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758 results about "Phase splitting" patented technology

Method for non-saponification extraction and separation of light rare earth elements

The invention discloses a method for non-saponification extraction and separation of light rare earth elements. After a compound extraction agent consisting of acid phosphorus type extraction agent, alkaline amine type extraction agent and solvent oil is mixed with phosphate solvent or organic alcohol solvent at 30-70 DEG C, chlorinated light rare earth liquid is extracted and separated; and the water washing and the hydrochloric acid reverse extraction are performed to finally realize the separation of La, Ce, Pr and Nd; and a mixed organic phase after the reverse extraction is returned to an extraction tank for recycling. The method pretreats the mixed organic phase consisting of the compound extraction agent and the solvent, so that such defects as high viscosity, weak mobility, easy emulsification and long phase splitting time are overcome; the method has no need to saponify the acid phosphorus type extraction agent, so that no alkali liquor consumption and no waste water emission in the extraction process are realized, but the separation capacity of a saponification extracting agent system is achieved, and the extraction grade is reduced compared with that needed by the saponification extracting agent system; and the method is a rare earth element separation process with economy and high efficiency.
Owner:GUANGXI NORMAL UNIV

Distribution network ground fault arc suppression method based on three-phase cascade H bridge converters

The invention relates to a distribution network ground fault arc suppression method based on three-phase cascade H bridge converters. The three-phase cascade H bridge converters are adopted to replace arc suppression coils and mounted between phase lines and the ground, and power is supplied to capacitors on the direct current side of the converters by using phase voltages, so that boosting transformers and grounding transformers are saved, and the problem of source taking difficulty on the direct current side of the converters is solved. The converters inject current to a distribution network in a phase splitting mode to compensate the total current of a ground fault to be zero or to inhibit the phase voltage of the fault to be zero, so that the arc is automatically extinguished; and the reference compensation current is calculated by using real-time measured zero sequence voltage, so that the fault phase identification link is saved. The operation is simplified by using the voltage arc suppression method of controlling the zero sequence voltage to adjust the injected compensation current. In view of the influence of circuit parameters and load current on the arc suppression effect and the deduced relation between the ground fault residual current after the voltage arc suppression method is applied and the zero sequence voltage after the fault, an adaptive arc suppression method is put forward by using the zero sequence voltage as a voltage and current arc suppression method.
Owner:SHANGHAI HOLYSTAR INFORMATION TECH

Automatic power-passing phase-splitting apparatus of AC drive electric locomotive

InactiveCN101434206APromise to leaveEnter smooth autoPower supply linesOvervoltageEngineering
The invention discloses an automatic passage method through phase splitting for an AC-DC-AC electric locomotive which comprises the following steps: before the electric locomotive runs into a neutral section, a traction control system controls a traction motor to work in a regenerative braking mode and controls an inverter to stabilize intermediate DC voltage; a pulse rectifier works in an inversion state; an alternating voltage equal to a traction voltage is generated on the primary side of a traction transformer, thereby making the primary side of the traction transformer obtain zero current from a power supply arm; after the electric locomotive runs into the neutral section, the intermediate DC voltage still maintains stability; the AC phase generated by the inversion of the pulse rectifier in the inversion mode changes gradually so as to make the voltage of the primary side of the traction transformer change to become equal to the traction voltage of a next power supply arm; and then the electric locomotive enters the next power supply arm and runs normally. The method enables the automatic passage through phase splitting; in addition during the phase splitting, a main circuit breaker does not need to be turned on and off without arc discharge, interception overvoltage and closing surge overcurrent, and an auxiliary system is not deenergized; and the passage through phase splitting has short time, low traction loss and small speed drop.
Owner:SOUTHWEST JIAOTONG UNIV

Method for extracting and salting organic acids out of fermentation liquor

The invention belongs to the technical field of bioengineering, and relates to a method for extracting and salting organic acids out of fermentation liquor. The method is characterized in that: soluble inorganic or organic salt solids or concentrated solution thereof and an extracting agent are added into the organic acid fermentation liquor, stirred for uniform mixing, and stood at room temperature for phase splitting; when two phases are formed by the salting-out and extraction, an upper phase is a solvent phase rich in the organic acids, while a lower phase is a salt phase rich in other components; if the extraction operation is directly performed without pretreating the fermentation liquor, a solid phase layer rich in bacteria and proteins is formed between the two phases; when three phases are formed, the upper phase is the solvent phase, a middle phase is the phase rich in the organic acids and the lower phase is the salt phase rich in the other components; therefore, the aim of extracting and separating the organic acids is fulfilled. The method solves the problems of difficulties in product separation, high cost and the like in the conventional process for separating the organic acids by a fermentation method, is simple, ensures separation time, low cost and high recovery rate, and is an organic acid separation method with industrial application prospect.
Owner:DALIAN UNIV OF TECH

Separation and recovery method for leaching solutions of waste battery material containing nickel, cobalt and manganese

