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155 results about "Analytical balance" patented technology

An analytical balance (often called a "lab balance") is a class of balance designed to measure small mass in the sub-milligram range. The measuring pan of an analytical balance (0.1 mg or better) is inside a transparent enclosure with doors so that dust does not collect and so any air currents in the room do not affect the balance's operation. This enclosure is often called a draft shield. The use of a mechanically vented balance safety enclosure, which has uniquely designed acrylic airfoils, allows a smooth turbulence-free airflow that prevents balance fluctuation and the measure of mass down to 1 μg without fluctuations or loss of product. Also, the sample must be at room temperature to prevent natural convection from forming air currents inside the enclosure from causing an error in reading. Single pan mechanical substitution balance maintains consistent response throughout the useful capacity is achieved by maintaining a constant load on the balance beam, thus the fulcrum, by subtracting mass on the same side of the beam to which the sample is added.

Micro fixed-bed reactor capable of realizing online thermal-state weighing and method

ActiveCN106053280AIntuitive performance of reaction statusElimination of Influencing Factors of Mass Transfer DiffusionMaterial weighingTemperature controlThermal state
The invention discloses a micro fixed-bed reactor capable of realizing online thermal-state weighing and a method. The device comprises an analytical balance, a thermal-radiation-preventing water cooling plate, a weighing rod, a liftable electric furnace, a silk screen bed layer, a thermocouple, a gas circuit and temperature control system, a transparent container, a fixed bed provided with an air distribution plate and a support, wherein the thermal-radiation-preventing water cooling plate is fixedly connected with the top of the transparent container; the top end of the weighing rod is located in the fixed bed, and the bottom end of the weighing rod is located on a tray of the analytical balance; the silk screen bed layer is fixedly connected with the top end of the weighing rod; the liftable electric furnace is fixedly connected with the outer side of the fixed bed; the temperature measuring end of the thermocouple is located in an inner cavity of the fixed bed, and the connecting end of the thermocouple is connected with a temperature measuring port of the gas circuit and temperature control system through a lead; a mass flow meter outlet of the gas circuit and temperature control system is connected with a ventilating port of the air distribution plate. With the adoption of the micro fixed-bed reactor and the method, online thermal-state weighing can be performed on solid reaction substances located in the fixed bed.
Owner:SOUTHEAST UNIV

Magnetic material curie temperature measuring method based on thermogravimetry changes

The invention belongs to the technical field of the thermomagnetic measurement of magnetic materials, and relates to a magnetic material curie temperature measuring method based on thermogravimetry changes. Through measuring the changing relationship between balance apparent weight and temperature under the effect of a low field intensity applied magnetic field, the curie temperature of a magnetic substance is obtained. The suction effect of an electromagnet to the magnetic substance is related to magnetic field intensity and also relies on the gradient changes of the magnetic field intensity, therefore the obvious thermogravimetry changes can be obtained under a non-uniform field intensity applied magnetic field with relatively lower field intensity, and the changes can be easily measured by a high-precision analytical balance. According to the magnetic material curie temperature measuring method based on the thermogravimetry changes, the obvious thermogravimetry changes can be obtained by using the non-uniform field intensity applied magnetic field with the relatively lower field intensity, and then the curie temperature of the magnetic substance can be measured; the problem of coil heating caused by the fact that a high-intensity magnetic field needs to be loaded when materials with weaker magnetism are measured by using a magnetic-thermo curve method is avoided; the method is economical and convenient, and is easy to popularize.
Owner:DALIAN UNIV OF TECH

Analytical method for content of short fibers in pole plate lead paste of lead-acid battery

The invention discloses an analytical method for the content of short fibers in pole plate lead paste of a lead-acid battery. The method comprises the following steps: dissolving positive plate lead paste with a mixed solution of nitric acid and hydrogen peroxide, or dissolving lead paste, a green plate and negative plate lead paste with a nitric acid solution; sieving and separating short fibers, and carrying out drying to obtain the short fibers; measuring the content of the short fibers with an analytical balance and calculating the mass percent of the short fibers in lead paste; wherein, the mixed solution of nitric acid and hydrogen peroxide is obtained by adding 20 mL of hydrogen peroxide with a mass concentration of 30% into 1000 mL of nitric acid with a mass concentration of 12%, and the nitric acid solution is nitric acid with a mass concentration of 12%. The method provided in the invention analyzes the content of short fibers in lead paste so as to determination uniformity of short fibers in lead paste and the content of short fibers in lead paste in a cured and dried green plate and in formed and dried positive and negative plates so as to determination whether there is a loss, thereby enabling the content of short fibers to meet technical requirements, strength of lead paste to be achieved and vibration resistance, cyclic endurance and no shedding of lead paste ofbattery pole plates to be guaranteed.
Owner:JIANGSU LEOCH BATTERY

Method for determination of calcium sulfite and calcium carbonate content of flue gas desulfurization gypsum

