3629 results about "Active group" patented technology

Devices and methods are described for providing continuous measurement of an analyte concentration. In some embodiments, the device has a sensing mechanism and a sensing membrane that includes at least one surface-active group-containing polymer and that is located over the sensing mechanism. The sensing membrane may have a bioprotective layer configured to substantially block the effect and / or influence of non-constant noise-causing species.

Devices and methods are described for providing continuous measurement of an analyte concentration. In some embodiments, the device has a sensing mechanism and a sensing membrane that includes at least one surface-active group-containing polymer and that is located over the sensing mechanism. The sensing membrane may have a bioprotective layer configured to substantially block the effect and / or influence of non-constant noise-causing species.

Devices and methods are described for providing continuous measurement of an analyte concentration. In some embodiments, the device has a sensing mechanism and a sensing membrane that includes at least one surface-active group-containing polymer and that is located over the sensing mechanism. The sensing membrane may have a bioprotective layer configured to substantially block the effect and / or influence of non-constant noise-causing species.

Devices and methods are described for providing continuous measurement of an analyte concentration. In some embodiments, the device has a sensing mechanism and a sensing membrane that includes at least one surface-active group-containing polymer and that is located over the sensing mechanism. The sensing membrane may have a bioprotective layer configured to substantially block the effect and / or influence of non-constant noise-causing species.

Devices and methods are described for providing continuous measurement of an analyte concentration. In some embodiments, the device has a sensing mechanism and a sensing membrane that includes at least one surface-active group-containing polymer and that is located over the sensing mechanism. The sensing membrane may have a bioprotective layer configured to substantially block the effect and / or influence of non-constant noise-causing species.

A method and apparatus for adding a member to an active call in a group communication network provides for receiving a member list from a user and sending a request to a server to add the member list to the active group call. The method and apparatus further provides for announcing each member in the member list that they are being added to the group call, receiving acknowledgement from a member who wishes to participate in the group call, and forwarding media to the member. The method and apparatus also provides for a significant reduction in the actual total dormancy wakeup time and latency by exchanging group call signaling even when mobiles are dormant and no traffic channel is active.

The invention discloses a method for producing humic acid and salt thereof through the oxidative degradation of young lignite. The method comprises the following steps: carrying out the oxidation reaction of the lignite containing the humic acid and aqueous hydrogen peroxide solution; after the reaction, obtaining water soluble fulvic acid through centrifugal separation, supernatant filtration, concentration and drying; adding alkali into the fulvic acid to prepare a fulvic acid salt product; carrying out the alkaline extraction and centrifugal separation of the residue deposit of the production of the fulvic acid, adding acid into the supernatant till the pH value is 1 to 2, carrying out a reaction at an increased temperature or room temperature, carrying out centrifugal separation after the reaction is finished, and obtaining purified ulmic acid after precipitation and drying; and directly concentrating and drying the supernatant in the previous step to obtain the humate. The method can improve the yield of the fulvic acid and total humic acid in the young lignite, and simultaneously increase the active group in the humic acid. The method can be used for producing fulvic acid, fulvic acid salt, ulmic acid and ulmic acid salt products. In particular, the method puts an end to the environmental pollution caused by the nitric acid which is taken as an oxidation degradation agent. In addition, the method has a short technological line, low cost, simple requirements on equipment, and moderate conditions. The method which can be applied to the industrialized production has good application prospect.

The invention belongs to the technical field of a new chemical material, and in particular relates to a high-durability super-hydrophobic self-cleaning coating material and a preparation method thereof. The coating material of the invention is prepared by curing and drying nanoparticles with photo-catalytic activity, a low-surface-free-energy polymer and a cross-linking agent at the room temperature, wherein the low-surface-free-energy polymer consists of one or more of polysiloxane fluoride, dimethyl silicone polymer and polyphenylene methyl siloxane, which contain active groups, such as hydroxyl alkoxy group, carbon-carbon double bond, silanol group, siloxy group, and the like; the cross-linking agent is hydrogen-containing silicone oil or aminosilane; and the mass content of the photo-catalytic nanoparticles in the coating ranges from 10 to 60 percent. The coating is formed into a micro-nanostructure by nanoparticle self-organization; a super-hydrophobic self-cleaning coating with lotus effect is prepared from the coating and a cross-linked filming matrix with low surface energy; the persistence of a lotus-shaped super-hydrophobic characteristic of the coating is realized by using the photo-catalytic decomposition characteristic of an organic pollutant for the nanoparticles; and thus the material is suitable for large-area construction and has high weathering resistance andprominent self-cleaning characteristic.

