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774results about "Surface tension analysis" patented technology

Apparatus and method for testing solid-liquid dynamic and static contact angles by actual liquid droplet method

The invention discloses an apparatus and a method for testing solid-liquid dynamic and static contact angles by an actual liquid droplet method. The method comprises the following steps of: during the testing, placing a solid phase sample on a sample table; controlling X, Y and Z of the sample table to move to a focusing position of a lens; sucking the liquid phase sample into a micro sample injector, injection pump or peristaltic pump; controlling the X, Y and Z of the sample injector to move to the focusing position; dripping a small droplet of the liquid and adsorbing the droplet to a needle head; moving the needle head to the surface of the solid phase sample until the liquid phase sample is adsorbed to the surface of the solid; making a software system control an optical imaging system (CCD) to capture a real-time picture and analyzing the picture by using the actual liquid droplet method; and displaying calculated solid-liquid contact angle value, solid surface free energy value and adhesion work value and managing the values by a database. The apparatus and the method can completely improve the accuracy of the analysis of the solid-liquid interfacial tension, are simple to operate, can be widely applied and have high popularization value.
Owner:上海梭伦信息科技有限公司

Real time determination of gas solubility and related parameters in manufacturing processes

Methods and apparatuses for determining entrained and / or dissolved gas content of gas-liquid mixtures. Data generated is used to control the True (air-free) or Apparent (air-containing) Density or Entrained Air content of liquids within optimum ranges, e.g. in paper coating processes and in the manufacture of food products, personal care products, pharmaceutical products, paints, petroleum blends, etc. For example, an indirect method of continuously determining the amount of gas entrained in a liquid, by: continuously measuring the temperature, flow rate, and apparent density of the mixture at two different pressure states, and calculating the volume percentage of the gas in the liquid by using equation (28) x⁢%=VsVs+V(28)wherein V is the volume of the gas-free liquid calculated by equation (23) V=1ρ1-[P2P2-P1⁢(1ρ1-1ρ2)-RTP2-P1⁢g⁡(Δ⁢ ⁢PQa)](23)in which P1 and P2 are two different ambient pressures and ΔP=P2−P1, ρ1 and ρ2 are apparent densities of the liquid sample measured at P1 and P2, respectively, R is the constant of the Ideal Gas Law, T is the liquid temperature, Q is the flow rate, g(ΔP / Qa) is a function for determining the amount of gas being dissolved between P2 and P1, and Vs is determined by equation (27) Vs=TsT⁢P1⁢P2Ps⁡(P2-P1)⁢(1ρ1-1ρ2)-RTsPs⁢(P1P2-P1⁢g⁡(Δ⁢ ⁢PQa)-g⁡(P1-PsQa)).(27)
Owner:APPVION INC

Method for synchronously measuring temperature, surface tension and contact angle of droplet by controlling temperature and humidity

The invention belongs to the technical field of chemical measurement. A temperature and humidity control system is adopted to accurately control the environment in a sample case, namely the temperature ranges from minus 80 DEG C to plus 300 DEG C and the accuracy is +/-0.1 DEG C, the relative humidity ranges from 0%-100% and the accuracy is +/-2%-+5%. A high-speed data acquisition system and a high-speed camera system are adopted to synchronously measure the temperature and profile image of a droplet accurately. The sampling frequency of the temperature can be as high as 1MHz and the sampling speed of the image can reach 420 frames/s. Sample data are transmitted to a computing system through data lines and the temperature of the droplet is obtained. The image data are fitted according to the Bashforth-Adams equation and Yong-laplace equation to obtain such numerical values as surface tension and contact angle, etc. The device has simple operation, high testing accuracy and good repeatability of experimental results and is suitable for synchronously measuring the temperature, surface tension and contact angle under the conditions of wide temperature range and total humidity.
Owner:NANJING UNIV

Interfacial rheological testing method and apparatus by using liquid drop imagery

The invention discloses an interfacial rheological testing method and an interfacial rheological testing apparatus by using liquid drop imagery. According to the invention, after least squares fitting and secondary optimization by using a Newton iteration method are carried out on a discretized Young-lapalace equation theoretical calculated curve and an actual liquid drop contour boundary curve, interfacial chemical properties like surface tension, interfacial tension and a contact angle value, the volume, the area and the wetting line of liquid drops, etc. can be calculated; then interfacial rheological properties like interfacial dilational elasticity Epsilon d and interfacial dilational viscosity Eta d can be obtained through analysis by using an interfacial tension relaxation method; a set of liquid drop sample introduction system and a set of testing apparatus are provided, liquid drop oscillation is realized through corresponding control software so as to increase or reduce the amount of liquid drops and allow oscillation process to accord with sine, cosine, square wave and sawtooth changes. The apparatus provided by the invention enlarges the application field of optical interface chemical analysis apparatuses and meets requirements for high-precision automatic testing of dynamic/static contact angle values, dynamic/static surface tension values, interfacial tension values and interface rheological measurement values.
Owner:上海梭伦信息科技有限公司

Apparatus and method for measuring middle and low-temperature smelt surface tension, density and wettability

Disclosed is an apparatus for measuring surface tension, density and wettability of a medium-low temperature fused mass, which relates to the technique field of fused mass property measurement. The apparatus comprises: a heating device (1), a transparent quartz furnace tube, a light source (8), a digital camera (11) and a computer (12); and the transparent quartz furnace tube is horizontally positioned in the heating device (1), and both ends of the transparent quartz furnace tube stretch out of the heating device by 10 to 15cm. The light source (8), the digital camera (11) and the transparent quartz furnace tube are positioned at the same horizontal line; and software installed on the computer (12) can realize the on-line connection with the digital camera (11), dynamic changes of melt drip contour can be displayed dynamically on a computer display directly, and photo taking and animation shooting can be controlled by the computer. The apparatus has the advantages of adjusting the level of base plate conveniently and accurately, improving the measuring precision and repeatability; good sealing, available selection of a plurality of atmospheres such as vacuum, air and high purity argon gas; realizable on-line measurement of thermal property such as surface tension; and low cost of manufacture and simple operation.
Owner:INST OF PROCESS ENG CHINESE ACAD OF SCI

