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129 results about "Sputter deposition" patented technology

Sputter deposition is a physical vapor deposition (PVD) method of thin film deposition by sputtering. This involves ejecting material from a "target" that is a source onto a "substrate" such as a silicon wafer. Resputtering is re-emission of the deposited material during the deposition process by ion or atom bombardment. Sputtered atoms ejected from the target have a wide energy distribution, typically up to tens of eV (100,000 K). The sputtered ions (typically only a small fraction of the ejected particles are ionized — on the order of 1 percent) can ballistically fly from the target in straight lines and impact energetically on the substrates or vacuum chamber (causing resputtering). Alternatively, at higher gas pressures, the ions collide with the gas atoms that act as a moderator and move diffusively, reaching the substrates or vacuum chamber wall and condensing after undergoing a random walk. The entire range from high-energy ballistic impact to low-energy thermalized motion is accessible by changing the background gas pressure. The sputtering gas is often an inert gas such as argon. For efficient momentum transfer, the atomic weight of the sputtering gas should be close to the atomic weight of the target, so for sputtering light elements neon is preferable, while for heavy elements krypton or xenon are used. Reactive gases can also be used to sputter compounds. The compound can be formed on the target surface, in-flight or on the substrate depending on the process parameters. The availability of many parameters that control sputter deposition make it a complex process, but also allow experts a large degree of control over the growth and microstructure of the film.

Method for prolonging service life of resistance spot welding electrode, manufactured resistance spot welding electrode cap and application

The invention discloses a method for prolonging the service life of a resistance spot-welding electrode, a manufactured resistance spot-welding electrode cap and application, and the method comprises the following steps: taking a chromium-zirconium-copper electrode cap as a base body, grinding the working surface of the base body step by step by adopting abrasive paper, and then sequentially polishing, ultrasonically cleaning and drying to obtain a pretreated base body; performing vacuum zirconium permeation treatment on the pretreated matrix by adopting a permeation agent so as to form a zirconium-rich solid solution diffusion layer in the pretreated matrix, thereby obtaining the matrix subjected to zirconium permeation reinforcement; physical vapor deposition treatment is adopted, and a metal transition layer is deposited on the surface of the solid solution diffusion layer of the matrix subjected to zirconium permeation strengthening; wherein the metal transition layer is a Cr transition layer or a Ti transition layer; and a graphite target and titanium target co-sputtering mode is adopted, and a composite gradient functional layer is sputtered and deposited on the surface of the metal transition layer of the matrix treated in the step S3. The electrode service life of the method is improved by magnitude order, and the effect is extremely remarkable.
Owner:BENGANG STEEL PLATES CO LTD

Vacuum sputtering preparation process of multi-layer gradient color film for streaming media rearview mirror cover plate

The invention discloses a vacuum sputtering preparation process of a multi-layer gradient color film for a streaming media rearview mirror cover plate, and belongs to the technical field of magnetron sputtering coating. The process depends on vacuum sputtering equipment comprising an upper sheet translation table, an upper sheet table, a sheet inlet chamber, a front fine extraction chamber, a front buffer chamber, a first coating chamber, a transition chamber, a second coating chamber, a rear buffer chamber, a rear fine extraction chamber, a sheet outlet chamber, a lower sheet table, a lower sheet translation table and the like. The method comprises the steps of glass substrate pretreatment, vacuum buffer stabilization, preparation of an aluminum layer and a silicon-aluminum alloy layer in a first coating chamber, stress release in a transition chamber, preparation of an aluminum-nitrogen oxide layer in a second coating chamber, post buffer stabilization, sheet discharging and discharging and the like. The technical effects that the color is continuously adjustable, the adhesive force of the film layer is high, the optical and electrical properties are balanced, and the production efficiency is high are achieved.
Owner:FOSHAN JINGBO TECH CO LTD

Layout design method for high-precision magnetron sputtering deposition equipment

