Method for detecting phenolic antibacterial agents in textiles through in-situ derivatization and dispersive liquid phase microextraction
A technology for dispersion liquid and textiles, applied in the field of product safety and detection, can solve the problems of inability to detect chlorophenol and o-phenylphenol at the same time, consumption of organic solvents, long detection process time, etc., and achieves low cost, environmental friendliness, Simple to use effects
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[0042] Example In situ derivatization-dispersive liquid phase microextraction-gas chromatography / mass spectrometry detection of phenolic antibacterial agents in textiles
[0043] 1 Materials and methods
[0044] 1.1. Instruments and reagents:
[0045] Gas chromatography-mass spectrometer (6890A / 5975C, Agilent, USA), DB-5MS capillary column (30m×0.25mm×0.25μm); BUCHI R-215 rotary evaporator, equipped with circulating cooling water system (Buehi, Switzerland); KQ5200DE Type ultrasonic cleaner (Kunshan Ultrasonic Co., Ltd.); MettlerAL204 analytical balance (Mettler-Toledo, Shanghai). 2,4,6-Trichlorophenol, 2,3,5,6-tetrachlorophenol, 2,3,4,5-tetrachlorophenol, 2,3,4,6-tetrachlorophenol, pentachlorophenol, O-phenylphenol (Dr. Ehrenstorfer, Germany); dichloromethane, chloroform, carbon tetrachloride, chlorobenzene, methanol, acetonitrile, acetone, isopropanol (all chromatographically pure); acetic anhydride, potassium carbonate ( All were analytically pure); water was high-purity...
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