10234results about How to "High extraction rate" patented technology

The invention disclosed relates to a method for the extraction of sweet glycosides from the Stevia rebaudiana Bertoni plant and recovery of individual rebaudioside A and stevioside. The extraction is developed in the presence of pectinase, and the extract is purified using cyclodextrin and bentonite. High purity rebaudioside A is obtained by crystallization and recrystallization from ethanol. High purity stevioside is prepared from the filtrate by purification with cyclodextrin, bentonit, and ion exchange resins. The enzymatic modification of the rebaudioside A, stevioside and the purified extract is carried out using the transferring enzymes derived from Thermoactinomyces vilgaris and Bacillus halophilus.

A solid state water soluble formulation in granular or tablet form is provided. The formulation is a natural products formulation containing a green tea plant extract in combination with other ingredients which create an effervescent liquid composition upon dispensing the formulation in a liquid. The liquid form of administration, as well as the effervescent properties of the dissolved formulation increase bioavailability of the advantageous components of the green tea plants such as Polyphenols, by increasing absorption speed and amount in the human body. The formulation may include additional components such as, other plant extracts, vitamins, ionic minerals, and other substances purported to be of a health benefit.

Thermal insulation is provided for use in applications requiring continuous resistance to temperatures of 1260° C. without reaction with alumino-silicate firebricks, the insulation comprises fibers having a composition in wt %65%<SiO2<86%MgO<10%14%<CaO<28%Al2O3<2%ZrO2<3%B2O3<5%P2O5<5%72%<SiO2+ZrO2+B2O3+5*P2O5 95%<SiO2+CaO+MgO+Al2O3+ZrO2+B2O3+P2O5 Addition of elements selected from the group Sc, La, Ce, Pr, Nd, Sm, Eu, Gd, Tb, Dy, Ho, Er, Tm, Yb, Lu, Y or mixtures thereof improves fiber quality and the strength of blankets made from the fibers.

The invention discloses a preparation method of a raw dendrobium officinale pulp beverage. The preparation method comprises the following steps of: (1), baking a fresh dendrobium officinale branch to be purple, adding water to the baked fresh dendrobium officinale branch for pulping, so as to obtain a primary serous fluid; (2), carrying out insulation treatment on the primary serous fluid, boiling and filtering the primary serous fluid, so as to obtain filter residue; (3) adding water to the filter residue for pulping, boiling and filtering the filter residue again to obtain the filter residue, repeating the sub-steps for a plurality of times, adding water to the final filter residue for the pulping, so as to obtain secondary serous fluid; (4), adding a cellulolytic enzyme into the secondary serous fluid for carrying out enzymolysis, so as to obtain an enzymolysis solution; (5) boiling and filtering the enzymolysis solution, to obtain the filter residue; (6) adding water into the filter residue for the pulping, boiling and filtering the filter residue again, to obtain the filter residue, and repeating the sub-steps for a plurality of times; (7) mixing all the filter solutions, boiling and sterilizing the mixed filter solution, so as to obtain the raw dendrobium officinale pulp beverage. The preparation method provided by the invention has the advantages that dendrobium officinale is baked, the filter residue is subjected to enzymolysis treatment, the extraction rate of functionality polyose and flavone is improved, the content of dietary fiber in the beverage is increased, and the prepared beverage color is bright and stable.

The invention disclosed relates to a method for the extraction of sweet glycosides from the Stevia rebaudiana Bertoni plant and recovery of individual rebaudioside A and stevioside. The extraction is developed in the presence of pectinase, and the extract is purified using cyclodextrin and bentonite. High purity rebaudioside A is obtained by crystallization and recrystallization from ethanol. High purity stevioside is prepared from the filtrate by purification with cyclodextrin, bentonit, and ion exchange resins. The enzymatic modification of the rebaudioside A, stevioside and the purified extract is carried out using the transferring enzymes derived from Thermoactinomyces vulgaris and Bacillus halophilus.

