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395 results about "Gold leaching" patented technology

Method for recycling and synchronous harmless treatment of gold, silver and iron in roasting-cyanidation tailings

The invention provides a method for recycling and synchronous harmless treatment of gold, silver and iron in roasting-cyanidation tailings, and belongs to the technical field of metallurgical waste residue utilization. The method comprises the following steps: mixing dried roasting-cyanidation tailings with a fluxing agent and a reducing agent; carrying out roasting at 750 to 900 DEG C for 3 to 5 hours; conducting water quenching on hot roasted sand for cooling; carrying out ore grinding and flotation to remove residual carbon; leaching gold and silver with an environment-friendly gold leaching agent; and conducting magnetic separation on the leaching residue to obtain fine iron powder. Containing no highly toxic cyanide, the rejects belong to general industry solid waste. As the fluxing agent is added for magnetic roasting, not only can gold and silver coated with an iron mineral be exposed, but also the fluxing agent can perform a solid-phase reaction with a silicate mineral to generate a dissoluble silicate, and gold and silver coated with the dissoluble silicate can also be exposed after ore grinding. According to the method, gold, silver and iron in the roasting-cyanidation tailings are recycled, harmless treatment is realized synchronously, and the purpose of clean production is realized.
Owner:UNIV OF SCI & TECH BEIJING

Method for extracting gold from waste printed circuit board

The invention provides a method for leaching gold from a deserted printed circuit board. The method comprises the specified steps: Step 1: the deserted printed circuit board is crushed and smashed to separate metals and plastics; Step 2: the metals obtained from the Step 1 are mixed with nitric acid solution, stirring and reaction are carried out for 1h to 6h at the constant temperature of 10 DEG C to 80 DEG C, products are filtered, copper is leached from the filtrate, and the filter residue is washed and dried; Step 3: the filter residue obtained from the Step 2 is added into the blended solution of first iodine solution and a pro-oxidant, a reaction pH value is controlled at 3 to 9 by an inorganic acid and alkaline solution, reaction is carried out for 2h to 5h in a constant temperature oscillator at the temperature of 10 DEG C to 60 DEG C; and Step 4: products obtained from the Step 3 are filtered, with the filtrate fed into the cathode region of an electrobath, second iodine solution composed of iodine, water-soluble iodide and water is used as the electrolyte and fed into the anode region of the electrobath, electrolysis is carried out, the solution at the cathode region is filtered, then the filter residue obtained is gold mud, and the second iodine solution at the anode region is recovered. The method has high gold leaching ratio, low cost and less environmental pollution.
Owner:DONGHUA UNIV

Method for pretreating refractory gold ore by employing microwave calcining

The invention relates to a method to pre-treat a hard-to-leach gold ores-pyrite by microwave roasting, which is characterized in that the gold ores-pyrite or fine gold ores-pyrite with the granularity being 200 meshes which takes 90% to 95% of the whole gold ores-pyrite is positioned in a reaction chamber of a microwave roasting oven, a nitrogen is filled fully into the reaction chamber, starting the microwave roasting oven, the gold ores-pyrite or fine gold ores-pyrite is radiated and roasted by the microwave in the nitrogen atmosphere, the roasting temperature is 450 to 580 degree centigrade, the power is 4 to 6kw, the microwave roasting oven stops working after roasting for 5 to 20 minutes, a roasted product is made when the roasting gold ore-pyrite is taken out. The method to pre-treat a hard-to-leach gold ores-pyrite by microwave roasting has the advantages of increasing the gold leaching yield of the hard-to-leach gold ores-pyrite up to over 90%, reaching purpose of the environment protection because the sulfur is precipitated as a free sulfur without the recovery process of smoke and dust, and saving the energy because the microwave roasting process is adopted and the pretreatment time is greatly shortened.
Owner:SHENYANG LIGONG UNIV

Beneficiation method for high-carbon micro-fine particle sub-microscopic gold ore

The invention discloses a beneficiation method for high-carbon micro-fine particle sub-microscopic gold ore, and belongs to the technical field of mineral processing. Roasted ore, namely, concentrated gold ore, is obtained by performing flotation after gold ore is ground, grinding and selecting the floated concentrated gold ore again, and performing oxidizing roasting on the floated concentrated gold ore. The content of carbon and sulphur in the floated concentrated gold ore is high; and when iron pyrite in the floated concentrated gold ore is enriched to a certain degree, the gold grade is difficult to improve. The concentrated gold core with high quality can only be obtained through the oxidizing roasting. Two-section oxidizing roasting is performed on floated tailings so as to prevent over-roasting or under-roasting, and a sulphide which coats the gold is damaged through roasting so that cracks appear on a gold-loaded mineral structure to inhibit negative impact of organic carbon on subsequent cyaniding gold extracting process; and therefore, the purpose of remarkably improving the leading rate of gold is achieved. The method has the characteristics of low production cost, high gold recovery rate, high adaptability, wide application range and the like; and recycling and utilization of the ore are realized.
Owner:NORTHWEST RES INST OF MINING & METALLURGY INST

