120results about How to "Simple growth process" patented technology

A novel method for growing semiconductor material including GaN is disclosed. The method involves placing a first substance into a growth reactor, supplying a second gaseous substance into the grouth reactor, and applying electrical field to the second gaseous substance to produce the cry stalline compound material.

The invention discloses a graphene sapphire substrate suitable for epitaxial growth of III-nitride. A preparation method of the substrate comprises the following steps of performing graphene chemicalvapor deposition on the sapphire substrate; performing plasma treatment on a system after the chemical vapor deposition, wherein the plasma treatment process specifically comprises oxygen plasma treatment, nitrogen plasma treatment or argon plasma treatment. The preparation method has the advantages that an III-nitride thin film can be quickly and efficiently prepared, and the preparation cost ofthe III-nitride thin film is greatly reduced; the obtained III-nitride can be further processed into LED (light emitting diode) devices, and the problem of overheat in a use process can be solved forthe prepared LED chip because of very good heat conductivity of the graphene.

The invention belongs to the field of crystal preparation, and in particular relates to a device for preparing aluminum nitride crystals and a corresponding process. The invention provides the device and the process for preparing aluminum nitride crystals by adopting a spontaneous crystal seed method. The device comprises an inductive heating coil, an insulating layer, a crucible device and a crucible lifting device. The crucible device consists of a crucible body, a crucible cover and a cover sheet. A hole which is 1-2mm in diameter is formed in the crucible cover, the cover sheet is located above the crucible cover and completely shields the hole, and the area of the cover sheet is between those of the hole and the crucible cover. The preparation process comprises the two steps of: (1) obtaining aluminum nitride single crystals through spontaneous crystallization at the hole to be used as the crystal seeds due to limit of anisotropic crystalline characteristic of aluminum nitride and geometric dimension of the hole at lower temperature; and (2) obtaining large-dimensional aluminum nitride crystals by weakening the anisotropic crystalline characteristic of aluminum nitride at high temperature and meanwhile slowly adjusting the position of the crucible by lifting through the lifting device.

The invention discloses a high-quality AlN thin film epitaxially grown on a Si substrate, and a preparation method of the high-quality AlN thin film. The preparation method specifically comprises the following steps of 1) choosing the Si substrate; 2) pre-paving an Al layer in an epitaxial manner; 3) enabling an AlN core-forming layer to be grown; and 4) enabling the AlN thin film to be grown, wherein in the growth process of the AlN thin film, trimethyl gallium is introduced at a speed of 0.2-0.5mL/min to be used as a surfactant. By adoption of the preparation method, the relatively thick and crack-free AlN thin film with a thickness which is greater than 1[mu]m can be manufactured; inter-island union and two-dimensional growth of the AlN thin film are realized; compared with a multi-step multi-layered or high-temperature AlN thin film growth technology, the time consumption for preparing the thin film by the method provided by the invention can be shortened; the growth process is unique, simple and feasible; the large-scale production can be realized conveniently; and the thin film can be widely applied to the fields of a photovoltaic thin film for an LED, an ultraviolet and deep ultraviolet device, a surface acoustic wave device and the like.

The invention relates to a double doped layer silicon-based film solar cell. In a p type doped layer and an n type doped layer, the optical band gap of the layer closely adjacent to an intrinsic layer is larger than that of the layer far away from the intrinsic layer, but the difference value of the band gaps is not larger than 0.45 eV. The difference of the optical band gaps of the double doped layer structure is realized by arranging different materials according to the matching principle, or by changing the growth technology parameter of the identical material to control the optical band gaps. According to the invention, the inhibition to the particle interaction at the interface between the doped layers and the intrinsic layer and the control to the dopant particles and the accumulation and the distribution of defects can be realized simultaneously, excessive defects in the intrinsic layer can be reduced, simultaneously, the initial photoelectric conversion efficiency and the irradiation stability of the solar cell can be improved, the production cost for the silicon-based film solar cells can be further reduced, therefore, the structure can be applied to any silicon-based single-junction solar cell, laminated solar cell and multi-junction solar cell with p-i-n structure and n-i-p structure.

The invention relates to a preparation method of a silica-based CdZnTe thin film ultraviolet light detector, which belongs to the technical field of ultraviolet light detector light-sensitive material and device manufacturing process. A near-space sublimation method is adopted, an N-type CdZnTe thin film is prepared on a P-type Si substrate, an ultraviolet light detector with a CdZnTe thin film/Si heterogeneous structure is formed, and a new method is provided for manufacturing the ultraviolet light detector with high performance. The invention relates to the silicon substrate-based heterojunction CdZnTe thin film ultraviolet light detector, which is characterized in that a CdZnTe thin film sample with high smoothness, uniform particle size and high quality is prepared on a Si chip by adopting the near-space sublimation method, and the prepared heterojunction detector has high sensitivity.

