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243 results about "Sputter deposition" patented technology

Sputter deposition is a physical vapor deposition (PVD) method of thin film deposition by sputtering. This involves ejecting material from a "target" that is a source onto a "substrate" such as a silicon wafer. Resputtering is re-emission of the deposited material during the deposition process by ion or atom bombardment. Sputtered atoms ejected from the target have a wide energy distribution, typically up to tens of eV (100,000 K). The sputtered ions (typically only a small fraction of the ejected particles are ionized — on the order of 1 percent) can ballistically fly from the target in straight lines and impact energetically on the substrates or vacuum chamber (causing resputtering). Alternatively, at higher gas pressures, the ions collide with the gas atoms that act as a moderator and move diffusively, reaching the substrates or vacuum chamber wall and condensing after undergoing a random walk. The entire range from high-energy ballistic impact to low-energy thermalized motion is accessible by changing the background gas pressure. The sputtering gas is often an inert gas such as argon. For efficient momentum transfer, the atomic weight of the sputtering gas should be close to the atomic weight of the target, so for sputtering light elements neon is preferable, while for heavy elements krypton or xenon are used. Reactive gases can also be used to sputter compounds. The compound can be formed on the target surface, in-flight or on the substrate depending on the process parameters. The availability of many parameters that control sputter deposition make it a complex process, but also allow experts a large degree of control over the growth and microstructure of the film.

Discontinuous metal film with tunneling effect, tunneling electrode chip and preparation method thereof

The invention provides a discontinuous metal film with a tunneling effect, a tunneling electrode chip and a preparation method of the tunneling electrode chip. A large-area uniform discontinuous metal film grows in situ on a glass substrate through a magnetron sputtering deposition method, and a charge tunneling structure with a random nano array is constructed. The discontinuous metal thin film comprises a substrate and a nano gap thin film arranged on the substrate, the nano gap thin film comprises a plurality of nano islands and a plurality of nano gaps which are randomly distributed, and a nano gap is formed between any two adjacent nano islands and a nano gap lt; 10 nm; the thickness of the nano-gap film is lt; the wavelength is 100 nm. According to the tunneling electrode chip, atomic-scale thickness control is achieved through high-precision thin film deposition, the uniformity of multi-batch devices is remarkably improved, the yield is improved by 50% or above compared with a traditional method, the limitation of high cost of micro-nano machining faced by a traditional tunneling device is broken through, and the tunneling electrode chip has the sensitive response capacity for different small molecule media and is suitable for large-scale popularization and application. Molecular information can be presented in the form of transient conductance information.
Owner:ZHEJIANG UNIV

A discontinuous metal film with tunneling effect, a tunneling electrode chip and a preparation method thereof

The present invention provides a discontinuous metal film with a tunneling effect, a tunneling electrode chip, and a method for preparing the same. A large-area uniform discontinuous metal film is in situ grown on a glass substrate by magnetron sputtering deposition, constructing a charge tunneling structure with a random nanoarray. The discontinuous metal film comprises a substrate and a nanogap film disposed on the substrate. The nanogap film comprises a number of randomly distributed nanoislands and a number of nanogaps. A nanogap is formed between any two adjacent nanoislands, and the nanogap is <10 nm. The thickness of the nanogap film is <100 nm. The tunneling electrode chip achieves atomic-level thickness control through high-precision thin film deposition, significantly improving the uniformity of multiple batches of devices and increasing the yield by more than 50% compared to traditional methods. This breaks through the expensive micro-nano processing limitations faced by traditional tunneling devices, has the ability to sensitively respond to different small molecule media, and can present molecular information as transient conductivity information.
Owner:ZHEJIANG UNIV

Near real-time, hands-off detection of airborne particulate contaminants and bioburden