Comprehensive recovery method of gold ore resource containing molybdenum multi-metal

The invention discloses a method for comprehensively recovering molybdenum-containing polymetallic gold ore resources, which comprises the following steps: firstly, crushing and grinding molybdenum-containing gold ores first, performing floatation on useful metallic elements to obtain bulk concentrate by a complete mixing floatation method, and discarding tailings; secondly, leaching out and recovering gold and silver from the bulk concentrate by CCL carbon paste wet-method gold leaching technology, and using tailings after gold leaching for preferred selection of molybdenum in the next step; thirdly, performing preferred separation and floatation of the molybdenum on the gold leaching tailings to obtain qualified molybdenum concentrate; fourthly, activating molybdenum-selecting tailings, and performing separation and floatation of lead to obtain lead concentrate; fifthly, performing separation and floatation of copper on lead-selecting tailings to obtain copper concentrate; and sixthly, performing floatation of sulfur on copper-selecting tailings to obtain sulfur concentrate, performing filtration and backwater circulation on sulfur-selecting tailings, and applying the sulfur-selecting tailings to the carbon paste wet-method gold leaching technology for recovery of the gold and the silver. The method greatly improves the grade of separated metals. The following products can be obtained by utilization of the method: more than or equal to 95 percent of alloyed gold, more than or equal to 45 percent of the molybdenum concentrate, more than or equal to 40 percent of the lead concentrate and more than or equal to 35 percent of the sulfur concentrate. The tailings after floatation are filtered by a ceramic filter (the moisture content is less than or equal to 15 percent), subjected to dry-type stacking, and used for soil sealing and land rehabilitation in late stage.
Owner:LINGBAO CITY JINYUAN MINING

Gold extracting method by thiosulfate using polyamine compoud as additive

The invention relates to a gold extracting method by thiosulfate using a polyamine compound as an additive, which comprises the steps: after ores are crushed and wet-ground until the fineness is over 90 percent of -200 meshes, 0.03-3mol/dm3 thiosulfate is added to be used as a leaching agent, and then 0.0015-0.09mol/dm3 polyamine compound and 0.0015-0.03mol/dm3 copper (II) ion are added to form a complex ion to be used as an additive to be stirred and leached; and after gold ores are leached, gold from a leaching solution is recovered. The leaching solution is used to extract gold from the ores, so that the gold leaching rate is high, the process operation is simple, the control is easy, the consumption of thiosulfate is extremely low, and the compositions of the gold leaching solution are simple and are favorable for the recovery of the gold; and the application range is wide, the leaching effect is good when the pH value is between 10 and 12, the leaching speed is quick for copper-containing, carbon-containing and other refractory gold ores, quite high gold leaching rate can be maintained, and sodium cyanide and other toxic substances are not used and toxic waste is not discharged in the whole gold extraction process, so the environment is protected.
Owner:KUNMING UNIV OF SCI & TECH

Method for strengthening gold extraction of iron gold concentrate roasted product containing sulphur and arsenic

The invention discloses a method for strengthening gold extraction of an iron gold concentrate roasted product containing sulphur and arsenic. The high-iron gold concentrate containing sulphur and arsenic, especially high sulphur and high arsenic, hinders the subsequent chemical gold leaching process after being subjected to oxidation roasting pretreatment because of the problem that iron oxide is inevitably generated to wrap gold in a high-temperature reaction process. The invention proposes a new method for strengthening gold extraction of the iron gold concentrate roasted product containing sulphur and arsenic by a flow of 'metallized reduction roasting-acid leaching-gold leaching', namely a method for strengthening gold extraction of the iron gold concentrate roasted product containing sulphur and arsenic aiming at the problem. The method comprises the steps of firstly, carrying out metallized reduction roasting on the iron gold concentrate roasted product containing sulphur and arsenic with a reducing agent, carrying out acid leaching on the metalized roasted product, and finally carrying out chemical leaching with an acid slag. By adopting the method disclosed by the invention, the leaching rate of the iron gold concentrate roasted product containing sulphur and arsenic is higher than 95%; and important theory and technical guidance are provided for effective gold extraction of the gold roasted product.
Owner:CENT SOUTH UNIV