The invention provides a separation and recovery method for leaching solutions of waste battery material containing nickel, cobalt and manganese. The method comprises the steps of adopting trialkyl hydroxamic acid for extracting solutions to be treated for obtaining organic phases 1 and aqueous phases 1, wherein the nickel and the cobalt are extracted into the organic phases 1, and manganese ions and lithium ions are left in the aqueous phases 1; adopting sulfuric acid or hydrochloric acid for carrying out reverse extraction on the organic phases 1 for obtaining organic phases 2 and aqueous phases 2, wherein the nickel and the cobalt are reversely extracted into the aqueous phases 2; adopting a second extraction agent for extracting the aqueous phases 2 for obtaining organic phases 4 and aqueous phases 4, wherein the cobalt is extracted into the organic phases 4 and the nickel is left in the aqueous phases 4 for forming nickel solutions; adopting the sulfuric acid or hydrochloric acid for carrying out reverse extraction on the organic phases 4 for obtaining cobalt solutions; adopting a third extraction agent for extracting the aqueous phases 1 for obtaining organic phases 5 and aqueous phases 5 after phase splitting, wherein the manganese is extracted into the organic phases 5 and the lithium ions are left in the aqueous phases 5; adopting the sulfuric acid or hydrochloric acid for carrying out reverse extraction on the organic phases 5 for obtaining manganese solutions.
Owner:TSINGHUA UNIV

Method of preparing phase-change energy-accumulation material microemulsion

InactiveCN101508887AHigh viscosityLarge apparent specific heat capacityHeat-exchange elementsFreeze thawingSurface-active agents
The invention relates to a method for preparing phase change energy storage material microemulsion, comprising the steps: first, 10 parts by weight of organic phase change energy storage material can be prepared; 1-4 parts by weight of surface active agent, 1-3 parts by weight of cosurfactant, 0.3-1.5 parts by weight of inorganic salt and 10-100 parts by weight of de-ionized water or distilled water are added into the organic phase change energy storage material; after that, the mixed solution is evenly stirred and mixed at a certain temperature and then stands still; finally, the microemulsion is obtained until bubbles are completely removed; wherein, the surface active agent is compound of surface active agent A and surface active agent B, the HLB values of which are respectively 1-10 and 11-20; the weight ratio between the surface active agent A and the surface active agent B is 1:1.5-4.5, and the HLB value is 8-18 after being compounded. The obtained microemulsion is a stable system of thermodynamics, has transparent appearance, and does not have the phenomenon of phase splitting and emulsion breaking caused by a plurality of times of phase transition process due to the actions such as a plurality of times of freeze thawing, centrifugal separation and the like, thereby fundamentally overcoming the defect of poor stability of conventional emulsion and being long in service life.
Owner:SHENZHEN GRADUATE SCHOOL TSINGHUA UNIV

Cascaded multi-level-based ground overvoltage phase splitting device

InactiveCN103818271ALower requirementRealize feed-through power supplyPower supply linesElectricityOvervoltage
The invention discloses a cascaded multi-level-based ground overvoltage phase splitting device. The cascaded multi-level-based ground overvoltage phase splitting device is characterized in that the position of a train is determined by the aid of locomotive position sensors CG1, CG2, CG3 and CG4 which are arranged on a rail, a ground overvoltage phase splitting device which is connected to two adjacent phases outputs single-phase alternating-current voltages under the control, and amplitude values, frequencies and phases of the voltages are identical to an amplitude value, a frequency and a phase of a voltage of an A-phase bridge arm when the train is positioned on an A-phase bridge arm side; when an electric locomotive enters a neutral section, output voltage which is identical to the A-phase voltages the amplitude values, the frequencies and the phases of the A-phase voltages is converted to be identical to the B-phase amplitude values, frequencies and phases of the B-phase voltages. The cascaded multi-level-based ground overvoltage phase splitting device has the advantages that flexible passing voltage phase splitting can be implemented on the electric locomotive (or a motor train unit) by the aid of the cascaded multi-level-based ground overvoltage phase splitting device, impact on an overhead line system and the electric locomotive (or the motor train unit) can be prevented, and requirements on switch devices can be lowered; uninterrupted power supply passing voltage phase splitting can be implemented on the train; the cascaded multi-level-based ground overvoltage phase splitting device has an important significance on implementing through type power supply on the overhead line system with electric phase splitting.
Owner:SOUTHWEST JIAOTONG UNIV

Sample pretreatment method for detection of organochlorine pesticide residue in food

The invention discloses a sample pretreatment method for detection of organochlorine pesticide residue in food and is characterized by comprising the following steps: water is added to a food sample, sample solution is swirled, and then inorganic salt and hydrophilic organic solvent are added to the sample solution, the sample solution is swirled and shaken uniformly, the sample solution undergoes phase splitting after centrifugation at room temperature, the upper-phase liquid is purified through dispersion solid-phase extraction method, the extraction temperature is 20-30 DEG C, and finally the upper-phase liquid is detected by gas chromatography; and the mass percent of the inorganic salt accounts for 5%-35% of the total mass of the system, the mass percent of the hydrophilic organic solvent accounts for 10%-50% of the total mass of the system, and water is of the residual amount, and the total mass of the system is the mass sum of water contained in the sample, the added water, the inorganic salt and the hydrophilic organic solvent. According to the sample pretreatment method, a dual-water-phase system consisting of the hydrophilic organic solvent, the organic salt and water is utilized, the partition coefficient is increased by means of changing the types and concentrations of the organic solvent and the inorganic salt, and the organochlorine pesticide residue in the sample can be directly extracted at room temperature.
Owner:YANTAI UNIV