Various implementations, systems and methods are disclosed for continuous, near real-time, hands-off sampling of airborne particulate matter, and qualification and / or quantification of biomolecules in the sample representative for biologic or microbial contamination. The systems and methods may utilize an electrostatic precipitator for sampling the matter; and a measurement assembly configured to illuminate, excite, or breakdown the sampled matter by electromagnetic radiation, and to detect a spectrum, or one or more wavelength bands of the scatter emitted by the sample. In an exemplary implementation, a sputter deposition process is employed to configure the sample for an enhanced plasmon resonance. The measurement data may be transferred via wireless communication means for cloud storage and signal processing.
Owner:BERNDT ERNST ULRICH +5

Magnetron sputtering device and sputtering cathode thereof

The invention relates to a magnetron sputtering device and a sputtering cathode thereof, the sputtering cathode comprises a target material, a first magnetic field generating device and a second magnetic field generating device, and the target material is provided with a target material surface; the first magnetic field generating device is used for forming a first magnetic field parallel to the surface of the target on the surface of the target; the second magnetic field generating device is used for forming a second magnetic field perpendicular to the surface of the target on the surface of the target; wherein under the combined action of the first magnetic field and the second magnetic field, the plasma area on the surface of the target material is expanded towards the substrate, so that the incident angle distribution of sputtering particles to the substrate is changed, and the sputtering deposition of the side wall of the deep hole or the groove is improved.
Owner:DONGGUAN KESHENG ELECTROMECHANICAL EQUIPMENT CO LTD +1

Magnetron sputtering target gun with high sputtering rate

The utility model relates to the technical field of magnetron sputtering, and particularly discloses a high-sputtering-rate magnetron sputtering target gun which comprises a target seat, an anode cover body arranged on the outer side of the target seat, a target material body mounted in a mounting groove, a copper back plate arranged on the upper side of the bottom end of the target seat, and a target material gland arranged on the outer side of the bottom end of the target seat, a magnetic ring is further arranged between the first cooling copper table and the second cooling copper table, a magnetic yoke is installed at the upper end of the second cooling copper table, a connecting aluminum table is installed at the upper end of the magnetic yoke, and an insulator is arranged on the outer side of the connecting aluminum table. According to the utility model, the spatial position of the permanent magnet magnetic steel and the structure of the target gun are optimized, so that the magnetic intensity penetrating through the surface of a target material is guaranteed, the magnetic field intensity of a magnetic control plasma area is high, the magnetic control effect is more obvious, the sputtering rate of magnetron sputtering is greatly improved, the production efficiency of magnetron sputtering is also improved, and the production cost is reduced. And for a magnetic material which cannot be sputtered by common magnetron sputtering, sputtering deposition can also be carried out, so that the application range of magnetron sputtering is wider.
Owner:JIANGSU CHIYU TECH CO LTD

High-crystallinity TCO film and preparation method thereof

The invention belongs to the technical field of TCO thin film preparation, and discloses a high-crystallinity TCO thin film and a preparation method thereof.The preparation method of the high-crystallinity TCO thin film comprises the following steps that 1, the TCO thin film is deposited under the condition that the substrate temperature is 100-200 DEG C through a low-temperature magnetron sputtering method; 2, carrying out first annealing treatment on the TCO thin film in a nitrogen environment at the annealing temperature of 300-400 DEG C; and 3, carrying out secondary annealing treatment on the TCO thin film subjected to the primary annealing treatment in an oxygen environment at the annealing temperature of 180-400 DEG C to obtain the high-crystallinity TCO thin film. The invention discloses a preparation method of a high-crystallinity TCO film, sputtering deposition is performed at a specific substrate temperature to obtain the TCO film, and then a specific annealing process is matched, so that the crystallinity of the TCO film is effectively improved, and the optical and electrical properties are improved.
Owner:FIRST RARE MATERIALS CO LTD