Non-contact techniques for measuring viscosity and surface tension information of a liquid

A non-contact method for measuring viscosity and surface tension information of a liquid in a first liquid containment structure. The steps of the method include oscillating a free surface of the liquid in the liquid containment structure; detecting wave characteristics of the oscillating free surface; and analyzing the wave characteristics. The oscillating step may be performed by propagating an acoustic wave from an acoustic wave emitter, through said liquid containment structure, towards the free surface. The detecting step may be performed by delivering a series of acoustic pulses at the free surface and detecting acoustic reflections from the free surface as the oscillating free surface relaxes. The analyzing step can be performed by comparing the wave characteristics with a candidate liquid wave characteristics. Prior knowledge and behavior of the selected candidate liquid can thus be imputed to the source or sample liquid. The sample liquid can be one of photoresist, solder or a biological compound. In a variation a method for acoustically ejecting a droplet of a first liquid from a first liquid containment structure comprises measuring viscosity and surface tension information of the first liquid in the first liquid containment structure and directing a variable amount of acoustic energy through the first liquid to cause the droplet ejection wherein the variable amount of acoustic energy is based on the measuring viscosity and surface tension information of the first liquid in the first liquid containment structure. Apparatuses and systems for carrying out the same are included.
Owner:LABCYTE

Device and method for testing contact angle and interfacial tension at ultrahigh pressure and high temperature

The invention discloses a device and method for testing a contact angle and interfacial tension at ultrahigh pressure and high temperature, and relates to a testing method for testing a contact angle and interfacial tension by the adoption of a vacuum liquid drop method or image fitting method for fitting a Young-Laplace equation, and a testing device for testing a contact angle and surface / interfacial tension at ultrahigh pressure and high temperature. The device is composed of two booster pumps, an ultrahigh-pressure and high-temperature cavity of a two-side observation window made of sapphire glass, a high-viscosity sample heating pool, a high-pressure connection accessory, a camera with a telecentric lens, a collimated light source and the like. After a liquid drop outline image is shot, the fitting Young-Laplace equation is used for testing the contact angle and the interfacial tension value, and the testing device and method can analyze the contact angles and interfacial tension values under different pressure conditions, have the extremely high popularization value in the fields of oil field, petrochemical engineering, new material research and the like, particularly can test the interfacial tension value and the contact angle by simulating recovery environment actual pressure and temperature conditions in tertiary oil recovery simulation experiments, and are quite effective.
Owner:上海梭伦信息科技有限公司

Method for synchronously measuring temperature and roll angle of droplet by controlling temperature and humidity

The invention belongs to the technical field of chemical measurement. A temperature and humidity control system is adopted to accurately control the environmental conditions in a sample case, namely the temperature ranges from minus 80 DEG C to plus 300 DEG C and the accuracy is +/-0.1 DEG C, the relative humidity ranges from 0% to 100% and the accuracy is +/-2%-+/-5%. A driver is adopted to accurately control the speed and angle of rotation, namely the rotating speed is 0.01 degree/S-10 degrees/S, the measurement ranges of the roll angle, advance angle and receding angle are between minus 180 degrees and plus 180 degrees and the accuracy is +/-0.01 degree. A high-speed data acquisition system and a high-speed camera system are adopted to synchronously measure the temperature and profile image of a droplet accurately. The sampling frequency of the temperature can be as high as 1MHz and the sampling speed of the image can reach 420 frames/s. Sample data are transmitted to a computing system through data lines and the temperature of the droplet is obtained. Software is adopted to analyze the image to obtain the temperature, roll angle, advance angle and receding angle of the droplet. The device has simple operation, high testing accuracy and good repeatability of experimental results and is suitable for synchronously measuring the temperature, roll angle, advance angle, receding angle and lag angle under the conditions of wide temperature and humidity ranges.
Owner:NANJING UNIV

Interface tension measuring device and method by hanging drop or bubble blowing way under high pressure

The invention relates to an interface tension measuring device and method by a hanging drop or bubble blowing way under high pressure and belongs to the technical field of high-temperature high-pressure interface tension measuring. The device comprises a window pressure chamber device composed of a metal pressure chamber cylinder body and high pressure resistant glasses at two ends, a liquid drop/bubble injection device, a support and locking device and a photo and data processing device, wherein a liquid/gas inlet hole is formed in the side wall of the pressure chamber cylinder body and connected with a gas cylinder or a liquid charging pump through a quick connector, so as to realize the feeding of environmental gas or liquid into the pressure chamber cylinder body; a liquid/gas outlet hole is connected with a three-way connector, one path of the three-way connector is connected with a drain valve, and the other path is connected with a vacuum pump for vacuum-pumping of the pressure chamber; the liquid drop/bubble injection device comprises an injection tube and a pressure sensor; the injection tube is inserted into the cylinder body, and is sealed and connected with the pressure sensor to monitor the injection pressure, and the other end of the injection tube is connected with the liquid charging pump or the gas cylinder through a precision needle valve; the support and locking device comprises a base, a support frame and a locking bolt; the photo and data processing device comprises a CCD camera, a backlight and a data processing computer.
Owner:DALIAN UNIV OF TECH
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