The invention discloses a super hydrophobic anti-icing coating and a preparation method thereof, and is realized by preparing a fluorine contained acrylic resin and combining the fluorine contained acrylic resin with organosilicon resin and nano particles. In a scheme of the invention, the fluorine contained acrylic resin has small surface energy and strong hydrophobicity. The organosilicon resin utilizes effect of -CH3 on a surface thereof and small polarity to substantially reduce contact angle hysteresis. The fluorine contained acrylic resin can crosslink and solidify with the nano particles and active groups in the organosilicon resin to form a composite network. The invention can overcome defects of complex technology, high costs and unsuitability for large scale usage of an ordinary method for preparing a super hydrophobic coating; and the prepared coating can realize super hydrophobic anti-icing effect through a regular spraying method.

The invention discloses a preparation method of multiple cross-linked polysaccharide injectable hydrogel. Modified water-soluble chitosan with carboxyl or hydroxyl groups as a first component and a hydroformylation-modified polysaccharide polymer or polysaccharide polymer mixer as a second component produce electrostatic action with each other and undergo a Schiff-base reaction to produce the hydrogel with a multiple cross-linked net structure. The multiple cross-linked polysaccharide injectable hydrogel has gelling time of 5-200s and has good mechanical properties. Through change of a chitosan and polysaccharide modification rate, a mole ratio of two components and solid content of hydrogel, gelling time, mechanical strength, microscopic morphology and water content are adjusted and controlled. The gel network contains a large amount of amino, carboxyl and aldehyde groups as active groups, the active groups can be bonded to drugs and proteins by covalent bonds, the multiple cross-linked polysaccharide injectable hydrogel as a novel medical material with excellent biocompatibility has a good application prospect in the fields of regeneration medical science, tissue engineering and drug controlled release.

The invention relates to a kind of nano cellulose solid - solid phrase change material and its producing method. Its characteristics are: in non-homogeneous phase system, according to the reactants proportions as polyethylene glycol containing active group at one end or both ends 19.8% - 82.0%, crosslinking agent 0% - 55.1% and nanometer cellulose or its ramification 4.0% - 69.5%, ingraft the polyethylene glycol containing active group at one end or both ends as energy storing function group onto nanometer cellulose or its ramification framework material. The biggest enthalpy of phase change of the nanometer cellulose solid - solid phrase change material of the invention can get to over 110 J / g, the phrase change temperature is 0 - 60 Deg. C, and can keep good solid state before and after the phrase change. It won't occur phrase separation, besides it is non-toxic and harmless, low cost, simple producing technics.

The invention relates to a transparent butyl hot-melt sealant, which is prepared with the following raw materials in parts by weight: 1-20 of butyl rubber, 10-80 of polyisobutylene, 5-30 of plasticizer, 3-10 of tackifier, 3-10 of softener, 0.1-5 of stabilizer, 5-30 of filler and 0.1-5 of adhesion promoting agent. The matching use of the butyl rubber and the polyisobutylene with different molecular weights facilitates the improvement of the strength and workability of the transparent butyl hot-melt sealant. The filler is selected from fumed silica or precipitated silica, which ensures the appearance transparency of the product. Due to the addition of the stabilizer and the strict control of the production process, the appearance transparency and the physical and chemical properties of the product are enhanced. The use of the active group substituted alkoxy silane as a coupling agent improves the adhesion of the product to glass, aluminum and other substrates.

A method for preparing the tinted contact lens with the covalently bonded novel reactive tinting compound is disclosed. The reactive tinting compound with mono vinyl functionality is prepared by reacting the reactive dye with a hydrophilic monomer containing both pendent hydroxyl and vinyl groups under an alkaline condition. The water soluble reactive dyes containing either difluoro-chloropyrimidine or β-sulphatoethylsulphone reactive groups are used for synthesis of the reactive tinting dye. The lens forming materials are photo-polymerized in the presence of the reactive tinting compound to prepare a tinted contact lens. The reactive tinting compound is copolymerized with the lens forming monomers in a single photo-polymerization step that requires no subsequently alkaline soaking or developing step as used in the prior art. In addition, the covalently bonded dye is stable and durable in the lens and does not fade or leach out after multiple high-pressure thermal sterilizations.