Multi-layer flexible radiation cooling composite diaphragm

The invention discloses a multi-layer flexible radiation cooling composite diaphragm which structurally comprises a flexible base layer film, and a SiO2 inorganic coating, a first layer of polyvinylidene fluoride (PVDF), a nano-silver layer deposited by magnetron sputtering and a second layer of PVDF which are sequentially coated to form a base layer film / SiO2 / PVDF / Ag / PVDF sandwich structure. The SiO2 layer is prepared through a sol-gel method, the surface roughness is smaller than 2 nm, and the visible light transmittance is larger than 95%; the thickness of the silver layer is 50 + / -5 nm, and the total thickness of SiO2 / PVDF / Ag does not exceed 150 nm. According to the composite diaphragm, ultraviolet reflection, visible light high transmission (greater than 92%) and near-infrared high reflection (greater than 88%) are realized through spectrum selective regulation and control, and meanwhile, SiO2 and PVDF synergistically enhance the infrared emissivity of an atmospheric window wave band (8-13 [mu] m). The flexible PET base material is combined with the PVDF interlayer design to restrain silver layer oxidation and interface stripping, the recovery rate is larger than 95% after 1000 times of bending circulation, and the NIR reflectivity attenuation is smaller than or equal to 5%. The composite diaphragm disclosed by the invention has the advantages of high light transmission, efficient cooling, excellent flexibility and long-term stability, and is suitable for flexible scenes such as agricultural greenhouses and the like.
Owner:NANJING UNIV +1

Method for prolonging service life of resistance spot welding electrode, manufactured resistance spot welding electrode cap and application

The invention discloses a method for prolonging the service life of a resistance spot-welding electrode, a manufactured resistance spot-welding electrode cap and application, and the method comprises the following steps: taking a chromium-zirconium-copper electrode cap as a base body, grinding the working surface of the base body step by step by adopting abrasive paper, and then sequentially polishing, ultrasonically cleaning and drying to obtain a pretreated base body; performing vacuum zirconium permeation treatment on the pretreated matrix by adopting a permeation agent so as to form a zirconium-rich solid solution diffusion layer in the pretreated matrix, thereby obtaining the matrix subjected to zirconium permeation reinforcement; physical vapor deposition treatment is adopted, and a metal transition layer is deposited on the surface of the solid solution diffusion layer of the matrix subjected to zirconium permeation strengthening; wherein the metal transition layer is a Cr transition layer or a Ti transition layer; and a graphite target and titanium target co-sputtering mode is adopted, and a composite gradient functional layer is sputtered and deposited on the surface of the metal transition layer of the matrix treated in the step S3. The electrode service life of the method is improved by magnitude order, and the effect is extremely remarkable.
Owner:BENGANG STEEL PLATES CO LTD

Short-process preparation method of Cu-Ag-Be-Mg composite strip for photomultiplier

The invention discloses a short-process preparation method of a Cu-Ag-Be-Mg composite strip for a photodynode, and relates to a preparation method of a Cu-Ag-Be-Mg composite strip for a photodynode. The invention aims to solve the problems that the traditional strip preparation process is long, the energy consumption is high, the production efficiency is low, and a composite film layer prepared by sputtering, deposition and other methods is low in interface bonding force, short in service life and the like. The method comprises the following steps: 1, smelting; 2, semi-continuous casting; 3, homogenization treatment; 4, hot die forging; 5, heat treatment; 6, cold rolling; 7, surface treatment; 8, finish rolling; and 9, rolling. The method is different from a traditional large ingot casting and large rolling deformation equal-length process technology, after semi-continuous casting and homogenizing heat treatment are adopted, hot die forging is directly carried out, the thin-wall cylindrical part is obtained, finish rolling deformation is directly carried out after unfolding, the preparation process is shortened, and the production efficiency is improved. According to the preparation method, the Cu-Ag-Be-Mg composite strip for the photomultiplier can be obtained.
Owner:XIANGTAN UNIV

Method for preparing silicon alloy negative electrode based on three-dimensional spin control magnetron co-sputtering