A method for extracting silicon dioxide, alumina and gallium oxide from high-alumina fly ash relates to the technology fields of environmental mineralogy and material, chemical industry and metallurgy. The method comprises the main steps as follows: causing the high-alumina fly ash to react with sodium hydroxide solution; filtering the solution; introducing CO2 to the filtrate for full gelation; cleaning, purifying, drying, grinding and calcining the silica gel after gel filtration to obtain finished white carbon black; adding limestone and a sodium carbonate solution into the filter mass after the reaction and filtration of the high-alumina fly ash and the sodium hydroxide solution; ball grinding the mixture into raw slurry; dissolving out the clinker obtained by baking the raw slurry; subjecting the filtrate to deep desiliconization to obtain sodium aluminate extraction liquid; filtrating the sodium aluminate extraction liquid after subjecting the sodium aluminate extraction liquid to carbon dioxide decomposition; baking the aluminum hydroxide after washing the filter mass to form the aluminum hydroxide product; and extracting the gallium oxide from the carbon dioxide decomposition mother solution and desiliconized solution. The method has the advantages of low material price, simple operating procedures, low investment, low production cost, low energy consumption and less slag.

The invention provides a subcritical liquid extraction device and a subcritical liquid extraction method of active ingredients of natural products, relating to a device and a method for extracting active ingredients of natural products. The device comprises a control system part and a leaching system part, wherein the leaching system part comprises an extraction tank 1, an evaporating tank 2, a buffer tank 3, a condenser 4, a solvent tank 5, an ultrasound generating device 11, a vacuum pump 9, a fire arrester 10, a compressor 8, a hot water pump 7 and a hot water box 6; the control system partcomprises a leaching temperature controller, a leaching time controller, a leaching frequency controller, a material dissolving ratio controller, an exsolution temperature regulation controller, an exsolution pressure feedback controller, an electric appliance controller of the device and an excess-temperature excess-pressure leaking alarm. The method can select different subcritical extraction media according to different extraction products, combines a subcritical liquid extraction technology and an ultrasonic extraction technology to increase extraction rate and reduce extraction time andis a new high-efficiency low-consumption environment-friendly technology for extracting active ingredients of natural products.

Disclosed is a process for reclamation of waste fluids. A conditioning container is employed for receipt of waste material on a continuous flow for treatment within the container by immersible transducers producing ultrasonic acoustic waves in combination with a high level of injected ozone. The treated material exhibits superior separation properties for delivery into a centrifuge for enhanced solid waste removal. The invention discloses a cost efficient and environmentally friendly process and apparatus for cleaning and recycling of flowback, or frac water, which has been used to stimulate gas production from shale formations. The apparatus is mobile and containerized and suitable for installation at the well site.

The invention discloses a method for preparing metallurgy-level aluminum oxide by using fluidized bed pulverized fuel ash as a raw material. The method comprises the following steps of: a) grinding the pulverized fuel ash, and removing iron by a wet magnetic separation method; b) reacting the pulverized fuel ash subjected to magnetic separation with hydrochloric acid to obtain hydrochloric acid immersion liquid; c) allowing the hydrochloric acid immersion liquid to pass through a large pore type cation resin column for further iron removal to obtain refined aluminum chloride solution; d) concentrating the refined aluminum chloride solution, and crystallizing to obtain an aluminum chloride crystal; and e) calcining the aluminum chloride crystal and decomposing to obtain the metallurgy-level aluminum oxide. The method has a simple process and an easily-controlled production process, and is high in aluminum oxide extraction efficiency, low in production cost and stable in product quality.

Provided is a method for joint-mining of coalbed gas and coal. The method comprises: a well-drilling step; a fracturing and penetration step; a coalbed gas extraction step: an ignition step, and an underground gasification step. The method combines an underground coal gasification technology and a coalbed gas extraction technology, not only allows for utilization of the high temperature of underground gasification to heat a coalbed. thus increasing the permeability of a coal seam. and increasing the recovery rate of the coalbed gas, but also allows for utilization of the coalbed gas to perform the drilling and the fracturing and penetration processes, thus increasing the efficiency of underground coal gasification for mining.

An intra-luminal device for the extraction of occlusive or partially occlusive material is disclosed. Said device comprises a novel catheter extension which minimizes cavitation of extracted fluids and also allows the better navigation of tortuous lumens or vasculature.