The invention provides a layout design method for high-precision magnetron sputtering deposition equipment. The method comprises the following steps: firstly, determining sputtering deposition subsystem layout parameters such as revolution radius, target-base distance, target length and the like according to an optimized target difference value of a to-be-plated element parameter, a target preliminary sputtering yield parameter and a film thickness; then, whether the film thickness distribution under the layout parameters meets an optimization target difference value or not is evaluated; and finally, vacuum chamber subsystem layout parameters such as the diameter and the height of the vacuum chamber are calculated. According to the method, a quantitative design mode is adopted, the problems that existing magnetron sputtering deposition equipment layout design depends on experience, and whether the magnetron sputtering deposition equipment meets design index requirements or not is difficult to evaluate are effectively solved, and the scientificity and rationality of equipment layout are improved.
Owner:SHANGHAI INST OF OPTICS & FINE MECHANICS CHINESE ACAD OF SCI

Automatic temperature control system and method for sputtering deposition device

The invention belongs to the technical field of sputter deposition, and provides an automatic temperature control system and method for a sputter deposition device, and the system realizes the accurate control of the cavity temperature in the sputter deposition process by integrating components such as a vacuum gauge, a gas cylinder, a valve, a thermocouple temperature measurement element and a PID (Proportion Integration Differentiation) regulator. The system monitors the temperature of the cavity in real time by using the thermocouple, and automatically adjusts the power of the heating wire through the PID regulator according to the comparison result of a set value and an actual value, thereby maintaining the stability of the temperature of the cavity. In addition, the system has the function of communicating with an upper computer, remote monitoring and control can be carried out through a software layer, and the automation level and the temperature control precision of the sputtering deposition process are improved. The problems that in the prior art, temperature control precision is low, the automation degree is insufficient, and stability is poor are solved, through linkage control over the temperature, the vacuum degree and the gas flow, the consistency of film performance is guaranteed, and the method is suitable for large-scale production of high-precision films.
Owner:ZHONGBEI UNIV

A physical vapor deposition apparatus, an electrochromic device, and a method of manufacturing the same

The application discloses a physical vapor deposition device, an electrochromic device and a preparation method thereof, and relates to the technical field of electrochromic devices. The preparation method comprises the following steps: sputtering and depositing an electrochromic layer of WO3 on the surface of a first ITO layer, and the oxygen content is any value in the range of 42.5% to 52.5%; sputtering and depositing a pre-set thickness of a tungsten oxide ion conduction layer on the electrochromic layer, and the oxygen content of the corresponding chamber is any value in the range of 35% to 45%; sputtering and depositing an ion storage layer containing lithium ions on the ion conduction layer; depositing a second ITO layer on the ion storage layer, and obtaining the electrochromic device after vacuum annealing treatment and cooling treatment; wherein the deposition temperature of the second ITO layer is any value in the range of 350 DEG C to 400 DEG C, and the annealing temperature of the vacuum annealing treatment is any value in the range of 450 DEG C to 500 DEG C. The electrochromic device prepared by the application has the characteristics of high transmittance and low sheet resistance.
Owner:SUZHOU BEARSUNNY TECHNOLOGIES INC

Sputter deposition

To provide a sputter deposition apparatus.SOLUTION: A sputter deposition apparatus (100) comprising a remote plasma generating arrangement (106) arranged to provide a plasma (120) for sputter depositing a target material (102) in a sputter deposition region (112), a confining arrangement arranged to provide a confining magnetic field to substantially confine the plasma to the sputter deposition region, a substrate (104) provided in the sputter deposition region, and one or more target support assemblies (108) arranged to support one or more targets in the sputter deposition region to effect sputter deposition of the target material on the substrate, wherein the confinement arrangement confines the remote plasma to the target support assembly such that, in use, target material is deposited as a first region on the substrate, target material is deposited as a second region on the substrate, and an intermediate region between the first region and the second region is free of target material. 2.SELECTED DRAWING: Figure 1
Owner:DYSON TECH LTD

Phase shift mask substrate and dynamic magnetron sputtering preparation method thereof

The invention relates to a phase shift mask substrate and a dynamic magnetron sputtering preparation method thereof, a MoSi-based gradient film layer is continuously and dynamically deposited on the substrate, and the method comprises the following steps: carrying out first-stage deposition on the substrate by adopting a molybdenum-silicon alloy target so as to form a transition layer; carrying out second-stage deposition on the transition layer to form a main body functional layer through deposition; and third-stage deposition is carried out on the main body functional layer to form a surface modification layer through deposition, and the MoSi-based gradient film layer is obtained. The invention provides a one-step sputtering deposition method capable of dynamically and accurately regulating and controlling, so that the inherent contradiction between the performance and the stress of a single-layer uniform film is fundamentally solved, and the complexity and the uncertainty of a traditional multi-step process are avoided.
Owner:SHAOXING XINLIAN SEMICON TECH CO LTD