The invention belongs to the technical field of lithium ion battery negative electrode material preparation, and relates to a method for preparing a silicon alloy negative electrode based on three-dimensional spin control magnetron co-sputtering, which comprises the following steps: 1, substrate preparation: selecting carbon particles as a negative electrode material substrate; 2, particle three-dimensional spinning suspension: placing the carbon particles in a three-dimensional spinning suspension device, and continuously rolling and rotating in a plurality of space directions in a high vacuum environment; 3, sputtering target material configuration, wherein a silicon target and at least one alloy metal target are arranged in a magnetron co-sputtering cavity; 4, co-sputtering deposition: performing magnetron co-sputtering on the rotating carbon particles in a high-purity argon working atmosphere, and dynamically adjusting the input power of each target to enable a deposition coating to form a gradient composite alloy structure from a rich metal buffer layer to a high-silicon content region to obtain a composite powder material; the high silicon content is guaranteed, meanwhile, a buffer alloy phase and an interface bonding layer are introduced, and the problems of volume expansion and interface stripping in the circulation process are effectively solved.
Owner:XI AN JIAOTONG UNIV

Vacuum sputtering preparation process of multi-layer gradient color film for streaming media rearview mirror cover plate

The invention discloses a vacuum sputtering preparation process of a multi-layer gradient color film for a streaming media rearview mirror cover plate, and belongs to the technical field of magnetron sputtering coating. The process depends on vacuum sputtering equipment comprising an upper sheet translation table, an upper sheet table, a sheet inlet chamber, a front fine extraction chamber, a front buffer chamber, a first coating chamber, a transition chamber, a second coating chamber, a rear buffer chamber, a rear fine extraction chamber, a sheet outlet chamber, a lower sheet table, a lower sheet translation table and the like. The method comprises the steps of glass substrate pretreatment, vacuum buffer stabilization, preparation of an aluminum layer and a silicon-aluminum alloy layer in a first coating chamber, stress release in a transition chamber, preparation of an aluminum-nitrogen oxide layer in a second coating chamber, post buffer stabilization, sheet discharging and discharging and the like. The technical effects that the color is continuously adjustable, the adhesive force of the film layer is high, the optical and electrical properties are balanced, and the production efficiency is high are achieved.
Owner:FOSHAN JINGBO TECH CO LTD

Preparation method and application of magnetron sputtering high-entropy nitriding composite coating

The invention provides a preparation method and application of a magnetron sputtering high-entropy nitriding composite coating, and belongs to the technical field of surface treatment.The preparation method comprises the steps that a TiZrNbTaW alloy target material is prepared, and the alloy target material is obtained through a powder metallurgy method; substrate treatment, wherein the substrate treatment comprises the steps of grinding and polishing a titanium substrate to be in a mirror surface state and performing ultrasonic cleaning; and the magnetron sputtering deposition process comprises the steps that a deposition chamber is vacuumized to a preset vacuum degree, a substrate is heated, surface impurities are removed through pre-sputtering, nitrogen is introduced under the condition of fixed power, a TiZrNbTaW coating and a TiZrNbTaWN 0.75 nitridation coating are alternately deposited, and the TiZrNbTaW Nx composite coating is formed. The method overcomes the defect of high cost of an existing precious metal protective coating in the field of proton exchange membrane electrolyzed water, provides a protective coating with corrosion resistance and conductivity, and is suitable for being applied to large-scale industrial production.
Owner:NORTH CHINA ELECTRIC POWER UNIV

Multispectral coating method for linear gradual filter and linear gradual filter

The invention provides a multispectral coating method for a linear gradual change optical filter and the linear gradual change optical filter, and the method comprises the steps: S1, putting optical glass into a cleaning agent for ultrasonic cleaning, and obtaining a substrate of the linear gradual change optical filter to be coated; s2, putting the substrate into a reaction cavity of a radio frequency magnetic control instrument, closing the reaction cavity, and setting environmental parameters of multispectral coating; s3, under the environmental parameters, sputtering and depositing target materials on the surface of the substrate by adopting double-target-position radio frequency magnetic control, using SiO2 and Si as the target materials for the double target positions respectively, and switching to use different target positions to alternately carry out sputtering deposition of the target materials by adjusting the power interval of the radio frequency magnetic control; and S4, closing the radio frequency magnetic control instrument, keeping the reaction cavity closed, naturally cooling to a preset cooling temperature, opening the reaction cavity, and taking out the coated substrate as the linear gradual change optical filter. The process is simple, and the optical filter finished product is good in infrared spectrum performance and suitable for various scenes.
Owner:SHENZHEN WAYHO TECH

