The application discloses a kind of efficient pretreatment methods for detecting element in extraction
system organic phase, it includes the following steps:
pipette appropriate amount of measured organic phase to
volumetric flask, add appropriate amount of back extraction acid, then add water to 1 / 3-2 / 3 of
volumetric flask volume, cover
bottle plug; Shake the back extraction of
volumetric flask, and stand and separate, then use
filter paper to draw and remove upper organic phase, after removing upper organic phase, the remaining aqueous phase is filtered using
filter paper and the primary filtrate is discarded, and the filtrate is the sample to be detected, for
element analysis detection.The method simplifies the operation process, is simple to operate, high in detection efficiency, and is not easy to contaminate;The organic
phase volume used in the pretreatment operation of the method is small, compared with the existing back extraction method of
separatory funnel, the amount of organic phase used is one tenth of the back extraction method of
separatory funnel, or even less, reducing the waste of organic phase, at the same time, the amount of back extraction acid is reduced, and the amount and consumption of
reagent are greatly reduced.