The invention discloses a zinc selenide single crystal growing method and a zinc selenide single crystal growing container. The method uses zinc and selenium as raw materials and iodine as a vapour phase reaction promoter, and further completes the growth of a zinc selenide single crystal in an ampoule. The method sequentially comprises the following steps: comprehensively cleaning the ampoule, feeding the materials into the ampoule and evacuating the ampoule, sealing the ampoule, cleaning a growing area of the sealed ampoule with hot water, growing crystals, cooling the crystals, and the like. The ampoule has the basic structure that: a raw material area is easy to mix Zn and Se elementary substances; and the growing area consists of a conical body formed by the tangency of two sections of arcs on the cross section of a middle axis of the ampoule. The technical scheme adopted by the invention can grow zinc selenide single crystals of a diameter of 12 to 20mm, and also can be applied to the preparation of other II-VI group compound semiconductor crystals. The grown zinc selenide single crystals have the characteristics of integral structure, good uniformity, small stress, low cost,and simple process.

The invention discloses a flat type InGaAs infrared focal plane device, which includes a flat type PN junction formed by Zn diffusion on an epitaxial wafer. The invention is characterized in that: a thickened Cr/Au ring electrode is positioned around the upper part of the Zn diffusion area and the limitation on a photosensor element is realized by the Au layer reflection of incident lights. The shape of the thickened electrode is decided by a photoetching graph, so the effective photosensor element area can be controlled precisely. The preparation method of the device is characterized in that: before heat treatment, generate SiO2 passive film to prevent Zn from out diffusion in the heat treatment course, improve PN junction thermal stability, and realize device surface passivation and light antireflection by controlling the thickness of SiO2 film. p electrode adopts single Au layer, which simplifies p electrode growth process and is important to process stability and device evenness. The Au and the InP have better adhesiveness. And the thermal annealing course under the protection of SiO2 layer can realize good ohmic contact with Au/Zn/Au.

The invention discloses a self-separation method for preparing a self-supporting GaN substrate, which includes steps of: 1) on a sapphire substrate, growing a uniformly-distributed Ga2O3 film, whereinthickness range of the film is 0.1-1 [mu]m; 2) in an ammonia atmosphere, performing complete nitridation to the film, thus forming a porous GaN film in latticed distribution; 3) on the porous GaN film, performing halide vapor phase epitaxy growth of a GaN thick film, thus forming a low stress and high quality GaN thick film; 4) after the epitaxy is completed, cooling the material to room temperature, so that the epitaxy GaN thick film is automatically separated from the sapphire substrate, thus obtaining the self-supporting GaN substrate.

The invention discloses a method for preparing a molybdenum sulfide two-dimensional material by adopting MOCVD (Metal Organic Chemical Vapor Deposition) equipment, and the method is used for growing the MoS2 two-dimensional material on a Sapphire substrate in multiple steps, and comprises the following steps of: adopting Sapphire as the substrate; conveying the Sapphire substrate into an MOCVD (Metal Organic Chemical Vapor Deposition) equipment; introduced N2 gas into a MOCVD cavity; raising the temperature to a constant-temperature growth temperature, wherein the initial pressure in the cavity is 90Torr; introducing H2S as a sulfur gas source; introducing MO (CO) 6 as a molybdenum gas source for nucleation; reducing the pressure intensity in the cavity step by step, and promoting nucleation crystal grains to transversely grow so as to obtain the MoS2 two-dimensional material growing on the Saphire substrate. The preparation method provided by the invention has the advantages of simplegrowth process, controllable material thickness, high quality and the like. Through the preparation method provided by the invention, the MoS2 two-dimensional material which is adjustable in forbidden band width and can be used for flexible chip application is grown.

The invention provides a preparation method of a lead-based organic-inorganic hybrid perovskite nanosheet, the lead-based organic-inorganic hybrid perovskite nanosheet is prepared by a two-step method, and comprises the following steps: 1, dripping supersaturated lead halide aqueous solution onto a substrate to prepare a lead halide substrate; and 2, heating an organic precursor to a gas phase state for fully contacting and reacting with the lead halide substrate to obtain a lead-based organic-inorganic hybrid perovskite nano sheet. In the gas phase method, hydrophobically modified piperazineis added to the organic precursor for treating lead halide. The wetting angle of the perovskite nanosheet increases obviously, which indicates that the water resistance of the perovskite nanosheet isimproved. Aging tests prove that perovskite can keep stable for a long time under high temperature and high humidity environment, and the perovskite can be prepared into a solar cell with good photoelectric efficiency. The lead-based organic-inorganic hybrid perovskite nanosheet provided by the preparation method has excellent comprehensive performance, can simultaneously have good photoelectric efficiency and stability, and has good market promotion prospects.