Method for promoting matching of thermal expansion coefficients of glass through hole substrate and copper by magnetron sputtering boride doped metal barrier layer

The invention discloses a method for promoting matching of thermal expansion coefficients of a glass through hole substrate and copper through magnetron sputtering of a boride-doped metal barrier layer, which comprises the following steps of: after carrying out ultrasonic cleaning and oxygen plasma treatment on the glass through hole substrate, co-sputtering and depositing the boride-doped metal barrier layer on the substrate in a vacuum environment and inert gas; and finally, sputtering and depositing metal Cu on the substrate, wherein the metal is any one of Ag, Ti, Cr and Bi. According to the invention, the multi-target co-sputtering technology is adopted, and the metal-doped ZrB2 thin film is introduced to relieve the thermal expansion coefficient difference between the Cu thin film and the glass substrate so as to promote the thermal expansion coefficient matching between the glass through hole substrate and the copper layer, so that the generation of residual stress in the copper electroplating process is reduced, and the warping phenomenon of the copper film is prevented. The boride doped metal disclosed by the invention has excellent conductivity and dielectric constant, so that an electromagnetic coupling effect does not occur in a signal transmission process, and the integrity of the signal is ensured.
Owner:LANZHOU JIAOTONG UNIV

Magnesium alloy with composite low-absorption coating and preparation method thereof

The invention relates to the technical field of space functional coatings, and discloses a magnesium alloy with a composite low-absorption coating and a preparation method of the magnesium alloy. The magnesium alloy comprises a magnesium alloy matrix, a micro-arc oxidation layer serving as a bottom coating and a magnetron sputtering deposition reflecting film serving as a surface coating. The phase of the micro-arc oxidation layer comprises SiO2, ZrO2, ZnO and MgO, and the phase of the magnetron sputtering deposition reflecting film comprises Si and SiO2. The invention provides a magnesium alloy with a multi-layer gradient composite low-absorption coating, which comprises a progressive gradient distribution multi-layer stacked strong-reflection micro-arc oxidation layer and a magnetron sputtering deposition reflecting film, and according to the stacking synergistic effect of the multifunctional coating and the thin film interference principle, the multi-layer gradient composite low-absorption coating is prepared. The magnesium alloy composite coating with multiple functional film layers connected in series for collaborative optimization is formed, excellent comprehensive performance is shown in the aspects of low absorption and corrosion resistance, and in addition, the coating also has excellent stability and space environment adaptability.
Owner:BEIJING XCHD SCI & TECH DEV CO LTD +1

Layout design method for high-precision magnetron sputtering deposition equipment

The invention provides a layout design method for high-precision magnetron sputtering deposition equipment. The method comprises the following steps: firstly, determining sputtering deposition subsystem layout parameters such as revolution radius, target-base distance, target length and the like according to an optimized target difference value of a to-be-plated element parameter, a target preliminary sputtering yield parameter and a film thickness; then, whether the film thickness distribution under the layout parameters meets an optimization target difference value or not is evaluated; and finally, vacuum chamber subsystem layout parameters such as the diameter and the height of the vacuum chamber are calculated. According to the method, a quantitative design mode is adopted, the problems that existing magnetron sputtering deposition equipment layout design depends on experience, and whether the magnetron sputtering deposition equipment meets design index requirements or not is difficult to evaluate are effectively solved, and the scientificity and rationality of equipment layout are improved.
Owner:SHANGHAI INST OF OPTICS & FINE MECHANICS CHINESE ACAD OF SCI

Preparation method of ultra-smooth nanocrystalline tungsten coating on surface of emitter