Optical device and manufacturing method therefor

An optical device includes, in sequence, a surface formed of a metal oxide, a samarium oxide-containing layer in contact with the surface formed of a metal oxide, and a magnesium fluoride-containing layer in contact with the samarium oxide-containing layer so as to suppress optical absorption resulting from high-rate sputter deposition of a magnesium fluoride-containing layer on a surface formed of a metal oxide.
Owner:CANON KK

Method and system for measuring net sputter deposition rate of hall thruster

The application provides a Hall thruster net sputtering deposition rate measurement method and system, and relates to the technical field of thrusters, comprising: obtaining a first initial mass corresponding to a first test piece, a second initial mass corresponding to a second test piece, and a ring cylinder initial mass corresponding to a thin-walled ring cylinder placed at the same height of the Hall thruster; obtaining a first final mass corresponding to the first test piece and a ring cylinder final mass corresponding to the thin-walled ring cylinder in the case that the Hall thruster is operated based on a first measurement condition; obtaining a second final mass corresponding to the second test piece in the case that the Hall thruster is operated based on a second measurement condition; and determining a net sputtering deposition rate measurement result corresponding to the Hall thruster based on the initial masses and the final masses. The application can simplify the measurement process of the net sputtering deposition amount and the required equipment requirements, and improve the measurement accuracy of the net sputtering deposition amount.
Owner:BEIHANG UNIV

Manufacturing process for solar control and / or low-emissivity glazing, transparent to radio frequencies: cracked sol-gel overcoat

ActiveFR3161677B1CoatingsSilicon oxideHYDROSOL
The present invention relates to a method for manufacturing a glass article comprising the following steps: - the provision of a glass substrate, - the deposition, on at least one face of said glass substrate, of a stack of layers comprising at least one functional metallic layer containing silver, each of said layers being deposited by magnetic field assisted sputtering, - the application of a sol-gel solution comprising at least one silicon oxide precursor and / or at least one transition metal oxide precursor, said solution being applied over said stack of layers, so as to form a sol-gel layer having an average thickness of between 50 nm and 3000 nm, preferably between 70 nm and 1500 nm, - the heat treatment at a temperature above 500°C, preferably between 540°C and 700°C, so as to crack the sol-gel layer and damage the stack of layers.The present invention also relates to a glass article that can be obtained by such a process which comprises a glass substrate coated on at least one of its faces: - with a stack of layers comprising at least one functional metallic layer containing silver, and - with at least one sol-gel layer located above said stack of layers and having an average thickness between 50 nm and 3000 nm, preferably between 70 nm and 1500 nm, said stack of layers and said sol-gel layer having cracks or fissures.
Owner:SAINT GOBAIN VITRAGE SA

Physical vapor deposition equipment, electrochromic device and preparation method of electrochromic device

The invention discloses physical vapor deposition equipment, an electrochromic device and a preparation method of the electrochromic device, and relates to the technical field of electrochromic devices. The preparation method comprises the following steps: sputtering and depositing the WO3 electrochromic layer on the surface of the first ITO layer, wherein the oxygen content is any one of 42.5-52.5%; sputtering and depositing a tungsten oxide ion conducting layer with a preset thickness on the electrochromic layer, wherein the oxygen content of the corresponding chamber is any one of 35%-45%; sputtering and depositing an ion storage layer containing lithium ions on the ion conduction layer; a second ITO layer is deposited on the ion storage layer, and the electrochromic device is prepared after vacuum annealing treatment and cooling treatment; wherein the deposition temperature of the second ITO layer is any one value from 350 DEG C to 400 DEG C, and the annealing temperature of the vacuum annealing treatment is any one value from 450 DEG C to 500 DEG C. The electrochromic device prepared by the invention has the characteristics of high transmittance and low sheet resistance.
Owner:SUZHOU BEARSUNNY TECHNOLOGIES INC