The invention provides a method and a device for preparing an Mg-doped ZnO nanowire array. The method comprises the following steps of: dissolving zinc acetate in 5 to 8 mass percent aqueous solution of polyvinyl alcohol (PVA) to prepare crystal seed solution with the zinc ion concentration of 0.001 to 0.1mol/L; coating the crystal seed solution on a substrate and drying to ensure that the coating material of the substrate is the PVA and the zinc acetate; performing heat treatment to ensure that the coating material of the substrate is zinc oxide; preparing 0.012 to 0.1mol/L standard aqueous solution of magnesium salt; adding the standard aqueous solution, zinc nitrate and hexamethylenetetramine into deionized water to prepare growth solution with the total metal cation concentration of 0.01 to 0.04mol/L; and suspending the substrate subjected to heat treatment in the growth solution, and growing in an 85 to 95 DEG C constant-temperature water bath for more than 2 hours to obtain the nanowire array. Therefore, the Mg-doped ZnO nanowire array can be grown at a low temperature, the cost of the used raw materials is low, and the production process is simple and has high repeatability.

An electro-optic semiconductor device comprising a semiconductor waveguide with a core region within which is located at least one active area wherein the core of the waveguide outside of the one or more active areas are not contaminated by diffuse active area material and the one or more active area(s) and the waveguide are monolithic and are grown in an additive growth process. Also provided is a method of making an electro-optic semiconductor device, comprising the steps of; growing a first part of a core layer of a semiconductor waveguide, selectively growing an active layer over a partial area of the first part of the core layer, and growing a second part of the core layer of the semiconductor waveguide over the first part and the active layer, characterised in that the method comprises an additive growth process.

The invention discloses an InGaN/GaN multi-quantum well grown on a ScMgAlO4 substrate. The InGaN/GaN multi-quantum well comprises a first GaN buffer layer, an amorphous AlN insertion layer, a second GaN buffer layer and an InGaN/GaN quantum well which are sequentially grown on the ScMgAlO4 substrate. The invention also discloses a preparation method of the InGaN/GaN multi-quantum well grown on the ScMgAlO4 substrate. The InGaN/GaN multi-quantum well has the advantages of simple growth process and low preparation cost, and moreover, the prepared InGaN/GaN multi-quantum well is low in defect density, good in crystal quality and excellent in luminous performance.

The invention discloses a preparation method of tantalump-doped potassium-sodium niobate lead-free piezoelectric single crystal with a high electromechanical coupling property, relates to a preparation method of potassium-sodium niobate base lead-free piezoelectric single crystal, and aims to solve the problems that the conventional potassium-sodium niobate base lead-free piezoelectric single crystal is hard to grow, small in size and low in electromechanical coupling coefficient. The chemical formula of the tantalump-doped potassium-sodium niobate lead-free piezoelectric single crystal with the high electromechanical coupling property is (K1-xNax)(Nb1-yTay)O3, wherein x is greater than 0.4 and less than 0.7, and y is greater than 0.20 and less than 0.35. The preparation method particularly comprises the following steps: step one, pre-sintering so as to synthesize a polycrystal powder raw material; step two, putting the polycrystal powder raw material into a single crystal pull furnace so as to carry out single crystal growth; step three, cooling and annealing by using a multi-step cooling method. The preparation method has the advantages that firstly, the growth process is simple and low in cost, secondly, the prepared tantalump-doped potassium-sodium niobate single crystal is large in size and good in quality, and thirdly, the high electromechanical coupling property is achieved. By utilizing the preparation method, a piezoelectric material with the high electromechanical coupling property is prepared.

The invention belongs to the field of microelectronic technology, particularly relates to a method for preparing a zinc oxide (ZnO)-based thin film transistor (TFT) by using organic chemical vapor deposition (MOCVD). The ZnO-based thin film transistor consists of a lining, a grid, an insulating layer, a ZnO based active channel layer, a source electrode and a drain electrode, wherein the insulating layer and the ZnO based active channel layer both adopt the MOCVD technology to finish the growth of materials, and compared with other extension technologies, the MOCVD technology has the advantage that a prepared semiconductor material has higher quality. The growth of material in all layers is finished in one step in MOCVD growth equipment, thereby the material growth process is greatly simplified, and the thickness of each layer of semiconductor material can be accurately controlled. The invention provides the process method for growing the ZnO-based TFT by adopting the MOCVD growth equipment suitable for industrial production, solves the key problems that the prepared ZnO-based TFT has low quality by using other methods, and the like, and prepares the ZnO-based TFT with higher quality.

The invention discloses a GaN film growing on a magnesium aluminate scandium substrate. The GaN film comprises a GaN buffer layer, a GaN nucleation layer, a GaN amorphous layer and a GaN film which sequentially grow on an ScMgAlO4 substrate, wherein a (0001) surface, which deviates from a (11-20) surface by 0.5-1 degrees, of the ScMgAlO4 substrate is an extension surface. The invention fuehrer discloses a preparation method and application of the GaN film. Compared with the prior art, the preparation method has the advantages that the growing process is simple, and the preparation cost is low; and meanwhile, by utilizing an amorphous layer technique, the GaN film prepared by virtue of the preparation method has the characteristics of good crystalline quality, low defect density and the like.