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97 results about "Ion bombardment" patented technology

Ion bombardment. noun. Physics Chemistry. The fact of being struck by a beam of ions; specifically the process of bombarding a surface with ions (usually ions of an inert gas) as a means of removing impurities.

Electron gun and ion source collaborative evaporation coating method, control method and control system

The invention belongs to the technical field of vacuum coating, and relates to an electron gun and ion source collaborative evaporation coating method, a control method and a control system. The electronic gun and ion source collaborative evaporation coating control method comprises the steps that key parameters in the coating process are continuously collected, and an electronic gun beam initial value and an ion source gas flow initial value are dynamically generated according to state diagnosis results of all the parameters; the beam current value of the electron gun and the gas flow value of the ion source are corrected in real time to inhibit the disturbance of the ion source to the beam current of the electron gun, and the electron gun and the ion source are cooperatively regulated and controlled to ensure the precise control of the coating uniformity; the invention further discloses an electron gun and ion source collaborative evaporation coating method, local hot spot compensation and global uniformity compensation are carried out by adopting a film thickness compensation mechanism so as to accurately control the film thickness. According to the invention, the cooperative control of the electron gun evaporation and ion bombardment process is realized, the film adhesion is enhanced, the evaporation coating rate is improved, and the film thickness uniformity is improved.
Owner:CHENGLIAN KAIDA TECH CO LTD

Method for ion-assisted self-limiting conformal etching

A method for forming a semiconductor device provides a substrate having a patterned structure containing a semiconductor material, wherein the patterned structure has a side profile including depressions, such as a patterned film stack, and a spacer layer conformally deposited on and within the depressions of the patterned structure; and a reaction layer formed on the spacer layer by reacting the surface of the spacer layer with a plasma-excited first etching gas, wherein the plasma-excited first etching gas contains fluorine, hydrogen, and nitrogen to form the reaction layer, and at least a portion of the reaction layer is removed by ion bombardment caused by exposure to a plasma-excited second etching gas. The spacer layer may be SiOCN. The reaction layer may be ammonium silicofluoride. The first etching gas may contain SF6, H2, and N2, or NF3, H2, and N2. The reaction and removal may be carried out at room temperature in the same chamber.
Owner:TOKYO ELECTRON LTD +1

VUV lamp ionization source device with efficient heat dissipation capability

The invention relates to the technical field of analysis instrument ionization sources, in particular to a VUV lamp ionization source device with efficient heat dissipation capacity. The device comprises a VUV lamp, a heat dissipation unit, a VUV lamp driving electrode, a driving circuit and an ion guide focusing unit. The heat dissipation unit carries out cooperative heat dissipation on the VUV lamp and the pulse transformer through a fan, and the problems of signal attenuation and device aging caused by temperature rise are solved. The driving electrode adopts a pairwise pairing structure of upper and lower and left and right electrode pairs to form an inclined electric field to prevent ions from bombarding the lamp wall and the light window; the drive circuit is a half-bridge or full-bridge topology, can adjust the pulse frequency and the power supply voltage, and achieves the switching between a high-voltage low-frequency mode and a low-voltage high-frequency mode. The ion guide focusing unit efficiently leads out and separates ions through cooperation of a conical focusing electric field and a conductive film forward electric field. Through four-dimensional innovation of heat dissipation, electrodes, driving and transmission, the stability, the service life and the detection sensitivity of the device are improved, and the device is suitable for analytical instruments such as ion mobility spectrometry and mass spectrometry.
Owner:DALIAN INSTITUTE OF CHEMICAL PHYSICS CHINESE ACADEMY OF SCIENCES +1