Multi-target ion beam sputter coating device and use method thereof

The invention provides a multi-target ion beam sputter coating device and a use method thereof.The device comprises a vacuum cavity, a base carrying disc and an auxiliary ion gun vertically opposite to the base carrying disc are arranged in the vacuum cavity, and the left side and the right side of the auxiliary ion gun are each provided with a main ion gun and a target material exchange mechanism; the target material exchange mechanism comprises a supporting frame, a target material base rotating by 360 degrees is arranged in the supporting frame, target materials are evenly distributed on the side, close to the main ion gun, of the target material base in the circumferential direction, a baffle is arranged on the side, close to the main ion gun, of the supporting frame, and a notch matched with the main ion gun is formed in the baffle. Target materials can be flexibly selected for thin film deposition according to needs, frequent manual target material replacement or equipment adjustment is not needed, time and labor cost are saved, and meanwhile thin film deposition continuity is ensured.
Owner:ZHONGYUAN ENGINEERING COLLEGE

Vacuum sputtering plating method for sawteeth

The invention relates to the technical field of workpiece surface treatment, and discloses a vacuum sputtering plating method for sawteeth. Comprising the steps of substrate pretreatment, sawtooth vacuum sputtering to form a mechanical occlusion structure, selective activation achieved through alternating soaking-inclined rotation catalytic activation, pulse stirring assisted double-liquid alternating chemical plating to form a composite coating, double-liquid gap gas purging to eliminate cross contamination, surface homogenization treatment, graded passivation treatment and the like. According to the invention, through a composite structure of the sawtooth sputtering layer and the chemical plating layer, a dual combination mode of mechanical occlusion and chemical bonding is formed; alternating soaking-inclined rotating catalytic activation is adopted to eliminate direction dependence, and controllable enrichment of a catalyst in a groove is achieved. The mass transfer limitation of the deep groove is overcome by adopting a pulsating stirring auxiliary plating technology; double-liquid alternate pollution is eliminated by adopting a gas purging technology; and a nickel-phosphorus / nickel-tungsten alternate multi-layer composite structure is formed, and high hardness and high toughness are achieved at the same time.
Owner:AOGE NEW MATERIALS (DALIAN) CO LTD

Low-temperature magnetron sputtering planar cathode structure

The utility model relates to the technical field of magnetron sputtering, and discloses a low-temperature magnetron sputtering plane cathode structure which comprises a cathode flange, a magnetic shoe is arranged on the inner side of the cathode flange, a cooling plate is arranged at the top end of the magnetic shoe, a target material is installed on the cooling plate through a limiting assembly, a target material baffle is arranged at the top of the cathode flange, and a target material baffle is arranged at the bottom of the cathode flange. A first water cooling channel is arranged in the target baffle of the cathode flange, and the first water cooling channel in the cathode flange and the first water cooling channel in the target baffle are communicated with each other. And heat generated during magnetron sputtering can be absorbed, comprehensive cooling of the working target surface can be achieved, heat borne by the substrate is only generated through sputtering deposition, heat radiation in the target material sputtering process is effectively reduced, and low-temperature coating is achieved.
Owner:ZHONGKE YUANCUI (JIANGSU) EQUIPMENT TECHNOLOGY CO LTD

Preparation method of AlN thin film for high-frequency broadband filter and AlN thin film

This application provides a method for preparing an AlN thin film for a high-frequency broadband filter and the AlN thin film itself, belonging to the field of semiconductor device technology. The method for preparing the AlN thin film includes the following steps: 1) growing a substrate layer on a Si substrate using MOCVD to obtain a substrate epitaxial wafer; 2) performing low-power PVD sputtering deposition on the substrate epitaxial wafer to grow an AlN intermediate layer; 3) then performing high-power PVD sputtering deposition on the AlN intermediate layer to grow an AlN top layer, thus obtaining the AlN thin film. This application, through the combined use of two PVD sputtering deposition steps, can simultaneously coordinate the warpage, surface roughness, and crystal quality of the AlN thin film, thereby obtaining an AlN thin film with excellent overall performance.
Owner:BEIJING ZHONGBOXIN SEMICON TECH CO LTD