A process for leaching laterite ores containing limonite and saprolite. Sufficient mineral acid is added to a slurry of limonite which is leached at atmospheric pressure to dissolve most of the soluble non-ferrous metals and soluble iron. After adding saprolite the slurry is further leached at a temperature above the normal boiling point and at a pressure above atmospheric pressure for a time sufficient to leach most of the contained nickel in the saprolite and to precipitate most of the iron in solution. The pressure of the slurry is then reduced, and nickel and / or cobalt is subsequently recovered from the leach solution by solvent extraction, resin-in-pulp or other ion exchange, sulfide or hydroxide precipitation, or other recovery method.

The invention relates to the field of coal chemical industry, and more specifically relates to a method of extracting phenolic compounds from coal liquefied oil or coal tar. The method comprises the following steps: 1) distilling coal liquefied oil or coal tar and cutting to obtain fractions at a temperature of 260 DEG C; 2) mixing an extractant with the obtained fractions and layering the extractant; 3) separating and collecting the extractant layer which contains phenolic compounds; 4) carrying out multistage back extraction on the phenolic compounds so as to obtain a stripping agent-phenol solution and an extractant; 5) separating the stripping agent-phenol solution by rectification, recovering the stripping agent for cyclic utilization, and carrying out separation to obtain crude phenols; 6) removing entrained neutral oil in phenolic compounds by water vapour so as to obtain crude phenol products. The method of extracting phenolic compounds from coal liquefied oil or coal tar provided in the invention avoids the usage of soda acid, exerts no influence on subsequent treating processes, and guarantees high recovery rate and purity of phenols.

The invention relates to a method for extracting blueberry anthocyanin, which comprises the following steps of: (1) pretreating a raw material; (2) extracting the blueberry anthocyanin, namely adding extracting solution in a volume ratio of the raw material to liquid for leaching to obtain leach liquor, centrifugally collecting and merging clarified supernate which is leached and centrifuged twice, and centrifuging and concentrating under reduced pressure to obtain crude extract of the blueberry anthocyanin; and (3) refining the blueberry anthocyanin, namely adsorbing and eluting the crude extract of the blueberry anthocyanin through macroporous resin, concentrating eluent under reduced pressure, and performing freeze drying or spray drying on concentrated solution of the blueberry anthocyanin to obtain a finished product of the blueberry anthocyanin. The method solves the problems of strong harvesting seasonality and difficult storage of blueberry fruits and huge economic loss due torot caused by the unsalable blueberry fruits, has the advantages of simple process, controlled operation, low cost and no pollution, and is particularly suitable for extracting the blueberry anthocyanin on a large scale.

The invention relates iron melt improving vanadium content and controlling calcium content cooling agent and the technology, specially relates the cooling agent of adjusting the proportion of cooling agent to stabilize calcium content in vanadium slag and the technology. The technology comprises the 56-60wt% iron scale, 30-40wt% iron concentrate powder containing vanadium, and 5-10wt% anchoring agent. The method stabilizes the calcium content and iron content in vanadium slag, and effectively solves the problems of great fluctuation of vanadium slag composition and superstandard calcium and iron. By controlling the thermoregulation material to meet the requirements of the improving vanadium temperature and calcium oxide content, the method improves the vanadium slag grade and extraction rate. The invention possesses the following characteristics: 1 shortening the converting time; 2 improving the vanadium slag grade and extraction rate, and stabilizing the calcium oxide content; 3 reducing the iron loss.

The invention discloses a method for extracting peony seed oil. In the method, peony seed powders are put in a supercritical CO2 extractor for supercritical extraction, and oil is collected to obtain the provided peony seed oil. In the method, the supercritical extraction temperature ranges from 30 to 50 DEG C, 45 DEG C is optimized, the pressure for supercritical extraction ranges from 20 to 35MPa, and 30MPa is optimized; time for supercritical extraction ranges from 0.5 to 2 hours, and 1 hour is optimized. The grain diameter of the peony seed powders ranges from 20 to 60 screen meshes. The provided supercritical CO2 extracting method for preparing peony seed oil needs no organic reagents, has simple and convenient extracting and separating method, the extraction yield can reach 27 percent, and obtained unsaturated fatty acid can reach 90 percent; and compared with the prior organic solvent extraction method, the contents of linolenic acid and linoleic acid in peony oil are increased to certain extent, and the extraction is completer.