Preparation method of high-entropy nitride anti-erosion coating

The invention provides a preparation method of a high-entropy nitride anti-erosion coating, which comprises the following steps: (1) polishing, cleaning and drying a sample in sequence, placing the sample in a vacuum coating chamber, introducing argon Ar, adjusting the flow of the argon Ar, and carrying out ion bombardment cleaning on the surface of the sample; (2) acquiring the optical emission intensity of the plasma after argon Ar is introduced and the optical emission intensity of the plasma after nitrogen N2 is introduced; (3) depositing a high-entropy alloy transition layer on the surface of the sample; (4) depositing a high-entropy nitride anti-erosion coating on the surface of the sample; and (5) taking out the sample to complete preparation of the coating on the surface of the sample. The preparation of the high-entropy nitride anti-erosion coating is completed by adopting a bipolar high-power pulse magnetron sputtering technology and an ion source to jointly construct a high-density plasma film forming environment, so that the nitridation reaction on the surface of the target material can be effectively inhibited, and the characteristic peak intensity of the plasma is kept unchanged; and the stability of plasma components in the film forming process is ensured.
Owner:INST OF MECHANICS CHINESE ACAD OF SCI

Ion thruster acceleration grid probability life evaluation method based on coupling competitive failure

The invention specifically discloses an ion thruster acceleration grid probability life evaluation method based on coupling competitive failure, and relates to the technical field of aerospace propulsion system life evaluation. The method comprises the following steps: firstly, obtaining deterministic parameters and random parameters of a thruster acceleration grid assembly; then based on an ion sputtering corrosion theory, considering material loss caused by charge exchange ion bombardment of the acceleration gate, and establishing a coupling corrosion model of the thickness and aperture of the acceleration gate; thirdly, constructing a competitive failure model, and realizing numerical solution of competitive failure life by dynamically iterating a corrosion state and a failure criterion; and finally, independently repeated random sampling is carried out based on probability distribution of random parameters, the random sampling is substituted into the competitive failure model to obtain an acceleration grid simulation life sample set, and statistical analysis is carried out on the life sample set to obtain a probability life evaluation result. The method solves the problem of errors caused by independent modeling of structural failure and electronic reflux failure in the prior art, and is helpful for reducing the system operation risk and improving the reliability of a spacecraft.
Owner:SICHUAN UNIV

Contact pole gap extra ventilation type hollow cathode

The invention discloses a contact pole gap additional ventilation type hollow cathode, which belongs to the technical field of spaceflight propulsion, and comprises a cathode assembly and a contact pole assembly, and the core is improved as follows: the contact pole assembly consists of a porous contact pole tube, a gas distributor and a contact pole ventilation ring which are mutually nested to form an independent gas supply system; after being subjected to pressure equalizing by the gas distributor and rectification by the contact pole ventilation ring, a working medium is uniformly injected into an annular gap between the contact pole and the cathode tube through circumferential ventilation holes of the contact pole tube with holes. The downstream gas density of the throttling hole is remarkably improved, discharge oscillation and ion bombardment corrosion are restrained, the gas supplementing amount can be dynamically adjusted and controlled, and the device is suitable for different working conditions. The cathode is simple and reliable in structure, highly compatible with an existing cathode, capable of prolonging the service life of the cathode and widening the stable operation interval, and suitable for long-service-life aerospace tasks of various electric propulsion systems.
Owner:BEIJING INST OF TECH

A SiCf / SiC composite material with ultra-high temperature ceramic gradient coating, its preparation method and application

This invention discloses a SiC with an ultra-high temperature ceramic gradient coating. f / SiC composite materials, their preparation methods, and applications. A double-layer glow discharge plasma surface metallurgical method is used to prepare SiC composite materials. f A (Hf,Si,Ta)C gradient composite coating was prepared on the surface of the SiC composite material. This coating was able to resist SiC in an oxygen atmosphere at 1773 K. f Effective protection of SiC composite materials. The specific advantages of this invention are: (1) Ion bombardment of the substrate significantly improves the point defects and conductivity of the composite substrate; (2) The (Hf,Si,Ta)C coating has a continuous gradient structure, forming a good metallurgical bond between the coating and the substrate, with high bonding strength; (3) The similar thermal expansion coefficients of the (Hf,Si,Ta)C coating and the substrate can improve the thermal mismatch between the coating and the substrate, reducing the tendency for coating peeling and cracking during service; (4) The (Hf,Si,Ta)C coating system has a high service temperature and self-healing ability. The coating prepared by this invention has excellent high-temperature protection performance, improving the protection of SiC. f The high-temperature service life of SiC composite materials has broad application prospects in the aerospace field.
Owner:NANJING UNIV OF AERONAUTICS & ASTRONAUTICS +1

