface at a constant speed to slide the droplet, and the high-speed camera monitors the deflection deformation caused by the droplet drag force of the capillary tube, calculates the dynamic drag force, and integrates the drag force-displacement curve to obtain the energy consumed by the droplet to overcome the microstructure. Finally, the solid-liquid interface energy barrier per unit area is obtained, overcoming the limitations of the conventional contact angle method, which cannot measure the dynamic interface energy barrier, and enabling direct and quantitative measurement of the surface solid-liquid interface energy of the microstructure.

The invention belongs to the technical field of spectral analysis and catalytic reaction monitoring, and particularly relates to a rapid scanning detection method and device based on flow stopping and in-situ infrared combination.The device comprises an infrared spectrometer, a signal sending module, a control module and a reaction module, and the reaction module is used for providing a heterogeneous reaction site; the infrared spectrometer is used for monitoring the reaction in the reaction module, the signal sending module is connected with the infrared spectrometer through the control module to control starting and stopping of scanning of the infrared spectrometer, and the signal sending module is further used for receiving and analyzing infrared signals collected by the infrared spectrometer; the reaction module comprises a crystal table, the crystal table is located in a test light path of the infrared spectrometer, a catalyst film is arranged on the upper surface of the crystal table, a buffer layer is arranged on the surface of the catalyst film, and a sample injector is arranged above the buffer layer and used for injecting a reaction solution into the surface of the buffer layer. According to the invention, intermediates and reactants of a solid-liquid interface can be synchronously collected and tracked.

The invention discloses a phase field method suitable for crystal growth under diffusion control in a molten salt system, and belongs to the field of numerical simulation of crystal growth in the molten salt system. According to the method, numerical simulation of the crystal growth process in the molten salt system is realized through the steps of geometric modeling, grid division, free energy function construction, order parameter and concentration evolution equation establishment, solution and the like. The method comprises the following steps: establishing a two-dimensional geometric model containing a crucible wall surface and a molten salt medium, and dividing grids; constructing a system free energy density functional; establishing a sequence parameter and concentration parameter evolution equation; and finally, calculating a phase field parameter and a physical property parameter of the single crystal material, and substituting the parameters into the equation for iterative solution to obtain a convergence solution of the sequence parameter and the concentration. Compared with the prior art, the method has the advantages that a solid-liquid interface does not need to be directly tracked, the model complexity and the calculation cost are reduced, the calculation requirement can be quickly responded, and the molten salt body ion concentration distribution can be calculated; the method can be applied to monitoring and prediction of the process of growing the single crystal material by the molten salt method.

The invention belongs to the technical field of semiconductor material processing, and particularly relates to a method for improving an OISF defect of an 8-inch light phosphorus-doped single crystal and a product thereof, and the method comprises the following steps: in the crystal pulling process, reducing the pulling speed, flattening a solid-liquid interface, balancing the growth rate and the release of thermal stress, so as to reduce the thermal stress and inhibit the formation of the OISF defect; the liquid opening distance is increased, the increase of the liquid opening distance enables the crystal to experience a slower cooling rate in the growth process so as to reduce the accumulation of thermal stress, so that the dislocation defect in the crystal is reduced, dislocation is a potential nucleation point of OISF, and therefore, the increase of the liquid opening distance can inhibit the formation of the OISF defect; after the crystal growth is finished, the cooling rate is increased, so that a crystal bar quickly passes through a temperature interval, the generation of O2V is reduced, the generation of OISF defects is avoided, oxygen atoms are in a solid solution state in the silicon crystal at high temperature, and the higher cooling rate can inhibit the diffusion and aggregation of oxygen, reduce the formation of oxygen precipitates, reduce the density of the OISF defects and also avoid the generation of the OISF defects; therefore, the OISF defect of the 8-inch light phosphorus-doped single crystal is reduced, and the electrical property of the 8-inch light phosphorus-doped single crystal is improved.