The invention discloses a method for non-saponification extraction and separation of light rare earth elements. After a compound extraction agent consisting of acid phosphorus type extraction agent, alkaline amine type extraction agent and solvent oil is mixed with phosphate solvent or organic alcohol solvent at 30-70 DEG C, chlorinated light rare earth liquid is extracted and separated; and the water washing and the hydrochloric acid reverse extraction are performed to finally realize the separation of La, Ce, Pr and Nd; and a mixed organic phase after the reverse extraction is returned to an extraction tank for recycling. The method pretreats the mixed organic phase consisting of the compound extraction agent and the solvent, so that such defects as high viscosity, weak mobility, easy emulsification and long phase splitting time are overcome; the method has no need to saponify the acid phosphorus type extraction agent, so that no alkali liquor consumption and no waste water emission in the extraction process are realized, but the separation capacity of a saponification extracting agent system is achieved, and the extraction grade is reduced compared with that needed by the saponification extracting agent system; and the method is a rare earth element separation process with economy and high efficiency.

The invention provides effective technology for extracting active ingredients of Entermorpha and a method for preparing an Entermorpha alga fertilizer. The method is characterized by comprising: taking the Entermorpha as a raw material, effectively extracting the active ingredients of the Entermorpha through technical processes such as pretreatment of raw materials, leaching, neutralization, concentration and combination, taking an extracting solution as a base fluid, combining the extracting solution with at least one composition of humic acid, urea, potassium dihydrogen phosphate, potassiumsulfate, monoammonium phosphate and microelement, and preparing the high-activity Entermorpha alga fertilizer. The Entermorpha alga fertilizer is rich in active substances of algae, not only can strengthen photosynthesis of crops, increase the yield of the crops and improve the product quality but also can strengthen the cold resistance, the drought resistance, the stress resistance and the disease resistance of the crops, promote earliness of the crops and increase the fertile flower percentage and the fertile fruit percentage, has lower production cost, good solubility and safe use, is friendly and harmless to human beings, domestic animals and the natural environment, and is a novel environment-friendly fertilizer suitable for modern agriculture.

The laminarin preparing process includes the technological steps of material treatment, crushing, defatting and decolorizing with alcohol, ultrasonic wall breaking, enzyme treatment and vacuum extracting and vacuum freeze drying. During the material treatment, the kelp material including kelp, waste kelp material and leftover from kelp processing is washed first with water and then with citric acid or acetic acid. During the enzyme treatment, the kelp material is enzymolyzed with cellulose and pectase. The present invention has kelp including kelp waste and leftover best utilized to extract laminarin of high purity in high yield, and the prepared laminarin may be served directly or used in developing other functional foods.

The present invention relates to a manufacturing method of refining rice bran top oil, which can effectively refining top oil from the rice bran and satisfy the people requirement to the health dieting. The invention includes the following steps: (1) crude oil filtering; (2) phosphoric acid degumming and light alkali alkali refining; (3) washing, drying; (4) dewaxing; (5) a primary decolorizing; (6) physical deacidification; (7) secondary alkali refining; (8) iron removing; (9) washing; (10) drying; (11) secondary decolorizing; (12) deodorization; (13) degreasing. The invention adopts a mode of combining the physical refining and chemical refining to realize a large-scale production of the rice bran top oil, provides a favorable technique to the rice bran deep-processing, improves the extraction rate from traditionally 55-60% to 75-80%, saves materials and reduces environmental pollution, has huge economic and social benefits. The invention is a major innovation to the edible rice bran oil production.

The invention provides an extraction method and a device used for extracting ultrasonic reinforced sub-critical water of effective component of a natural outcome. The method is mainly characterized in that a pre-disposed raw material is arranged in an extraction kettle; the sub-critical water is taken as an extraction solvent to carry out the exaction under the conditions of 1 to 20MPa of extraction pressure, 50 to 500W of ultrasonic power and 20 to 80KHz of ultrasonic frequency. The method has high extraction efficiency and short extraction time. The device is mainly characterized in that the extraction kettle is provided with an ultrasonic reinforced part which comprises an ultrasonic generator and an energy changing head; the ultrasonic generator is arranged on the external surface of the extraction kettle and at the upper part of the extraction kettle; the energy changing head and the extraction kettle cover are processed into a whole; the piezoelectric ceramic wafer of the energy changing head is arranged at the upper end of the extraction kettle cover; the variable-spoke rod of the energy changing head is directly arranged in the extraction kettle by the extraction kettle cover. The device can carry out selectable exaction of the articles to be extracted by changing the extraction parameters (temperature, pressure, time, etc.), thus realizing static extraction or dynamic circulation extraction.