Quick molding process for valve core and valve sleeve of servo valve without match grinding

The invention discloses a match-grinding-free quick forming process for a valve element and a valve sleeve of a servo valve, and relates to the technical field of servo valve machining and forming. Step 2, material inspection; step 3, surface treatment; step 4, ultrasonic cleaning; step 5, clamping the part; step 6, vacuumizing; seventhly, argon ion bombardment cleaning is conducted; 8, depositing a chromium base layer; 9, depositing a gradient chromium carbide transition layer; 10, depositing a hydrogenated diamond-like carbon top layer; and eleventhly, cooling and discharging are conducted. According to the match-grinding-free quick forming process for the valve element and the valve sleeve of the servo valve, the machining period of a sliding valve assembly can be shortened by 30%, the material cost is reduced by 80%, and the interchangeability of the valve sleeve and the valve element in the sliding valve assembly is achieved.
Owner:SHANGHAI HENGTUO HYDRAULIC CONTROL TECH

A coating that does not form acicular phases at the interface with nickel-based alloys and a method for producing it

The present application relates to high temperature protective coating technical field, specifically to a coating which does not form needle-shaped phase with nickel-based alloy interface and a preparation method. The coating is composed of carbon interstitial nickel-based, cobalt-based or nickel-cobalt-based alloy and dispersed nano-carbide particles; the preparation method is prepared by regulating vacuum cathode arc plasma in-situ reaction, and the preparation steps include: ① the substrate is subjected to conventional grinding, polishing and oil removal pretreatment, ② the alloy target material is installed, vacuum is drawn and the substrate is subjected to ion sputtering cleaning, ③ the vacuum arc plasma with the coating target material as the cathode is ignited, ④ the workpiece surface is bombarded and activated by cation with energy of 300eV-1000eV, ⑤ the coating is formed on the workpiece surface by depositing the gas containing carbon elements through plasma activation reaction by regulating the partial pressure. The coating can avoid the precipitation of needle-shaped harmful phase at the interface with nickel-based high-temperature alloy, and the method has the advantages of simple and controllable process, suitable for batch preparation and the like.
Owner:INST OF METAL RESEARCH - CHINESE ACAD OF SCI

Method for coating film in hole of ceramic substrate

The invention relates to a method for coating a film in a hole of a ceramic substrate, which is characterized by comprising the following steps of: assembling the ceramic substrate on a conductive clamp, assembling the conductive clamp on a rotating stand in a film coating chamber, connecting the rotating stand with a high-frequency power supply, exhausting air in the film coating chamber, and starting a heating system to bake the film coating chamber. Starting an ion beam cleaning power supply and a bias power supply, and carrying out ion beam cleaning treatment on the surface of the substrate; cleaning the surfaces of the titanium target material and the copper target material; preparing a bottom layer on the surface of the substrate by using a titanium target; preparing a transition layer on the base layer by using a titanium target material and a copper target material; and preparing a copper sputtering layer on the transition layer by using a copper target material. According to the technical scheme provided by the invention, argon ion bombardment cleaning and titanium layer bottoming, transition layer and copper sputtering layer preparation are sequentially carried out on the ceramic substrate. Copper plating is carried out in a high-vacuum high-temperature environment, titanium is adopted for bottoming to improve the binding force, and a high-frequency power supply is adopted for applying bias voltage to the surface of a workpiece, so that a film layer in a hole is uniform.
Owner:ANHUI CHUNYUAN COATING TECH CO LTD

Preparation method and application of micro-pit with polycarbonate as base material