Aluminum strip surface strengthening process based on CVD (Chemical Vapor Deposition)

The invention belongs to the technical field of aluminum strip surface treatment, and particularly relates to a CVD (chemical vapor deposition)-based aluminum strip surface strengthening process. The method aims at solving the problem that an existing aluminum strip surface strengthening method is difficult to improve the durability of an aluminum strip in a high-salt-mist environment. The method comprises the following steps: firstly, straightening and activating an aluminum strip, and after the treatment is completed, feeding the aluminum strip into a deposition chamber for magnetron sputtering deposition, specifically comprising a metal injection stage, a nitriding support stage and a composite deposition stage. And then, the aluminum strip is fed into a deposition workshop to be subjected to a pulse CVD process, functional modification is carried out after the pulse CVD process is completed, and a Ti-Si diffusion layer, a TiSiN diffusion layer, a Ti-Si-C-N composite layer, a multi-layer corrosion-resistant layer and a fluorine-containing layer are sequentially arranged on the surface of the aluminum strip subjected to the surface strengthening process. According to the surface strengthening process provided by the invention, the use durability of the aluminum strip in a high salt mist environment can be effectively guaranteed, and the aluminum strip has excellent surface hardness and structural stability.
Owner:SUZHOU LILAI IRON & STEEL CO LTD

Apparatus for magnetron sputter deposition of multilayer high-entropy alloy coatings

The utility model relates to vacuum coating equipment technical field especially is concerned on a kind of equipment of magnetron sputtering deposition multilayer high-entropy alloy coating, including vacuum cavity and the workpiece rotating stand being set in the inside of vacuum cavity, the cylindrical target assembly extends to the inside central region of vacuum cavity along axial direction, the lateral target assembly includes lateral target material, backplate and the composite magnetic field generating unit of installation in the corresponding vacuum cavity inboard side of backplate, the composite magnetic field generating unit includes permanent magnet array and electromagnetic coil assembly, which is arranged around or stacked on the side or back of permanent magnet array, an independent power supply terminal is respectively provided on the cylindrical target assembly and each lateral target assembly, the vacuum cavity is also connected with air interface, the utility model realizes the millisecond level accurate switching of bias, gas ratio, deposition time and power supply power, supports the continuous preparation of multilayer high-entropy alloy coating with variable composition and excellent bonding force under single vacuum atmosphere.
Owner:WENZHOU UNIV

Target structure and magnetron sputtering method and magnetron sputtering apparatus thereof

PendingCN122358132AEtchingThin membrane
This application provides a target structure, a magnetron sputtering method, and a magnetron sputtering apparatus. The target structure includes a first cylindrical target, a second cylindrical target, a first magnetic element, and a second magnetic element. The first and second cylindrical targets are arranged parallel to each other and symmetrically. The first magnetic element is movably disposed within the first cylindrical target along a first axial direction, and the second magnetic element is movably disposed within the second cylindrical target along a second axial direction. In the target structure provided by this application, the first magnetic element is movably disposed within the first cylindrical target along the first axial direction, and the second magnetic element is movably disposed within the second cylindrical target along the second axial direction. This allows for sufficient etching of both the first and second cylindrical targets, avoids waste of material from both targets, ensures the utilization rate of both targets, and improves the thickness uniformity and compositional consistency of the sputtered deposited film.
Owner:JIANGSU MICROVIA NANO EQUIP TECH CO LTD

Heat-insulation electromagnetic shielding film for spaceflight and preparation method of heat-insulation electromagnetic shielding film