The invention discloses a preparation method of an ultra-smooth nanocrystalline tungsten coating on the surface of an emitter, the tungsten coating is prepared by adopting a magnetron sputtering method, and the specific process is as follows: pretreating an emitter workpiece, then placing the emitter workpiece in a vacuum chamber, pre-vacuumizing, then introducing inert gas, cleaning the surface of the emitter workpiece by utilizing gas ion reverse sputtering, and finally removing the surface of the emitter workpiece. And then adjusting the gas pressure, bombarding and cleaning the surface of the emitter workpiece by using metal ions, and finally sputtering and depositing to form the tungsten coating. The tungsten coating is prepared through the magnetron sputtering technology, the tungsten coating has the characteristics of being compact in structure, good in combination and uniform and smooth in surface, the mechanical property and structural stability of the tungsten coating in the high-temperature service environment can be guaranteed, the deposition technology is simple, the preparation efficiency is high, and the tungsten coating is green and free of pollution, in addition, preparation of the tungsten coating composed of different phases can be achieved, and the application prospect is wide. The application requirements in the fields of electronic industry, nuclear industry and the like are met.
Owner:NORTHWEST INSTITUTE FOR NONFERROUS METAL RESEARCH

Surface treatment method for improving corrosion resistance of 8Cr4Mo4V steel bearing

The invention discloses a surface treatment method for improving the corrosion resistance of an 8Cr4Mo4V steel bearing, and aims to solve the problems of poor binding force and limited improvement of the corrosion resistance in an existing bearing steel surface treatment process. The surface treatment method comprises the following steps: 1, ultrasonically cleaning a bearing steel workpiece; secondly, argon is excited through radio frequency to form plasma, and the bearing steel workpiece is subjected to etching treatment; 3, adopting radio frequency to excite nitrogen to form plasma, and performing nitrogen ion implantation treatment to form a pretreatment layer; 4, performing chromium layer deposition on the bearing steel workpiece by adopting a magnetron sputtering process; 5, adopting radio frequency to excite nitrogen to form plasma, and performing nitrogen ion implantation treatment; and 6, the magnetron sputtering treatment and the nitrogen ion injection chromium layer treatment are repeated for multiple times. According to the method, the composite coating is generated on the surface through alternate magnetron sputtering deposition of chromium and nitrogen ion implantation, each layer is composed of dispersed nanocrystalline Cr, CrN and Cr2N, and the corrosion resistance and the surface hardness of the bearing steel are remarkably improved.
Owner:HARBIN INST OF TECH

Automatic temperature control system and method for sputtering deposition device

The invention belongs to the technical field of sputter deposition, and provides an automatic temperature control system and method for a sputter deposition device, and the system realizes the accurate control of the cavity temperature in the sputter deposition process by integrating components such as a vacuum gauge, a gas cylinder, a valve, a thermocouple temperature measurement element and a PID (Proportion Integration Differentiation) regulator. The system monitors the temperature of the cavity in real time by using the thermocouple, and automatically adjusts the power of the heating wire through the PID regulator according to the comparison result of a set value and an actual value, thereby maintaining the stability of the temperature of the cavity. In addition, the system has the function of communicating with an upper computer, remote monitoring and control can be carried out through a software layer, and the automation level and the temperature control precision of the sputtering deposition process are improved. The problems that in the prior art, temperature control precision is low, the automation degree is insufficient, and stability is poor are solved, through linkage control over the temperature, the vacuum degree and the gas flow, the consistency of film performance is guaranteed, and the method is suitable for large-scale production of high-precision films.
Owner:ZHONGBEI UNIV

A physical vapor deposition apparatus, an electrochromic device, and a method of manufacturing the same