The invention belongs to the technical field of extraction and purification of plant ingredients and particularly relates to a method for extracting and purifying cannabidiol from China-hemp. In the method, an ingredient of cannabidiol is extracted from floral leaves in a mature period of the China-hemp according to a supercritical CO2 extraction technique, a cannabidiol extract is further purified by macroporous adsorbent resin and a rapid purification system, a cannabidiol content of an obtained product is 98% or higher, and the cannabidiol product does not contain a psychotoxic ingredient tetrahydrocannabinol. According to the method, a chemical organic solvent is not used in an extraction process, so that the method is environment-friendly and is low in toxicity and high in efficiency; the loss of cannabidiol in an adsorption elution process is reduced in a purification process, so that the impurity ingredients such as tetrahydrocannabinol and the like are effectively removed, and the use of an organic regent is decreased, so that the purification cost is lowered, and the environmental pollution is reduced. The product is high in yield and purity, and the requirement for development of a value-added product of the China-hemp, in particular to the market requirement of the active ingredient of the cannabidiol product in the China-hemp, can be met, and especially, the cannabidiol product has the great application advantage in the pharmaceutical field.

The invention relates to a method for extracting vanadium by decomposing vanadium slag under normal pressure with sodium hydroxide solution. The method comprises the following steps of: adding vanadium slag or preprocessed vanadium slag, water and NaOH into a normal pressure reactor, wherein the mass ratio of NaOH to the vanadium slag is (2-6): 1, and the mass concentration of the sodium hydroxide solution is 65-90wt%; oxidizing in the presence of an oxidizing gas at the temperature 180-260 DEG C for 0.5-6 hours, and then diluting the obtained reaction sizing agent with diluent, thus mixed sizing agent containing sodium hydroxide, sodium vanadate, sodium chromate and slag tailing is obtained; and filtering and separating the mixed sizing agent at the temperature of 80-130 DEG C, thus the slag tailing and aqueous solution containing vanadium are obtained. The method provided by the invention has the advantages that the operating temperature is below the boiling temperature of solution, the process can be carried out under normal pressure, the operation is easy, and the safety is good; and the operating temperature is far less than the operating temperature of the traditional vanadium extracting process, the extraction ratio of vanadium is high, and the total vanadium content in the slag tailing is 0.5-1wt% (taking the weight of V2O5 as the basis).

The invention provides a high-pressure pneumatic blasting pressure relieving and transmission increasing method, comprising the steps of constructing a blasting drill hole in a coal layer, and carrying out high-pressure water jet seam cutting operation in the blasting drill hole at intervals, so that a lead seam groove is formed in a coal body around the blasting drill hole; feeding a blasting steel pipe with plugged top part into the blasting drill hole, forming a plurality of air vents at the front part of the blasting steel pipe, and sealing a section inside a hole opening of the blasting drill hole by 8-10 m, so as to form a cement plug; and connecting the blasting steel pipe with a high-pressure air station through a pipeline at the exposed end of the blasting steel pipe, and opening a valve arranged on the pipeline to inject high-pressure gas, so that the high-pressure gas is jetted by the blasting steel pipe from the air vents. On the basis of forming cracks and fractures formed in the fractures and cutting grooves of the original coal body, the high-pressure gas instantly impacts the blasting effect, so that the cracks and the fractures can be continuously expanded, and a lot of new fractures can be generated. Finally, a mutually communicated large fracture screen is formed in the coal body by using the blasting drill hole as a center, so that the purpose of pressure relief and transmission increase of the coal body can be realized. Furthermore, the high-pressure pneumatic blasting pressure relieving and transmission increasing method has the advantages of simple operation, easiness of realization and obvious effect.