The film is of a layered structure, the middle of the film is an organic base material, the base material comprises a first surface and a second surface, and a transition layer, an electromagnetic absorption layer, an isolation layer, an electromagnetic reflection layer and a thermal radiation reflection layer are sequentially distributed on the first surface and the second surface. Meanwhile, penetrating through holes are distributed in the surface of the film, and conductive layers are attached to the inner walls of the through holes to communicate all the layers. The thin film utilizes the closed reflection effect of the electromagnetic reflection layer and the loss effect of the electromagnetic absorption layer, and the electromagnetic shielding effectiveness of the thin film in the wave band of 10 MHz to 10 GHz is larger than 80 dB; the hemispherical emissivity of the heat radiation reflecting layer on the outermost layer is 0.03-0.05, and the solar absorptivity is 0.09 + / -0.02. The preparation method of the thin film comprises the steps of substrate plasma modification, magnetron sputtering deposition of the multi-layer functional film, punching, vacuum evaporation plating of the heat radiation reflecting layer, annealing treatment and the like, and the process controllability is high. The thin film integrates the functions of electromagnetic shielding, thermal control, static prevention and heat dissipation, and has important application value in the field of aerospace equipment.
Owner:BEIJING TIANYU AEROSPACE NEW MATERIAL TECH CO LTD +1

Photo-thermal regulation and control multilayer film and preparation method thereof

The invention provides a photo-thermal regulation and control multilayer film and a preparation method thereof, and belongs to the technical field of optical films, the film comprises a fourth film layer, a third film layer, a second film layer and a first film layer which are sequentially sputtered and deposited on the surface of a graphite substrate from bottom to top; wherein the first thin film layer and the second thin film layer are used for realizing visible light structural color regulation and mechanical protection, the third thin film layer is used for realizing directional radiation of a target angle in a medium and long infrared band, and the fourth thin film layer, the third thin film layer, the second thin film layer and the first thin film layer form a Fabry-Perot resonant cavity. Therefore, the wave absorbing performance of the whole film in a medium-long infrared band can be regulated and controlled. The photo-thermal regulation and control multi-layer thin film successfully realizes organic coupling of mechanical protection, visible light structural color regulation and control, and medium and long infrared directional radiation and radiation heat dissipation.
Owner:HARBIN INST OF TECH

Film forming apparatus and film forming method

A film forming apparatus includes a processing container, a substrate holder configured to hold a substrate inside the processing container, a cathode unit disposed above the substrate holder, and a gas introducing mechanism configured to introduce a plasma generating gas into the processing container. The cathode unit includes a target, a power supply configured to supply electric power to the target, a magnet provided on a rear side of the target, and a magnet driving part configured to drive the magnet. The magnet driving part includes an oscillation driver configured to oscillate the magnet along the target, and a perpendicular driver configured to drive the magnet in a direction perpendicular to a main surface of the target independently of driving performed by the oscillation driver. Sputtered particles are deposited on the substrate by magnetron sputtering.
Owner:TOKYO ELECTRON LTD

Infrared detector chip preparation method based on gold-free electrode

A preparation method of an infrared detector chip based on a gold-free electrode relates to the technical field of infrared detection, and comprises the following steps: preparing a required to-be-metallized infrared detector wafer, sputtering and depositing a gold-free electrode film layer on the to-be-metallized infrared detector wafer; depositing a gold-free electrode film layer with a certain thickness on the surface of the wafer by setting parameters of sputtering power, gas flow and heating temperature, and completing preparation of a metal electrode after a stripping process; the infrared detector wafer after electrode preparation is subjected to dilute acid solution post-treatment, an oxide layer and impurities on the surface of the metal electrode are removed through a dilute acid solution, and preparation of the infrared detector wafer is completed; and finally, cutting the infrared detector wafer to complete the preparation of the infrared detector chip. According to the invention, good ohmic contact between the electrode and an infrared focal plane detector wafer and good flip-chip interconnection between the electrode and high-purity indium are realized, and the electrode is used as a low-cost choice for replacing a system taking Au as a core electrode.
Owner:CHINA AVIATION KAI MAI(SHANGHAI)INFRARED TECH CO LTD

Thin film deposition equipment

The utility model relates to the technical field of vacuum coating, in particular to thin film deposition equipment. The thin film deposition equipment comprises a bias power supply device, a driving device, a vacuum chamber, a workpiece positioning device and a deposition source, wherein the workpiece positioning device and the deposition source are arranged in the vacuum chamber; wherein the workpiece positioning device is provided with a positioning area for positioning a workpiece; the deposition source is used for generating a thin film source material and enabling the thin film source material to be sputtered outwards, and the sputtering end of the deposition source is arranged towards the positioning area of the workpiece positioning device; the voltage output end of the bias voltage power supply device extends into the vacuum chamber and is connected with the workpiece positioning device so as to apply bias voltage to the workpiece through the workpiece positioning device; and a driving shaft of the driving device extends into the vacuum chamber, is connected with a rotating shaft of the workpiece positioning device through an insulating coupling, and drives the workpiece positioning device to rotate. According to the workpiece positioning device capable of avoiding applying the bias voltage, the bias voltage is transmitted to the outside through the driving shaft of the driving device, short circuit of a power supply is avoided, and potential safety hazards are reduced.
Owner:O NET COMM (SHENZHEN) LTD