The invention belongs to the technical field of material preparation, and particularly relates to a preparation method and application of a micro-pit with polycarbonate as a base material. The method provided by the invention mainly comprises the following steps: accelerating heavy ions by using an accelerator, bombarding a base material by using the accelerated heavy ions, and after the heavy ions damage polycarbonate, etching the polycarbonate by using an etching agent added with a corrosion inhibitor to obtain micro-pits with specific diameters and depths, and cleaning and drying the etched sample. The preparation of the micro-pit is realized by accelerating impact of the polycarbonate with heavy ions, the method breaks through the limitation of the traditional photoetching technology, the pattern of the micro-pit is directly defined through heavy ion bombardment, a mask is not needed, the material cost is reduced, production interruption and extra cost caused by damage of the mask are also avoided, and the production efficiency is improved. And the processing process is relatively simple, multiple complex photoetching and etching steps are not needed, the production efficiency is greatly improved, the production period is shortened, and the production cost is reduced.
Owner:RUICHANG INST OF APPLIED NUCLEAR PHYSICS +1

Method for horizontal gap filling in semiconductor manufacturing

Aspects of the present disclosure provide a method for filling a horizontal gap of a semiconductor structure. For example, the method can include providing a workpiece that includes a stack of alternating first layers and second layers that are parallel with each other. At least one of the second layers can be recessed with respect to vertical sidewalls of two neighboring first layers that sandwich the second layer. A horizontal gap can be formed between the recessed second layer and the two neighboring first layers. The method can further include depositing a gap-filling material to cover the sidewalls of the first layers and fill the horizontal gap, etching back a portion of the gap-filling material that is deposited on the sidewalls of the first layers in an ion bombardment process, and forming a gap filler that includes a remaining portion of the gap-filling material that fills the horizontal gap.
Owner:TOKYO ELECTRON LTD +1

Surface treatment method for valve plate base body and valve plate

The invention provides a surface treatment method for a valve plate base body and a valve plate. The method comprises the steps that a valve plate base body is subjected to polishing, ultrasonic cleaning and drying treatment; the cleaned valve plate is placed in a vacuum ion nitriding furnace to be subjected to nitriding treatment under the treatment conditions that a vacuum pump is started for air exhaust, after the pressure value in the furnace reaches a first specified value, high pressure is started, argon is introduced, the vacuum degree of a furnace cavity is kept at a second specified value, the surface layer starts to be heated through high-energy ion bombardment, and the surface layer is heated; after the temperature of the workpiece reaches 480-510 DEG C, nitrogen is introduced, the volume ratio of nitrogen to argon is set to be 1: 6, the air pressure is adjusted to 300-500 Pa, and heat preservation is conducted for 6-8 h; and the valve plate subjected to nitriding treatment is transferred to multi-arc ion plating equipment for coating deposition, and the treatment conditions of coating deposition are as follows: nitride is selected as a deposition material, the substrate temperature is kept at 450 DEG C in the deposition process, the target current is controlled to be 120-150 A, the vacuum degree is 2-3 Pa, and the deposition time is 60-90 min.
Owner:BEIJING RES INST OF AUTOMATION FOR MACHINERY IND

Nickel-based superalloy with surface subjected to ion nitriding and preparation method of nickel-based superalloy

The invention discloses a surface ion nitriding nickel-based superalloy and a preparation method thereof, and belongs to the field of metal material surface hardening treatment.The preparation method comprises the steps that the nickel-based superalloy is polished and cleaned; carrying out ion bombardment on the cleaned nickel-based high-temperature alloy in a hydrogen atmosphere; carrying out ion nitriding on the nickel-based high-temperature alloy subjected to ion bombardment in the atmosphere of nitrogen and hydrogen; and cooling the nickel-based high-temperature alloy after ion nitriding to below 100 DEG C along with the furnace, and discharging the nickel-based high-temperature alloy after surface ion nitriding to obtain the nickel-based high-temperature alloy after surface ion nitriding. According to the method, the surface of the nickel-based high-temperature alloy is bombarded by adopting high-energy ions before nitriding, so that a passivation layer, oil stains and other impurities on the surface of a workpiece can be removed at the same time, the problem that a passivation film hinders nitrogen permeation in the nitriding process is avoided, additional pretreatment is not needed, and the overall period is shortened; by optimizing the process parameters of ion nitriding, the time-consuming steps of slowly decomposing nitrogen atoms by depending on gases such as ammonia gas in atmosphere nitriding and then passively diffusing the nitrogen atoms are omitted, and the nitriding efficiency is greatly improved.
Owner:AVIC BEIJING INST OF AERONAUTICAL MATERIALS