The invention provides a graphene / polysiloxane composite coating material and a preparation method thereof. The method comprises the following steps: modifying the graphene surface with active groups by a chemical modification technique to obtain modified graphene, mixing the modified graphene with a silane compound, a dispersion medium, a non-essential comonomer and a non-essential accelerator, and carrying out hydrolytic condensation or hydrolytic condensation-free radical polymerization to generate a graphene / polysiloxane composite resin in situ; and mixing the resin with a non-essential blend resin, a non-essential curing agent, a non-essential solvent, a non-essential pigment and filler and a non-essential aid, and carrying out physical blending, amino epoxy addition reaction, Michael addition reaction and the like to form a film, thereby obtaining the graphene / polysiloxane composite coating material. The uniformly dispersed graphene lamellae and polysiloxane have strong interface effects, also have the gas / liquid barrier and heat shielding effects, and endow the coating with excellent corrosion resistance, flame retardancy and the like, thereby greatly enhancing the mechanical properties, corrosion resistance, scratch resistance, wear resistance and the like of the coating.

The invention relates to a preparation method of a terminated-type cation water-borne polyurethane color fixing agent, belonging to the field of organic adhesives. The terminated-type cation water-borne polyurethane color fixing agent with solid content of 20-40% of and transparent or translucent yellowish appearance can be prepared by the following steps of: (1) polyurethane prepolymer reaction, (2) terminated reaction, and (3) acid neutralization and ionization reactions. In the invention, partial terminating after prepolymerization is adopted, a small number of isocyanate groups is inactivated and a self-emulsifying method is adopted to synthesize the water-borne polyurethane color fixing agent; in the color fixing process, closed active groups are released through baking at high temperature and are carried out crosslinking reaction with hydroxyl and amino groups on textile fabrics and reactive dyes so that the color fastness to washing of the textile fabric is improved.

The invention discloses a silicon chip shallow trench isolation etching method which is used for etch groove on silicon. The method comprises the following steps: A. upper layer silicon etching step; B. oxide layer etching step, which is used for etching the oxide layer between upper layer silicon and base silicon and is also used for etching partial base silicon for the top fillet etching preparation; C. base silicon etching step which is used for etching groove on silicon base and to form slippery top fillet at the junctional position of oxide layer and silicon base on the sidewall of groove. The etching process gas used in the Step B is mixed gas consisting of HBr gas and CHF3 gas. The etching process gas is ionized into active groups like Br*, CHF*, etc., and can form the top fillet during Step C. The method has the advantages of simple process with less steps, low cost and slippery top fillet formation of etching groove, and is applicable to shallow trench isolation etching and other etchings of various type of semiconductor silicon wafers.

The invention relates to a surface hydrophilic modification method for a polytetrafluoroethylene bulked membrane, which is characterized by comprising the steps of: pretreating a polytetrafluoroethylene membrane by adopting low-pressure glow discharge plasma to make the surface of the polytetrafluoroethylene membrane generate active groups, and grafting acrylic acid to form a relatively stable hydrophilic layer. The method has the advantages that: the active groups are generated on the surface of the polytetrafluoroethylene membrane by low-pressure plasma treatment, and the relatively stable hydrophilic layer can be formed on the surface of the membrane by acrylic acid grafting treatment, so that the hydrophilicity of the polytetrafluoroethylene membrane is effectively improved, and the effect is lasting; and the polytetrafluoroethylene membrane is treated by the low-pressure plasma induction and acrylic acid grafting, so the treatment method is simple, high-efficiency, water and energy-saving, and suitable for industrialized production.

The invention relates to a functional resin tectorial membrane proppant and a preparation method thereof, and belongs to the technical field of oil-gas field development. The functional resin tectorial membrane proppant comprises aggregate and a resin film coated on the aggregate. Said resin film comprises organic silicon compounds of one or more active groups of amino, hydroxyl, carboxyl, alkoxyl and hydrosulphonyl. The side chain of the organic silicon compound is a hydrophobic group. The cured resin film has different wetting qualities for oil and water. The functional resin tectorial membrane proppant of the invention has a function of allowing the smooth permeation of oil gas and preventing water from penetrating through the proppant. Such a function improves the separation effect ofoil gas and water and reduces the oil production cost. The excellent hydrophobicity of the resin film facilitates the proppant to have excellent water resisting property and improves the crushing resistance of the proppant, so that the stream guidance effect is good for a long time.