Preparation method of replicated ultra-cold neutron extraction conduit

The invention discloses a preparation method of a replicated ultra-cold neutron extraction conduit, and belongs to the cross technical field of neutron optical device manufacturing and precision manufacturing, and the preparation method comprises the following steps: providing plate glass with the surface roughness superior to 0.5 nm as a substrate, and depositing a Ni / Ti neutron super mirror aperiodic multilayer film on the substrate by adopting a magnetron sputtering technology, the bottommost layer of the super-mirror multilayer film is a Ni layer in direct contact with the glass substrate, and the topmost layer is a Ti layer; a Cu seed layer continues to be sputtered and deposited on the non-periodic multilayer film of the Ni / Ti neutron super mirror, a mask plate is used in the sputtering process, and an uncoated blank area of 3-5 mm is reserved between the edge of the deposited film layer and the edge of the glass substrate. According to the method, a replication process route of super mirror preparation, seed layer deposition, precise electroplating, stress regulation and control, mechanical stripping and precise shaping is adopted, preparation of all high-performance film layers is completed on a super-smooth plane substrate, and it is ensured that the quality of the functional film is not limited by the geometrical shape of a base body.
Owner:CHINA SPALLATION NEUTRON SOURCE SCI CENT +1

Sputtering deposition equipment and methods

A sputtering deposition apparatus (100) includes: a plasma generation device (106) arranged to provide a single plasma (120) for sputtering deposition of target material within a sputtering deposition region (112); a transport system (110) arranged to transport a substrate (104) through the sputtering deposition region in a transport direction (D); and one or more target support assemblies (108) arranged to support one or more targets (108) in the sputtering deposition region to provide sputtering deposition of target material on the substrate using plasma, such that during use, when the substrate is transported through the sputtering deposition region, the following are deposited: a first stripe on the substrate; and a second stripe on the substrate, wherein the first stripe includes at least one of a target material of a different density or a target material of a different composition than the second stripe.
Owner:DYSON TECH LTD

Silicon carbide-based strain temperature micro-nano sensor and preparation and detection method thereof

PendingCN122305900ACarbide siliconEtching
A silicon carbide-based strain-temperature micro / nano sensor is provided, comprising a silicon carbide substrate, on which an N-type buffer layer and a P-type functional layer are grown to form a strain-sensitive substrate; the P-type functional layer is precisely processed using NLD etching, and the remaining area forms four interconnected piezoresistive blocks; in a designated area on the four piezoresistive blocks, Ti thin films, Ni thin films, and Pt thin films are sequentially sputtered using magnetron sputtering to form four metal electrodes, and the four piezoresistive blocks form a four-resistance bridge to achieve high-sensitivity strain measurement, thereby forming a strain sensor; on the back side of the silicon carbide substrate, a strip-shaped, tortuous, hollowed-out area is defined, and an alumina barrier layer and a platinum Pt thin film layer are sequentially sputtered and deposited using magnetron sputtering to form a strip-shaped, tortuous, tortuous temperature sensing strip, the temperature sensing strip including two ends for external electrical connection; the present invention also provides its preparation method and detection method.
Owner:NINGBO UNIV

Preparation method of A-axis highly preferred orientation perovskite composite film

The invention discloses a preparation method of an A-axis highly preferred orientation perovskite composite film, and the method comprises the following steps: S1, coating a layer of perovskite precursor through a spin coating technology under the conditions of atmospheric environment and room temperature, and carrying out the low-temperature baking of about 70 DEG C, thereby obtaining a perovskite film; s2, under the vacuum condition, preparing a metal molybdenum thin film with the thickness of 3-10nm on the surface of the perovskite thin film through a magnetron sputtering deposition technology; and S3, forming a composite film structure by the metal molybdenum film and the perovskite film, wherein the film structure shows highly preferred orientation in the A-axis direction. According to the invention, the method has the advantages of simple operation, green and environment-friendly preparation process flow, short preparation period, low cost, large-area production and the like.
Owner:SHANGHAI SECOND POLYTECHNIC UNIVERSITY