Surface ion nitriding TiAl alloy and preparation method thereof

The invention discloses a surface ion nitriding TiAl alloy and a preparation method thereof, and belongs to the field of metal material surface hardening treatment.The preparation method comprises the steps that the TiAl alloy is polished and cleaned; the cleaned TiAl alloy is subjected to ion bombardment in the hydrogen atmosphere; the TiAl alloy subjected to ion bombardment is subjected to ion nitriding in the nitrogen atmosphere; and the TiAl alloy subjected to ion nitriding is cooled to 100 DEG C or below along with the furnace and discharged out of the furnace, and the TiAl alloy subjected to surface ion nitriding is obtained. According to the method, the surface of the TiAl alloy is bombarded by adopting high-energy ions before nitriding, impurities such as an oxidation film and oil dirt on the surface of a workpiece can be removed at the same time, the problem that the oxidation film hinders nitrogen permeation in the nitriding process is avoided, additional pretreatment is not needed, and the overall period is shortened; by optimizing the process parameters of ion nitriding, the time-consuming steps of slowly decomposing nitrogen atoms by depending on gases such as ammonia gas in atmosphere nitriding and then passively diffusing the nitrogen atoms are omitted, and the nitriding efficiency is greatly improved.
Owner:AVIC BEIJING INST OF AERONAUTICAL MATERIALS

Gear ring coating, preparation method and internal gear pump

The invention belongs to the technical field of mechanical part surface treatment, and relates to a gear ring coating, a preparation method and an internal gear pump. The invention provides a vacuum coating plating technology and a preparation method for an interface of a gear ring shell of an internal gear pump, the technology adopts a multilayer composite structure design, the multilayer composite structure design comprises a metal bottom layer, a nitride transition layer and a diamond-like carbon functional layer, and through material combination and structure optimization, the composite structure is prepared. And the wear resistance, the corrosion resistance and the bonding strength are synergistically improved. In the process aspect, the procedures of precise cleaning, ion bombardment activation, vacuum coating, low-temperature annealing and the like are adopted, parameters of all links are strictly controlled, and it is ensured that the coating quality is stable and reliable. The prepared coating is excellent in comprehensive performance, the problems of abrasion and corrosion under high-pressure and high-speed working conditions can be effectively solved, the service life of the gear pump is prolonged, and the maintenance cost is reduced.
Owner:CHENGLIAN KAIDA TECH CO LTD

An AlO x Preparation method of Al2O3 low-reflection etching-resistant composite coating

ActiveCN122061105BPulsed DCOxygen vacancy
An AlO x A method for preparing an Al2O3 low-reflection, etch-resistant composite coating includes the following steps: In a first chamber, the surface of a substrate is cleaned by ion bombardment; in a second chamber, argon and oxygen are introduced, and at least one layer of Al2O3 is deposited on the surface of the substrate using pulsed DC magnetron sputtering. x Layer; containing AlO x The substrate of the layer is fed into the third chamber, argon and oxygen are introduced, and AlO is sputtered using pulsed DC magnetron sputtering. x An Al2O3 layer is deposited on the surface of the layer and cooled in the furnace to obtain AlO. x - Al2O3 low-reflection, etching-resistant composite coating. This invention constructs a non-stoichiometric Al2O3 composite coating within the composite coating. x A gradient structure of oxygen content gradually transitioning from a layer to a dense Al2O3 layer, with low oxygen content AlO2O3. x The layer has a high oxygen vacancy concentration and low reflectivity, which can effectively reduce the reflection intensity in the ultraviolet-visible band. The dense Al2O3 layer formed on the surface has good structural stability and chemical inertness, thus significantly improving the etching resistance of the coating in the plasma etching environment.
Owner:SOUTH CHINA UNIV OF TECH +1

Systems and methods for multi-step directed patterning

The present disclosure relates to systems and methods for multi-step directed patterning. A semiconductor process system includes an ion source configured to bombard a photoresist structure on a wafer. The semiconductor process system reduces a width of the photoresist structure by bombarding the photoresist structure with ions in a plurality of different ion bombardment steps having different characteristics.
Owner:TAIWAN SEMICONDUCTOR MANUFACTURING CO LTD