The invention provides a high-scratch-resistance abrasion-resistant coating material and a preparation method thereof. The preparation method comprises the following steps: modifying the graphene surface by using active groups by a chemical modification technique to obtain modified graphene, and blending the modified graphene with polysiloxane to obtain the high-scratch-resistance abrasion-resistant nano composite coating material. The surface modification is carried out to enhance the dispersity of the graphene and the interactions between the graphene and polysiloxane matrix, thereby enhancing the mechanical properties of the coating. No pigment or filler is added. The scratch resistance of the transparent graphene / polysiloxane composite coating is enhanced by 140% or above, and the abrasion loss is reduced by 60% or above. The transparent graphene / polysiloxane composite coating has excellent adhesion, heat resistance, weather resistance, flame retardancy and corrosion resistance. The graphene / polysiloxane composite coating can be used for surface protection and shielding of various metals, plastics, wood, concrete, glass and other substrates, and is applicable to the fields of automobile paints, photoelectric materials, precision instruments, marine heavy-corrosion protection, buildings and the like.

A water-soluble photo-activatable polymer including: a photo-activatable group adapted to be activated by an irradiation source and to form a covalent bond between the water-soluble photo-activatable polymer and a matrix having at least one carbon; a reactive group adapted to covalently react with a biomaterial for subsequent delivery of the biomaterial to a cell; a hydrophilic group; and a polymer precursor. A composition including a monomolecular layer of the water-soluble photo-activatable polymer and a matrix having at least one carbon, wherein the monomolecular layer is covalently attached to the matrix by a covalent bond between the photo-activatable group and the at least one carbon. The composition further includes a biomaterial having a plurality of active groups, wherein the biomaterial is covalently attached to the monomolecular layer by covalent bonding between the active groups and reactive groups. Also provided is a method for delivery of a biomaterial to a cell.

The invention relates to a dopamine surface-modified two-dimensional nanometer material and a preparation method. A two-dimensional nanometer material wrapped with polydopamine is prepared through a one-step reaction. The invention solves the problem of poor dispersion of traditional two-dimensional nanometer materials in interstitium (water, organic matter). This characteristic preparation method provides a method for modifying the surface of two-dimensional nanomaterials with dopamine. After the surface of two-dimensional nanomaterials is modified by dopamine, functional groups (hydroxyl and amino groups) are successfully introduced. Compatibility between matter and two-dimensional nanomaterials. Therefore, this invention has great scientific significance, and has great practical application value in the production of friction-resistant composite materials, lubricating grease, and heat-conducting composite materials.

The invention discloses a method for directly growing graphine on various substrates. The method comprises the following steps: A) putting a substrate material in a plasma enhanced chemical vapor deposition (PECVD) cavity, vacuuming, heating the substrate to 400-600 DEG C, introducing hydrocarbon gases and other noble gases, and controlling the pressure of the gases to be at most 1Torr; and B) switching on a plasma power supply so that the hydrocarbon is ionized and cracked to active groups, and reacting on the substrate surface of 400-600 DEG C, thereby achieving the direct growth of the graphine. By the method in the invention, the problem that high-quality graphine is directly grown on the surface of a non-specific substrate is solved; and the method in the invention has an important sense at the aspects of exploring a large-area direct growth technology of graphine, understanding a growth mechanism of graphine, researching a fundamental physical problem of graphine, exploring practical applications of graphine films and broadening application ranges of graphine.

The invention discloses a magnetic carbon nanotube composite material and a preparation method and an application thereof. The preparation method comprises the following steps: adding FeCl3.6H2O to an ethylene glycol solution; then adding anhydrous sodium acetate and polyethylene glycol; adding a carboxylated multiwalled carbon nanotube; performing ultrasonic dispersion; adding hexamethylenediamine or ethanediamine; heating to 200-300 DEG C for reaction for 8-24h; and washing and performing vacuum drying to prepare the amino-modified magnetic Fe3O4-carbon nanotube composite material. The amino-modified magnetic Fe3O4-carbon nanotube composite material prepared by the invention is of nanoscale and superparamagnetism, can be stably dispersed in solutions, and can be quickly separated and enriched through a simple action of a magnetic field. As an adsorbent, the material is large in superficial area and has various active groups on the surface. The material can adsorb pigments from complex substrates through pi-pi electron interaction and hydrophobic effect of the carbon nanotube and can adsorb compounds such as organic acids and phenols through weak anion exchange effect of amino groups on the surfaces of magnetic nanoparticles.