A lead zirconate titanate thin film and a low-temperature preparation method and application thereof

The application relates to the technical field of piezoelectric materials, in particular to a lead zirconate titanate film and a low-temperature preparation method and application thereof, the preparation method comprising the following steps: Ti metal is taken as a radio frequency target material to perform first sputter deposition treatment on a substrate to form a Ti adhesion layer; a bottom electrode is formed on the Ti adhesion layer; Pb x Zr 0.52 Ti 0.48 O3 ceramic is taken as a radio frequency target material to perform second sputter deposition treatment on the bottom electrode, rapid heat treatment is performed, a PZT seed layer is formed; Pb x Zr 0.52 Ti 0.48 O3 ceramic is taken as a radio frequency target material to perform third sputter deposition treatment on the PZT seed layer, rapid heat treatment is performed, the step is repeated, and a lead zirconate titanate film is formed. In the process of sputter deposition of the PZT film material, the substrate tray is not additionally heated, the loss and volatilization of PbO are reduced, the film component stability can be effectively maintained; more crystal nuclei are provided by the PZT seed layer, the uniform crystallization of the PZT film is promoted, the crystallization quality and electrical properties of the PZT film are improved, the crystal boundary defects are reduced, and the adhesion and stability of the film and the substrate are enhanced.
Owner:SOUTHERN UNIVERSITY OF SCIENCE AND TECHNOLOGY

Preparation method of probe surface coating of MEMS probe card

The invention relates to a preparation method of a probe surface coating of an MEMS probe card. The preparation method comprises the following steps: 1) fixing a metal probe in a deposition chamber of a three-dimensionally rotatable magnetron sputtering tool; (2) introducing inert gas into the deposition chamber, and applying direct-current negative bias to remove pollutants on the surface of the probe; (3) applying negative bias voltage in a pulse mode; (4) sputtering and depositing a metal and silicon composite coating in an inert gas atmosphere; (5) introducing acetylene, applying negative bias to deposit a high-hardness diamond-like carbon layer on the surface of the composite coating, and synchronously introducing carbon tetrafluoride; (6) continuously increasing the flow of carbon tetrafluoride and reducing the flow of acetylene; (7) stopping introducing acetylene when the flow of the carbon tetrafluoride reaches 120sccm and the refractive index is less than or equal to 1.8; (8) switching off the power supply, introducing inert gas for temperature control cooling, and taking out the probe after cooling to room temperature; and (9) stripping the coatings of the probe head and the probe tail, so that the conductivity of the probe is not influenced.
Owner:NINGBO UNIVERSITY OF TECHNOLOGY

Preparation method of high plasticity cadmium telluride film with super-nanotwin and equiaxed crystal structure

The application discloses a preparation method of a high-plasticity cadmium telluride film with super-nanometer twin crystal and equiaxed crystal structures. The cadmium telluride film is prepared by means of magnetron sputtering deposition, and the film with super-nanometer twin crystal and equiaxed crystal structures is prepared by means of work gas pressure regulation and intermittent sputtering at a certain working temperature. The work gas pressure ranges from 1.5 Pa to 3.0 Pa, the working temperature ranges from 25 DEG C to 75 DEG C, the intermittent sputtering method is that sputtering is performed for 20 min to 30 min, sputtering is stopped for 15 min to 30 min as a cycle, and the sputtering is repeated for several cycles so that the total sputtering time is 3 h to 5 h. The cadmium telluride film prepared by the method has an equiaxed crystal average grain size of 5 nm to 10 nm and an average twin crystal layer thickness of 1.2 nm to 2.0 nm, and both are in the order of magnitude of super-nanometer (<10 nm), and the plasticity is increased by 3 to 6 times under the condition that the strength is equivalent to that of a traditional columnar crystal structure.
Owner:WUHAN UNIV OF TECH