Process for extracting nickel and cobalt from laterite by ore pulp extraction technology

The invention relates to a process for extracting nickel and cobalt from laterite by ore pulp extraction technology, which comprises the following steps of: crushing and grinding the laterite; putting into a high-pressure kettle, and carrying out high-pressure acid leaching to remove iron; pouring into a mixing settling extraction tank with a stirring and settling tank and a baffle plate, carrying out 5-12 grade of extraction, back extraction and phase splitting and washing to respectively obtain mixed solution of nickel and cobalt, waste liquid containing impurities and the ore pulp; extracting and separating nickel from cobalt to respectively obtain pure nickel solution and pure cobalt solution; and precipitating and calcining to obtain nickel oxide and cobalt oxide products. The solution with high concentration is obtained by extraction, the process is shortened, the liquid-solid separation load and a number of washing and filtering processes are reduced, so that energy consumption of production and production cost are reduced and the economic benefit is improved. An extracting agent can be used repeatedly after being saponified and has relatively low comprehensive consumption. The speed of the extraction process is high and is commonly less than 10 minutes. The extraction efficiency is high. The extracted ore pulp can be neutralized uniformly so as to reduce the treatment cost of tailings. The process is simple; the recovery rate is higher; and the nickel and cobalt recovery rates are both more than or equal to 90 percent and the process is easy to popularize.
Owner:JILIN JIEN NICKEL IND +1

Method for extracting lithium from salt lake brine by extraction method

The invention relates to a method for extracting lithium from salt lake brine by an extraction method. The method is suitable for a production process that lithium carbonate and lithium chloride are prepared from high magnesium-lithium ratio salt lake brine and concentrated old brine which contains lithium of salt pan. Co-extraction agent FeCl3, extraction agent and diluent are adopted to carry out lithium extraction, wherein the extraction agent is mixture of neutral phosphorus oxide compound A and phase modifier B, the phase modifier B is organic compound which can generate protonation reaction with the neutral phosphorus oxide compound A in an extraction reaction process, an extraction complex composition obtained after the extraction agent is used for lithium extraction is xLiFeCl4.yHCl.aA.bB, and the extraction complex can be easily dissolved in diluent; an extraction system has good phase splitting performance and reverse extraction and regeneration performance, and the lithium extraction technology of the extraction method is further optimized. The method has a low requirement on equipment, the adopted organic compound is cheap and can be easily obtained, and therefore, the method is suitable for industrial application.
Owner:JIANGXI HZONE LITHIUM TECH

Medium-voltage flexible direct current tractive power supply system and controlling method thereof

The invention discloses a medium-voltage flexible direct current tractive power supply system and a controlling method thereof. The tractive power supply system comprises more than one traction powersubstation. The traction power substation comprises a three-phase step-down transformer, a three-phase electric reactor, a voltage source current converter and a first direct current bus which are connected successively. The input end of the three-phase step-down transformer is connected to a three-phase power grid. The positive pole and the negative pole of the output end of the voltage source current converter are connected to the positive pole and the negative pole of the first direct current bus. The positive pole and the negative pole of the first direct current bus are connected to a contact system and a steel rail. The beneficial effects of the medium-voltage flexible direct current tractive power supply system are that the electric energy quality of the system can be greatly improved, the electric phase splitting link is completely eliminated, and the through power supply of the whole traction network is realized. In addition, the system is capable of increasing the power supply distance of the single traction substation, and realizing the renewable energy sources along the railway and the effective utilization of the locomotive regenerative braking energy.
Owner:SOUTHWEST JIAOTONG UNIV

Preparation method of GO (graphene oxide)-SiO2 hybrid particle composite fiber super/microfiltration membrane

The invention discloses a preparation method of a GO (graphene oxide)-SiO2 hybrid particle composite fiber super/microfiltration membrane. The method comprises the following steps: 1) preparing GO-SiO2 hybrid particles; 2) preparing a high-molecular polymer, an additive, the GO-SiO2 hybrid particles, a solubilizer and an organic solvent into multiple homogenized film casting solutions in different proportions; 3) removing stains on the surface of a braided hose; 4) uniformly coating the film casting solution onto the outer wall of the braided hose; and 5) sending the coated braided hose into a gel bath, and carrying out phase splitting, thereby finally obtaining the modified hollow fiber composite super/microfiltration membrane. The GO-SiO2 hybrid particles with favorable dispersity are added to effectively enhance the solubility of the nanoparticles in the film casting solution under the synergic action of the solubilizer, thereby enhancing the tensile strength of the hollow fiber composite membrane wire and obtaining larger membrane area by using a small amount of the film casting solution. The composite membrane has high anti-pollution and antibacterial capacities, and maintains higher flux and a certain interception rate.
Owner:XI'AN UNIVERSITY OF ARCHITECTURE AND TECHNOLOGY
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