The invention discloses a preparation method of ganoderma lucidum polysaccharide with high yield, which comprises the following steps: firstly, crushing ganoderma lucidum fruiting bodies into ganoderma lucidum powder, then sequentially extracting the ganoderma lucidum powder by adopting a microwave-assisted hot water extraction method and an ultrasonic-assisted hot water extraction method, and carrying out concentration, impurity removal, concentration, alcohol precipitation and drying on the obtained extracting solution to obtain water-soluble ganoderma lucidum polysaccharide; and extracting the ganoderma lucidum residues by adopting an alkali extraction method, and carrying out neutralization, dialysis, concentration, impurity removal, alcohol precipitation and drying on the obtained extracting solution to obtain alkali-soluble ganoderma lucidum polysaccharide. The method is used for extracting the ganoderma lucidum polysaccharide by combining microwave heating action and ultrasonic cavitation and extracting the alkali-soluble polysaccharide in the ganoderma lucidum by utilizing the alkali extraction method, thereby reducing the loss of the ganoderma lucidum polysaccharide; and the prepared ganoderma lucidum polysaccharide has the characteristics of high production yield, strong immunological activity and the like.

The invention relates to a method for efficiently extracting lithium from salt lake brine. The method comprises the following steps: (1) forming an extraction organic phase by an extraction agent, a co-extraction agent and a diluent, and then mixing the extraction organic phase with salt lake brine according to the volume ratio of (3-4):2 for three-stage extraction with single extraction time being 2-10 minutes to obtain an organic phase; and (2) mixing the organic phase obtained in step (1) with a reverse extraction acid solution (0-1 mol / L) for three-stage reverse extraction with single reverse extraction time being 2-10 minutes, and collecting an aqueous phase which is an aqueous solution containing lithium ions. The co-extraction agent of an extraction system of the method is hydrophobic ionic liquid, compared with conventional synergist ferric trichloride, the interference caused by iron ions is avoided, the reverse extraction acidity is greatly reduced, more importantly the lithium-magnesium separation factor is significantly improved, and the elution step of magnesium ions is reduced; in addition, the method provided by the invention is easy in process, easy to control, high in operation reliability, and good in recyclability of the organic phase, and greatly reduces the production cost for extracting the lithium from the salt lake brine.

The invention discloses a refection reducing and outburst eliminating method for deep-hole hydraulic fracture driving gas shallow hole extraction. The method comprises the following steps of: gradually and alternately constructing hydraulic fracture holes and gas extraction holes in the coal bed direction in a coal mining working face tunnel, an airway or a tunneling working face, and performing high-pressure water injection and gas extraction; stopping injecting water after the water is injected into the hydraulic fracture holes for 0.5 to 5 hours, and changing gas extraction pipe joints to extract gas; after the hydraulic fracture hole or gas extraction concentration is lower than 5%, changing water injection pipes to perform static pressure water injection; and when the coal mining working face is recovered to the position 5 meters away from the static pressure water injection holes or the tunneled working face is tunneled again, stopping a pump or closing a static pressure water valve to stop water injection. According to the method, refection reduction of the gas-containing coal bed is realized, the gas extraction rate is improved, the gas in the mining space is effectively prevented from exceeding the limit, outburst risks of coal and gas are reduced, and safe and efficient recovery of coal is ensured. The method is simple and good in effect.

A process for extracting protein and chitin from fly maggot and preparing chitosan from the chitin incldues such steps as extracting hydrolytic protein by enzyme hydrolysis, removing stink and enhancing fragrance by Maillard reaction, enzymolyzing, removing yellow substances and black spot, etc. The quality of produced protein and chitin conforms with food grade standard.

A process technology using enzymolysis method to extract leftover fish oil from fish processing comprises the following steps: preliminary treatment, in which the leftovers from the fish processing are cleaned and minced; protease hydrolysis, in which neutral protease and papain are hydrolyzed simultaneously; oil-water separation, in which hydrolysate is centrifugally filtered to remove residues, and filtrate undergoes oil-water separation via a centrifuge, thereby obtaining the fish oil and hydrolyzed protein; and fish oil refinement, in which refined fish oil can be obtained after the fish oil is degummed, depickled, decolored and deodorized. The leftovers from the fish processing can be hydrolyzed with the proteases to destroy the associative relation of protein and fat, thereby releasing axunge which undergoes oil-water separation by the tubular centrifuge to obtain the fish oil with high quality, and meanwhile, the protein therein can be fully utilized to produce hydrolyzed protein, so as to change wastes into valuables and synthetically and efficiently utilize the resources of the fish and the processing leftovers.