The invention relates to a fire assaying measurement method, in particular to a method for measuring
gold content in a K gold ornament based on a fire assaying method, which comprises the following steps: step 1, weighing materials, and preparing a sample and a standard sample; 2, a fluxing agent and a catalyst are prepared, and the catalyst is used for increasing the
reaction rate and reducing gold and silver residues in
slag; 3, a fluxing agent, a catalyst and a cupel are pretreated, the inner surface of the cupel is thinly coated with the catalyst, the cupel is preheated, 10-15 wt% of
borax is calcined at the same time, and the
borax is dehydrated for use; step 4, filling a cupel; 5,
soot blowing is conducted, specifically, the cupel filled with the lead buckles is placed in a
soot blowing furnace, after the lead buckles are melted, a furnace door is slightly opened, the temperature is kept at 950 DEG C for 10-15 minutes, and after the furnace door is closed, the temperature is kept for 3-5 minutes; 6, separating gold; and step 7, calculating the content of K gold, and by thinly
coating a catalyst in the cupel, in the
soot blowing process, the
silicone oil is boiled and decomposed and continuously penetrates through the melt from the surface of the cupel, so that the elemental gold and
silver particles are far away from the
slag.