The embodiment of the application provides a kind of mineral dissolution precipitation simulation model construction method, device and equipment, it is related to oil and gas field development field, the method is by obtaining shale mineral image and dividing boundary grid, the spatial position of solid-liquid reaction interface is clear, secondly, the calculation formula of net reaction flux is determined by combining reactant property parameter and preset rate reaction rule, the consumption of hydrogen ion of unit area solid-liquid interface is quantified, the two reactions of dissolution and precipitation are distinguished by the positive and negative of net reaction flux, then the volume source term representing the hydrogen ion consumption intensity of unit grid volume is derived based on net reaction flux, then the volume source term is integrated into the preset distribution function evolution equation to obtain the simulation model, the hydrogen ion migration process and the mineral dissolution and precipitation process caused by hydrogen ion are integrated into the same simulation system to operate synchronously, eliminate the simulation deviation caused by only single simulation mineral dissolution in prior art, improve the accuracy of mineral dissolution and precipitation simulation.

The application discloses a method for regulating solidification structure of aluminum-silicon-iron alloy by gas-phase synergistic double-melt blending. CH4 gas is introduced into high-temperature aluminum-titanium alloy liquid, C-containing active particles are decomposed from the CH4 gas in the alloy melt and gas-liquid reaction occurs between the C-containing active particles and Al and Ti particles to generate intermediate phases such as Al4C3 and Ti3AlC and unstable TiC particles, and the intermediate phases react to generate thermodynamically stable TiC nanoparticles. Meanwhile, aluminum-silicon alloy melt and aluminum-iron alloy melt with significant difference in volume and temperature are blended in a controlled diffusion manner to obtain aluminum-silicon-iron melt. During the gas-liquid blending process, due to the opposite directions of solid / liquid interface advancing direction and solute diffusion direction during melt solidification, there exist non-local micro temperature and concentration fluctuations, and grain refinement is realized by controlling the solidification nucleation and diffusion growth process. The gas-liquid casting technology is a new process with multiple processes in synergistic action, and multiple processes can have a superposition effect under synergistic action, so that the synergistic refinement of aluminum-silicon-iron alloy second phase and aluminum grains is realized.

The application discloses a preparation method of a metal oxide passivation film on a gallium nitride surface; the method comprises the following steps: mixing a metal nitrate precursor solution and a hole sacrificial agent to obtain a mixed solution; placing a substrate containing a GaN layer into the mixed solution and performing photochemical deposition under ultraviolet light to obtain a metal oxide passivation film formed on the surface of the GaN layer. The preparation method uses a metal nitrate as a precursor, and under ultraviolet light, photo-generated electrons and holes of the GaN are used to initiate a redox reaction at a solid / liquid interface to form a uniform and dense metal oxide passivation film. The method is simple in process, is performed at room temperature, does not need vacuum, has small interface damage, can be used to reduce the trap state density of the GaN surface, improve the interface stability and reliability of a device, and is suitable for surface / interface passivation treatment of power electronic and ultraviolet photoelectric devices.

The present application relates to the technical fields of chemical engineering automation control, and discloses an intelligent closed-loop control system for producing p-dichlorobenzene by biomass method, which comprises a signal acquisition module, a residence time reconstruction module, a thermal coupling analysis module, a parameter self-adaptive scheduling module and an execution control module. The rheological characteristics of raw materials are monitored by acquiring the current of the stirring motor, the liquid level is dynamically increased by the residence time reconstruction module to prolong the residence time of materials, and the periodic migration strategy of the liquid level is introduced to prevent the gas-liquid interface from scaling. The thermal resistance lag factor is calculated by the thermal coupling analysis module and the parameter self-adaptive scheduling module, the temperature control parameters are corrected in real time, and the upper limit of the cooling output is limited to prevent the overcooling crystallization of the inner wall. The problems of the decrease of the conversion rate, the decrease of the heat transfer efficiency and the wall-hanging of the equipment caused by the viscosity fluctuation of the biomass raw materials are effectively solved, and the adaptive stable control of the reaction process is realized.