Method for recycling gold from refractory gold concentrate

The invention relates to a method for recovering gold from unmanageable gold concentrate, which comprises the steps in the following process order: a. stirring and leaching: sodium cyanide solution is added into the gold concentrate to be stirred and leached; the liquid-solid ratio of the ore pulp is 1 to 4:1, the concentration of the sodium cyanide is 0.5 millesimal to 4 millesimal of the weight of the ore pulp, the leaching time is 12h to 36h, and pregnant solution 1 and leaching slag 1 are filtered; b. leaching while milling: the leaching slag 1 after stirring and leaching is put into a milling and leaching machine to be leached and milled; the liquid-solid ratio of the ore pulp is 1 to 4:1, the concentration of the sodium cyanide is 0.5 millesimal to 4 millesimal of the weight of the ore pulp, the milling and leaching time is 1h to 6h, and pregnant solution 2 and waste slag are filtered; c. recovery: the pregnant solution 1 and the pregnant solution 2 are recovered, to obtain sponge gold. The method is characterized by high gold leaching rate, low-grade gold in cyanidation tailing, short technological process, short treatment and recovery time, low sodium cyanide consumption, low requirement for the corrosion resistance of the equipment and the like, and is in particular applicable in the recovery and application of the gold in gold concentrate with complicated package.
Owner:ZIJIN MINING GROUP

Gold extraction method employing gold cyanided tailing roasting-ultrasonic intensification thiourea gold leaching-activated carbon enrichment

The invention relates to a gold extraction method employing gold cyanided tailing roasting, ultrasonic intensification thiourea gold leaching and activated carbon enrichment, and belongs to the field of wet method metallurgy. According to the gold extraction method, gold-containing cyanided tailing is subjected to roasting treatment, then thiourea is used for leaching gold, meanwhile the ultrasonic intensification treatment is carried out, solid-liquid separation is performed after the gold leaching, gold contained in the liquid phase is gathered by the activated carbon through enrichment, solid-liquid separation is performed after the enrichment, the activated carbon is used for extracting and resolving gold, after resolving, the activated carbon is activated to be recycled repeatedly, a large quantity of thiourea exits in the tail liquid, and the thiourea can be circularly used for the leaching process after being simply treated. The gold extraction method is used for extracting gold in the cyanided tailing through leaching, the leaching speed is high, the extraction rate can be more than 90%, the cycle is short, and the activated carbon and the tail liquid can be recycled, so the production cost is greatly reduced, the economical benefit on the utilization of gold cyanided tailing is improved, and meanwhile, the environmental protection is facilitated.
Owner:INNER MONGOLIA UNIV OF SCI & TECH

Method for extracting gold from thiosulfate adopting ethanediamine as additive

The invention relates to a method for extracting gold from thiosulfate adopting ethanediamine as an additive. The method comprises the following steps that: the ethanediamineas is adopted as ligand and forms ethanediamine copper (II) complex ion with copper (II) ion, the formed ethanediamine copper (II) complex ion is used as the additive, and the thiosulfate is used as a leaching agent and is used for extracting the gold from ore pulp; and calculated by water amount, the adding amount of the thiosulfate is 0.03-3mol/dm<3>, the adding amount of the ethanediamine is 0.0015-0.09mol/dm<3>, and the adding amount of copper (II) ion is 0.0015-0.03mol/dm<3>. The leachate is used for extracting the gold from the ore, the leaching rate of the gold is high, the technique operation is simple, the control is easy, the consumption amount of the thiosulfate is extremely low, and the ingredients of the gold leachate are simple and are beneficial to recovery of the gold therein. The method has wide application range, has good leaching effect when the pH is between 10 and 12, also has fast leaching speed of gold ores which contain copper, carbon and the like and are difficult to treat, can maintain quite high gold leaching rate, and the whole gold extracting process does not use toxic substances of sodium cyanide and the like, also does not discharge toxic waste, and is environment-friendly.
Owner:KUNMING UNIV OF SCI & TECH

Method for preparing pure gold from silver anode mud through potential control

ActiveCN107460324AHigh purityGold powder with a purity of 99.99%, high direct recovery rate of goldProcess efficiency improvementSulfite saltSlurry
Provided is a method for preparing pure gold from silver anode mud through potential control. The silver anode mud is leached out in a nitric acid solution, after nitric acid leaching residue is immersed and digested in concentrated sulfuric acid, coarse gold powder is obtained, hydrogen peroxide is added into a hydrochloric acid solution containing the coarse gold powder to conduct potential controlling and gold leaching by chlorination, slurry is subjected to solid-liquid separation after being cooled, gold leaching liquid is added into sodium hydroxide and sodium sulfite to conduct potential controlling and reduction, and reduction gold powder is obtained, and after the reduction gold powder is subjected to concentrated sulfuric acid refining, pure gold powder is obtained. According to the method for preparing the pure gold from the silver anode mud through potential control, a potential control mode is adopted to achieve adjustment and controllability of the process for preparing the pure gold from the silver anode mud, the gold powder with the purity being 99.99% is prepared, the direct recovery rate of gold reaches to over 99.9%, the method has the advantages of being high in gold direct recovery rate, stable in technological process and high in product purity, and the environmental pollution problem existing in a traditional aqua regia dissolution method is solved.
Owner:CENT SOUTH UNIV
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