InactiveCN104849173ADrive mass adoptionJudging the retarding effectWeighing by removing componentPortland cementAnalytical balance
The invention discloses a method for determination of calcium sulfite and calcium carbonate content of flue gas desulfurization gypsum and belongs to the method for determination of calcium sulfite and calcium carbonate content. The method comprises respectively dissolving flue gas desulfurization gypsum subjected to full oxidation treatment and unoxidized flue gas desulfurization gypsum by a diluted hydrochloric acid solution, determining mass losses of the flue gas desulfurization gypsum and the unoxidized flue gas desulfurization gypsum by an analytical balance in dissolution, calculating calcium carbonate content of the flue gas desulfurization gypsum according to the mass loss of the flue gas desulfurization gypsum subjected to full oxidation treatment, and calculating total content of calcium sulfite and calcium carbonate of the flue gas desulfurization gypsum according to the mass loss of the unoxidized flue gas desulfurization gypsum, wherein the difference of the calcium carbonate content and the total content of calcium sulfite and calcium carbonate is the total content of calcium sulfite of the flue gas desulfurization gypsum. Calcium sulfite of the flue gas desulfurization gypsum produces large influence on portland cement setting time and strength, and through determination of calcium sulfite and calcium carbonate content, flue gas desulfurization gypsum slow setting effects on portland cement can be determined. The method promotes large scale use of flue gas desulfurization gypsum as industrial waste residue. The method has the advantages of simple determination method, accurate result and low determination cost.
Owner:CHINA UNIV OF MINING & TECH +1

Method for detecting holdup of split phases in oil sludge based on induction heating technique and system

The invention discloses a method for detecting holdup of split phases in oil sludge based on an induction heating technique and a measuring system. The detection method is based on the formation mechanism and physical-chemical characteristics of the oil sludge, the induction heating technique is adopted, the oil sludge is pyrolyzed according to the set heating curve, and the oil gas and water steam produced by pyrolysis are condensed and collected, and are sent into a metering cylinder; the oil and water in the metering cylinder are naturally separated, the volume of water at the lower layer is read via the scales of the metering cylinder, and the mass of the water is obtained by combining with density; the total mass of oil and water is weighed by an analytical balance, the mass of the water is deducted, and the mass of the oil is obtained; the mass of the oil and the mass of the water are deducted from the mass of the oil sludge, so as to obtain the mass of residue, thereby calculating the holdup of split phases in the oil sludge; by adopting the detection method, the holdup of split phases in the oil sludge can be simultaneously detected, the stored and transported oil sludge can be quickly detected within about one hour, and the detection absolute errors of the three phases are respectively smaller than 2%. The measuring system mainly consists of an induction heating powersupply, an induction heater, a temperature detection module, a controller, a condensing device and a metering test tube.
Owner:ZHEJIANG UNIV

Capillary burette gravimetric titration method

The invention belongs to the chemical analysis field and relates to a general and rapid mini type weighing titrimetry analysis method; the invention is characterized in that a common dull polish titrimetry device is substituted by the simplest and most cheapest capillary drip tube (the quality of drop liquid is 0.005-0.02g); a mechanical analysis scale is substituted by an electronic scale; the volume of a titrant solution is substituted by the quality of the titrant solution, and the contents of measured ingredients is calculated; the invention simplifies the device, lowers cost, is easy for operation and is in favor of the rapid capitation of a liquid reagent; the method in the invention is more convenient and more swift than the common weighing titration method and the general volume titration method. The key points of the method in the invention are as follows: a measured liquid in certain quality (or certain volume) is provided in a taper bottle (or a small beaker); the quality of the capillary drip tube is known, and the capillary drip tube absorbing a standard solution is used to drip the measured liquid (a magnetic force blender can be used); the quality of the capillary drip tube is weighed again when the capillary drip tube dripps at the end of the scale; the difference between the qualities of the capillary drip tube weighed at the two times is the quality of the consumed standard solution, according to which the contents of the measured ingredients can be calculated out.
Owner:蔡成翔

Oil-water separator in oil shale dry distillation analysis and oil-water content determination method

The invention relates to an oil-water separator in oil shale dry distillation analysis and an oil-water content determination method. According to the invention, an oil absorption device, a water absorption device and a tail gas recovery device are connected to the end of a conduit of an aluminum retort or a Gray-King dry distillation device in order. The outside of the oil absorption device is provided with a constant temperature heating device, and the inside of the oil absorption device is loaded with an oil-absorbing material. The water absorption device contains a water-absorbing material inside. Compared with a toluene method for distillation separation of shale oil and water, the method provided in the invention greatly shortens the experimental time, avoids using toluene and other dangerous reagents, improves work efficiency, saves a lot of electric power and water energy, and has no damage to the ecological environment. Compared with a conical flask condensation method, the method provided in the invention has the characteristics of simple and convenient operation, and sufficient absorption of shale oil and water. The method uses an analytical balance to directly weigh the weight gains of the oil absorption device and the water absorption device, the weighing precision is high, and the precision and accuracy of the determined oil content and moisture content are both superior to traditional methods. The separator has the advantages of simple structure, low cost, convenient operation, simplicity and practicability.
Owner:JILIN UNIV