Compounds are disclosed having the general formula R1—X—R2, wherein R1 and R2 are biologically active groups, at least one of which is polypeptidic. X is a non-peptidic polymeric group. R1 and R2 may be the same or different. Preferred R1 and R2 groups are interleukin-1 receptor antagonist, 30 kDa TNF inhibitor, interleukin-2 receptors and CR1 and muteins thereof. Also included are site selectively modified interleukin-1 receptor antagonist and 30 kDa TNF inhibitor.

This invention achieves data capacity efficiency via data de-duplication and maximizes a power-saving effect by disk operation control. In a storage system, when data is received from a computer, a value representing the bit string for the data is calculated and whether or not a value identical to the calculated value is stored in a data management table is judged. If it is judged that an identical value is not stored, the received data is registered in the data management table and stored, based on a group management table, in disk device(s) associated with a logical unit number of a logical unit constituting an active group. Meanwhile, if it is judged that an identical value is stored, the received data is stored in disk device(s) based on the group information managed in the group management table and the management information managed in the data management table.

Disclosed are general and “substantially pure” branched discrete polyethylene glycol constructs useful in attaching to a variety of biologically active groups, for example, preferential locators, as well as biologics like enzymes, for use in diagnostics, e.g. imaging, therapeutics, theranostics, and moieties specific for other applications. In its simplest intermediate state, a branched discrete polyethylene glycol construct is terminated at one end by a chemically reactive moiety, “A”, a group that is reactive with a biologic material that creates “A”, which is a biologically reactive group, connected through to a branched core (BC) which has attached at least two dPEG-containing chains, indicated by the solid line, , having terminal groups, which can be charged, non-reactive or reactable moieties and containing between about 2 and 64 dPEG residues.

The invention relates to a modified cotton fiber manufacturing method. It belongs to textile fiber material modification technique. It includes the following steps: boiling-off twisted cotton yarn and bleaching; processing selective oxidation reaction by putting the cotton yarn into periodate with 0.1-3g / L concentration at 30-60 centigrade degree for 1-2h; removing the oxidant; washing; dehydrating; drying; gaining oxidation cotton fiber with less than 25% strength stretch ratio; using the matter with -NH2, -OH active group to graft and cross link. Thus the cotton fiber is modified to gain multifunction composite cotton fiber. It can increase its wearability and addition value, expand application area, and solve the cotton fiber function in textile fiber material field.

A software method and computer system using said method are disclosed for efficiently reallocating unused system resources in a system in which unused system resources are initially allocated among groups that may become active or inactive. The method reallocates unused resources among active groups by scaling up these groups' initial entitlement shares, subject to maximum caps that may apply. For each group, the method calculates a scaling ratio equal to the cap divided by the entitlement, and then sorts the groups according their scaling ratios. The method processes each group in increasing order of their scaling ratios and reaches a maximal share of system resources to be allotted to each group, where the maximal share for an active group is between, or equal to, the group's initial entitlement value and its cap. Inactive groups have maximal shares equal to zero, reflecting that they receive no system resources. As the method processes the groups, it attempts to simply scale each active group by its scaling ratio. If scaling all unprocessed groups by the current group's scaling ratio would exceed the unallocated resources, then the remaining groups are scaled by the remaining resources divided by the sum of the entitlements of the remaining groups. Because the groups are sorted in order of increasing scaling ratios, the remaining active groups may be scaled as described without exceeding their caps.

The invention provides a fluorin-containing POSS acrylate polymer. The fluorin-containing POSS acrylate segmented polymer resin has a structure shown by M'-M-M', wherein the M' is a fluorin-containing acrylate structure unit; and M is an irregular polymerization unit containing active group acrylate and POSS acrylate, and the fluorin-containing POSS is fluorin-containing polyhedral oligomeric silsesquioxane. The invention also provides a method for preparing the fluorin-containg POSS acrylate polymer and a paint containing the fluorin-containing POSS acrylate polymer. The preparation method adopts the POSS acrylate monomer with lower cost and fluorin-containing acrylate monomers to prepare the fluorin-containing POSS acrylate polymer with fluorin-containing acrylate structure units distributed on the two ends of the polymer by controlling the adding sequence of the fluorin-containing acrylate monomers, and has the advantages of simple process and low cost; and the prepared paint has low surface energy and high fouling resistance.