The application discloses a physical vapor deposition device, an electrochromic device and a preparation method thereof, and relates to the technical field of electrochromic devices. The preparation method comprises the following steps: sputtering and depositing an electrochromic layer of WO3 on the surface of a first ITO layer, and the oxygen content is any value in the range of 42.5% to 52.5%; sputtering and depositing a pre-set thickness of a tungsten oxide ion conduction layer on the electrochromic layer, and the oxygen content of the corresponding chamber is any value in the range of 35% to 45%; sputtering and depositing an ion storage layer containing lithium ions on the ion conduction layer; depositing a second ITO layer on the ion storage layer, and obtaining the electrochromic device after vacuum annealing treatment and cooling treatment; wherein the deposition temperature of the second ITO layer is any value in the range of 350 DEG C to 400 DEG C, and the annealing temperature of the vacuum annealing treatment is any value in the range of 450 DEG C to 500 DEG C. The electrochromic device prepared by the application has the characteristics of high transmittance and low sheet resistance.
Owner:SUZHOU BEARSUNNY TECHNOLOGIES INC

Packaging method for reducing RDSON resistance value of chip based on multi-layer metal structure

The invention discloses a packaging method for reducing the RDSON resistance value of a chip based on a multi-layer metal structure, and relates to the technical field of chip packaging, a chip packaging structure based on the multi-layer metal structure comprises a chip base layer, a multi-layer metal layer and an electroplated layer which are arranged in a linear direction, and the multi-layer metal layer comprises an adhesion layer, a connection layer and a combination layer; comprising the following steps that cleaning pretreatment is conducted in a plasma cleaning mode, variation detection and analysis are conducted, and first-step variation analysis and / or second-step variation analysis are / is conducted after detection data are obtained; sputtering deposition of the multiple metal layers is carried out through the physical vapor deposition technology, and sputtering parameters are intelligently adjusted; coating photoresist on the surface of the top end of the multi-layer metal layer, and performing exposure and development; depositing thick copper by using an electroplating process; according to the method, the deposition quality of each metal layer can be improved, so that the stability and the performance of the multi-layer metal structure are ensured.
Owner:WUXI QIANYE MICRO NANO TECH CO LTD

Sputtering deposition equipment and method

Certain examples described herein relate to a sputter deposition apparatus that includes a substrate holding device, a target loading device, a plasma source for generating a plasma, and a magnet arrangement. The substrate holding device is configured to position a substrate in a sputter deposition zone for sputter depositing target material from a first target onto the substrate in use. The target loading device is configured to move a second target from a target activation zone to the sputter deposition zone for sputter depositing target material from the second target onto the substrate in use. The magnet arrangement is configured to confine the plasma within the apparatus to the target activation zone and the sputter deposition zone. Within the target activation zone, the respective target is exposed to the plasma in use. The sputter deposition zone provides for sputter deposition of the target material.
Owner:DYSON TECH LTD

Sputter deposition

To provide a sputter deposition apparatus.SOLUTION: A sputter deposition apparatus (100) comprising a remote plasma generating arrangement (106) arranged to provide a plasma (120) for sputter depositing a target material (102) in a sputter deposition region (112), a confining arrangement arranged to provide a confining magnetic field to substantially confine the plasma to the sputter deposition region, a substrate (104) provided in the sputter deposition region, and one or more target support assemblies (108) arranged to support one or more targets in the sputter deposition region to effect sputter deposition of the target material on the substrate, wherein the confinement arrangement confines the remote plasma to the target support assembly such that, in use, target material is deposited as a first region on the substrate, target material is deposited as a second region on the substrate, and an intermediate region between the first region and the second region is free of target material. 2.SELECTED DRAWING: Figure 1
Owner:DYSON TECH LTD

A preparation method of an ultra-low on-resistance MOS transistor based on an SGT process