Method and apparatus for determining apparent density of pervasive solid substance

ActiveCN104964895ASolve SolubleSolve easy infiltrationSpecific gravity measurementApparent densityThermodynamics
The invention relates to a method and apparatus for determining apparent density of a pervasive solid substance. A specific gravity bottle or Webster balance can be used for determining the density of insoluble solid, the density of soluble solid can be determined by utilizing a gas specific gravity method, but the requirement for the instrument manufacturing precision is high, and the economic performance and convenience are poor. The method is characterized in that solid fluid is adopted as a volume replacement medium; the volume of a to-be-detected substance is determined by utilizing a special volume determination apparatus; the mass of the to-be-detected substance is determined by utilizing an analytic balance; the determination of the apparent density is realized by virtue of calculation of a special formula. The apparatus consists of a lower bottle body, a middle bottle body, an upper bottle body, a measuring range tube and charged solid fluid. The apparatus is simple in structure, practical and economical; the solid fluid can be reutilized and is environment-friendly; the solid fluid is charged in one step, the to-be-detected substance is separated from the solid fluid by utilizing a fixed screen in the process for inverting the apparatus, and the operation is very convenient; the apparatus is suitable for determining the apparent density of all solid substances, and the difficulty for determining the apparent density of soluble or wettable solid substances with irregular shape can be solved.
Owner:SHAANXI UNIV OF SCI & TECH

Permanent magnet temperature coefficient open-circuit measuring device and method

The invention relates to a permanent magnet temperature coefficient open-circuit measuring device and method. The permanent magnet temperature coefficient open-circuit measuring device comprises a balance support. The balance support is a box. A rack is placed at the bottom inside the balance support. A uniform gradient field generating device is placed on the rack and connected with a constant current power source. A high temperature furnace is placed on the uniform gradient field generating device or penetrates through the uniform gradient field generating device to be placed on the rack. The high temperature furnace is connected with a temperature control unit. An analytical balance is placed at the top of the balance support and connected with a computer. The computer is further connected with the temperature control unit. A sample suspension line is fixed to the lower end of the analytical balance. The sample suspension line penetrates through the top face of the balance support to extend into the high temperature furnace. The tail end of the sample suspension line is connected with a sample sleeve. A sample to be measured is placed inside the sample sleeve. According to the permanent magnet temperature coefficient open-circuit measuring device and method, the problem that at present, the accuracy and resolution ratio of permanent magnet temperature coefficient measurement are low is effectively solved, and the method and means are provided for measurement of critical materials in the aerospace field.
Owner:NAT INST OF METROLOGY CHINA

Half-mold blowing lift-augmentation wind tunnel test method and test device for transporter

The invention discloses a transport plane half-mold blowing high lift wind tunnel test method and a test device. The test method comprises the following steps: step a, calibrating the influence of high-pressure air on balance load after passing through an air bridge; b, installing a test device and a test model, and adjusting the attitude angle of the test model to a zero point; c, calibrating a momentum coefficient; d, adjusting the attitude angle of the test model to a zero point, and collecting an initial reading; e, adjusting the wind speed to a test wind speed, and adjusting the blowing capacity coefficient to a test state; f, adjusting the attitude angle of the test model, and recording a balance signal, an attitude angle signal, a pressure sensor signal and a temperature sensor signal; step g, processing balance data; and step h, analyzing balance data. By the adoption of the half-mold blowing lift-augmentation wind tunnel test method and device for the transport plane, the precision of blowing parameter control and aerodynamic force measurement is improved; and reliable wind tunnel test data is provided for the evaluation of the air blowing lift augmentation aerodynamic performance of transportation aircrafts.
Owner:LOW SPEED AERODYNAMIC INST OF CHINESE AERODYNAMIC RES & DEV CENT

Laser photoelectric analytical balance

The invention provides a laser photoelectric analytical balance, which is characterized in that two quartz glass trips with silver mirrors coated on the surfaces are parallel up and down; one laser transmitter transmits laser beams to the lower surface of the upper glass strip of a deformation element at a fixed inclination angle and the laser beams are reflected multiple times between the two mirror surfaces of the upper and lower glass strips; a light spot position sensor is arranged at the falling point of the laser beams after multiple times of reflection and is connected in an electrical bridge as a variable resistor; the two output ends of the electrical bridge are connected at the input interface of a measuring and amplifying circuit in a current electrical balance. When the pressure on the upper glass strip changes, deformation change leads to corresponding change of the angles of the reflected laser beams, after multiple times of reflection, accumulation and reinforcement, the light spot position sensor outputs corresponding resistance and the resistance is processed by the measuring and amplifying circuit, thereby realizing weighing. The analytical balance has the advantages of good linearity, high sensitivity and electromagnetic interference resistance.
Owner:卢能晓
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