Grid regulation type vertical structure micro-nano plasma triode

PendingCN121483943ASolid cathode detailsCold-cathode tubesInsulation layerIon bombardment
Aiming at the problem that the service life of a device is shortened due to electrode damage caused by ion bombardment, the invention provides a grid regulation and control type vertical structure micro-nano plasma triode which is of a vertical structure and comprises a substrate, a lower electrode, a grid, an upper electrode, a vertical insulating layer and a horizontal insulating layer. The lower electrodes are arranged above the substrate, the grid electrode is arranged above the lower electrodes, the horizontal insulating layers cover the upper layer and the lower layer of the grid electrode, the vertical insulating layers are distributed on the side edges of the grid electrode, the upper electrodes are arranged above the upper horizontal insulating layers, the edges of the upper electrodes are flush with the edges of the vertical insulating layers, and a vertical air channel is formed between the two upper electrodes. The grid electrode can effectively regulate and control ion and electron distribution in a channel, collision ionization is increased, micro-nano plasma formation is promoted, and the working voltage of the device is reduced. In addition, the grid electrode can regulate and control the electric field distribution in the vertical channel, change the ion motion trail, inhibit high-speed ions from directly bombarding the electrode, and prolong the service life of the device.
Owner:UNIV OF ELECTRONICS SCI & TECH OF CHINA

Lens surface treatment process

PendingCN121314879AVacuum evaporation coatingPretreated surfacesPolycarbonate plasticIon bombardment
The invention discloses a lens surface treatment process which sequentially comprises the following steps: carrying out injection molding on polycarbonate plastic to obtain a lens; coating a first optical organic silicon hardening coating on the surface of the lens; performing optical vacuum coating on the lens with the first coating to form a coating layer; carrying out ion bombardment cleaning on the coating layer by using inert gas under vacuum / high vacuum, removing pollutants and generating an activated microstructure so as to improve the adhesive force of a subsequent coating; coating a second optical organic silicon hardening coating on the surface of the bombarded coating layer; and cooling to room temperature to obtain a finished product. The process breaks through the bottleneck that an organic silicon coating cannot be secondarily coated after traditional film coating, a composite protection system is formed, the abrasion resistance and firmness of a lens film layer are remarkably improved, the film layer is prevented from being abraded and faded, the problem of electrostatic reaction of a film coating layer and an electrostatic protection film is solved, the process is suitable for helmet lenses, goggles and the like, and the process is stable and easy to industrialize.
Owner:陈国统 +1

Systems and methods for implementing atomic layer etching and radical enhanced deposition in a single chamber

This invention discloses a system and method for achieving atomic layer etching (ALE) and radical-enhanced deposition (REED) in a single chamber. The system features a switchable DC blocking capacitor for grounding an electrostatic chuck (ESC) to eliminate the plasma sheath, and employs high-power short-pulse RF to suppress ion bombardment during ALE surface modification and REED deposition steps, thereby achieving efficient processing and making it suitable for applications such as the fabrication of high aspect ratio structures.
Owner:SHANGHAI ATOMIC QIZHI SEMICONDUCTOR EQUIPMENT CO LTD

Plasma carburizing composite heat treatment equipment and process for thin metal plate

The invention discloses plasma carburizing composite heat treatment equipment and process for a thin metal plate. The heat treatment equipment comprises a furnace body, a heating electrode plate, a pressurizing mechanism, a micro-motion mechanism, a plasma power supply, a gas supply system and a control system. The heat treatment process comprises the following steps: S1, pretreatment; s2, charging and vacuumizing; s3, ion bombardment cleaning; s4, performing first-stage pressurized carburization; s5, carrying out micro displacement; s6, second-stage pressurized carburization is conducted; s7, diffusion is carried out; s8, quenching is conducted; and S9, tempering. Heating, pressurizing and shaping, plasma carburizing, quenching and tempering are completed in the same vacuum furnace body in an integrated mode, workpieces do not need to be transferred midway, and oxidation and secondary deformation are avoided. Through the design of the four-foot hollow clamping head, the thin metal plate is stably supported and limited, meanwhile, the contact area is remarkably reduced, uniformly-distributed heat transfer points are formed, buckling deformation of the thin plate at high temperature is effectively restrained, and carburizing blind areas are reduced.
Owner:LUOYANG INST OF SCI & TECH

Preparation method and application of nitride nuclear fuel

The invention belongs to the field of nuclear fuels, and particularly relates to a preparation method and application of a nitride nuclear fuel, the preparation method comprises the following steps: mixing an oxide raw material and a carbon source, and then pressing into a green body; and carrying out carbon thermal reduction and nitridation reaction on the green body by adopting a plasma method or a flash burning method to prepare the nitride nuclear fuel. According to the method, high-energy ion bombardment of plasma is utilized, so that the activity of reactants is remarkably improved, the carbon thermal reduction nitridation reaction is carried out at a lower temperature, the reaction temperature is reduced, and the reaction time is shortened, for example, high temperature is needed in a traditional carbon thermal reduction method; the reaction temperature can be reduced to be not higher than 1400 DEG C, meanwhile, the reaction period is shortened, and the reaction time can be shortened to be within 15 min. By adjusting the gas flow and energy parameters, the stoichiometric ratio of the nitride can be controlled, generation of an unstable intermediate phase is avoided, and meanwhile energy consumption is reduced.
Owner:CHINA NUCLEAR POWER TECH RES INST CO LTD +1

PVD (Physical Vapor Deposition) composite coated cooker and preparation method thereof

The preparation method comprises the following steps: carrying out surface cleaning and activating treatment on a metal cooker base body, putting the cooker into PVD coating equipment, vacuumizing, configuring a titanium target, a multi-component composite target and an oxide target, cleaning the surface of the cooker by adopting ion bombardment, depositing a titanium transition layer with the thickness of 0.1-0.5 mu m, and carrying out vacuum treatment to obtain the PVD composite coating cooker. The thickness of the deposited copper-aluminum-silicon-chromium carbide composite functional layer is 4.5-5.5 microns, the thickness of the deposited oxide surface layer is 0.2-0.8 microns, and furnace cooling is carried out after film plating is completed. The three-layer gradient structure design is adopted, the titanium transition layer and the base body form metallurgical bonding, the copper-aluminum-silicon-chromium carbide composite functional layer provides hydrophobic and oleophylic performance, the oxide surface layer blocks oxygen and nitrogen diffusion, and the comprehensive performance of being high in film layer bonding force, resistant to high temperature and lasting and non-sticky is achieved.
Owner:余成有

Highly densified alumina coating and process for its production

The application discloses a high-densification alumina coating and a processing technology thereof, and belongs to the technical field of ceramic coating materials. The alumina coating comprises at least one alumina single layer, and a dense interface layer is formed on each alumina single layer by ion bombardment on the surface of the alumina single layer; the alumina single layer is composed of AlO x , wherein the oxygen content is 0
Owner:NUCLEAR POWER INSTITUTE OF CHINA

Vacuumizing method and sputtering method

The application provides a vacuum pumping method and a sputtering coating method. The vacuum pumping method comprises the following steps: installing a target material in a coating chamber; isolating the coating chamber from the atmosphere, and then starting a vacuum pump; conveying a plate into the coating chamber; introducing working gas (Ar) into the coating chamber, starting a sputtering power supply, and forming a first electric field in the coating chamber, so that the working gas is converted into plasma, ions in the plasma bombard the plate, plate particles sputtered from the plate react with gas to be removed in the coating chamber and generate non-gaseous substances; eliminating the first electric field, stopping the introduction of the working gas, and continuing to pump high vacuum. The vacuum pumping method can shorten the vacuum pumping time required by the coating chamber.
Owner:SHENZHEN ARRAYED MATERIALS TECH CO LTD

Film coating equipment for completing film coating on inner wall of slender pipe through transfer station in vertical single cabin

The invention discloses a vertical single cabin film coating device for completing film coating of the inner wall of a slender pipe through a transfer station, the vertical single cabin film coating device comprises a feeding and discharging device and a furnace body, the feeding and discharging device comprises a material frame, an overturning power mechanism, a clamp and a push-pull mechanism, the overturning power mechanism provides power for state switching of the material frame, the clamp is slidably connected to an outer guide assembly of the material frame, and the push-pull mechanism is connected to the furnace body. An inner guide assembly, a translation power mechanism and process step treatment stations are arranged in the furnace body, the process step treatment stations at least comprise a vacuumizing station, an ion bombardment cleaning station and a coating station, a gas adsorption rod, an ion bombardment electrode device and a magnetron sputtering target are arranged at the upper end of the furnace body, and a lifting mechanism and a vertical telescopic cabin are correspondingly arranged at the upper end of the furnace body; and the gas adsorption rod, the ion bombardment electrode device and the magnetron sputtering target are positioned in the vertical telescopic cabin. According to the invention, the process steps required for coating the inner wall of the slender pipe can be simultaneously completed, and the slender pipe can be uniformly vacuumized and uniformly distributed with gas, so that the coating quality is ensured.
Owner:DONGGUAN HUICHENG VACUUM TECH

Inclined powder cleaning equipment

The invention discloses inclined powder cleaning equipment which comprises a cavity used for being connected with an anode of a power source; the tray is obliquely arranged in the cavity, the tray is provided with a containing groove, the bottom of the tray is used for being connected with a cathode of a power source, the containing groove is used for containing powder to be cleaned, and after the cavity and the tray are powered on, plasma used for bombarding the powder on the tray can be generated between the cavity and the tray; the stirring blades are rotationally arranged on the tray and are used for stirring the powder; the driving element is used for driving the stirring blades to rotate; the rotating structure is used for driving the tray to rotate; and the vacuumizing device is communicated with the cavity and is used for enabling the interior of the cavity to be in a negative-pressure vacuum state. Ion bombardment is carried out on the surface of the powder, so that oxides, dirt and other impurities on the surface of the powder are removed; the tray can rotate around the axis of the tray due to the rotating structure, so that in the cleaning process of the powder, besides mechanical stirring of the stirring blades, stirring under the gravity of the powder under the action of the inclination angle is increased, and the whole cleaning process is more uniform and thorough.
Owner:NINGBO YUNTU TECH CO LTD

Preparation method and application of micro-pit with polyimide as base material

The invention belongs to the technical field of material preparation, and particularly relates to a preparation method and application of a micro-pit with polyimide as a base material. The method provided by the invention mainly comprises the following steps: accelerating heavy ions by using an accelerator, bombarding polyimide by using the accelerated heavy ions, etching the polyimide by using an etching agent added with a corrosion inhibitor after the polyimide is damaged by the heavy ions to obtain micro-pits with specific diameters and depths, and cleaning and drying the etched sample. According to the method, the polyimide is impacted in an accelerated mode through heavy ions, the micro-pits are prepared, the limitation of a traditional photoetching technology is broken through, the patterns of the micro-pits are defined directly through heavy ion bombardment, a mask plate does not need to be used, the material cost is reduced, production interruption and extra cost caused by damage of the mask plate are avoided, and the production efficiency is improved. And the processing process is relatively simple, multiple complex photoetching and etching steps are not needed, the production efficiency is greatly improved, the production period is shortened, and the production cost is reduced.
Owner:RUICHANG INST OF APPLIED NUCLEAR PHYSICS +1

Method for changing the surface condition of a component by ion bombardment

The present invention relates to a method for plasma treating a target surface of a component, comprising the following steps: - obtaining a target surface on the component, - placing the component in a chamber of a plasma generator, - evacuating the chamber to a pressure of between 10 ‑6 and 10 mbar, - injecting a suitable gas into the chamber until the pressure in the chamber reaches between 10 ‑4 and 10 2 mbar, - generating an electric current discharge in the chamber via an electric generator to generate a plasma, - exposing the target surface of the component to the plasma for a predetermined time, depending on the power of the electric current discharge, the gas injected into the chamber and the material of the target surface, thereby deteriorating the surface condition of the target surface in order to increase its roughness to matte or more matte the target surface.
Owner:RUBART & WELLMAN GMBH