The application relates to a preparation method of an ultra-low on-resistance MOS tube based on an SGT process, and relates to the technical field of semiconductors; the method comprises the following steps: performing nitrogen source doping deposition on a substrate to form an N-type drift layer; sequentially growing a gallium nitride buffer layer and an aluminum gallium nitride barrier layer on the N-type drift layer, and cooling to room temperature to form a heterojunction; coating a positive photoresist and exposing to define a three-dimensional groove, then developing with a developing solution after hard baking to form a mask, and etching the three-dimensional groove; performing segmented injection in the main groove to form a gradually-changing super junction and performing high-temperature annealing treatment, performing high-dosage arsenic ion injection to form an N + region, depositing aluminum oxide gate medium, magnetron sputtering deposition of titanium nitride to completely fill the groove, then polishing, and then performing electrode preparation, passivation and metal interconnection; gradient doping epitaxy technology is used to realize gradient optimization of the resistance of the drift region, and a three-dimensional cross-groove array is defined on the surface of the heterojunction layer, so that the on-resistance is less than or equal to 5 m omega*mm2 when the breakdown voltage is greater than or equal to 650 V, which is reduced by more than 40% compared with the traditional SGT process.
Owner:深圳辰达半导体有限公司

Phase shift mask substrate and dynamic magnetron sputtering preparation method thereof

The invention relates to a phase shift mask substrate and a dynamic magnetron sputtering preparation method thereof, a MoSi-based gradient film layer is continuously and dynamically deposited on the substrate, and the method comprises the following steps: carrying out first-stage deposition on the substrate by adopting a molybdenum-silicon alloy target so as to form a transition layer; carrying out second-stage deposition on the transition layer to form a main body functional layer through deposition; and third-stage deposition is carried out on the main body functional layer to form a surface modification layer through deposition, and the MoSi-based gradient film layer is obtained. The invention provides a one-step sputtering deposition method capable of dynamically and accurately regulating and controlling, so that the inherent contradiction between the performance and the stress of a single-layer uniform film is fundamentally solved, and the complexity and the uncertainty of a traditional multi-step process are avoided.
Owner:SHAOXING XINLIAN SEMICON TECH CO LTD

Optical device and manufacturing method therefor

An optical device includes, in sequence, a surface formed of a metal oxide, a samarium oxide-containing layer in contact with the surface formed of a metal oxide, and a magnesium fluoride-containing layer in contact with the samarium oxide-containing layer so as to suppress optical absorption resulting from high-rate sputter deposition of a magnesium fluoride-containing layer on a surface formed of a metal oxide.
Owner:CANON KK

Method and system for measuring net sputter deposition rate of hall thruster

The application provides a Hall thruster net sputtering deposition rate measurement method and system, and relates to the technical field of thrusters, comprising: obtaining a first initial mass corresponding to a first test piece, a second initial mass corresponding to a second test piece, and a ring cylinder initial mass corresponding to a thin-walled ring cylinder placed at the same height of the Hall thruster; obtaining a first final mass corresponding to the first test piece and a ring cylinder final mass corresponding to the thin-walled ring cylinder in the case that the Hall thruster is operated based on a first measurement condition; obtaining a second final mass corresponding to the second test piece in the case that the Hall thruster is operated based on a second measurement condition; and determining a net sputtering deposition rate measurement result corresponding to the Hall thruster based on the initial masses and the final masses. The application can simplify the measurement process of the net sputtering deposition amount and the required equipment requirements, and improve the measurement accuracy of the net sputtering deposition amount.
Owner:BEIHANG UNIV

Manufacturing process for solar control and / or low-emissivity glazing, transparent to radio frequencies: cracked sol-gel overcoat

The present invention relates to a method for manufacturing a glass article comprising the following steps: - the provision of a glass substrate, - the deposition, on at least one face of said glass substrate, of a stack of layers comprising at least one functional metallic layer containing silver, each of said layers being deposited by magnetic field assisted sputtering, - the application of a sol-gel solution comprising at least one silicon oxide precursor and / or at least one transition metal oxide precursor, said solution being applied over said stack of layers, so as to form a sol-gel layer having an average thickness of between 50 nm and 3000 nm, preferably between 70 nm and 1500 nm, - the heat treatment at a temperature above 500°C, preferably between 540°C and 700°C, so as to crack the sol-gel layer and damage the stack of layers.The present invention also relates to a glass article that can be obtained by such a process which comprises a glass substrate coated on at least one of its faces: - with a stack of layers comprising at least one functional metallic layer containing silver, and - with at least one sol-gel layer located above said stack of layers and having an average thickness between 50 nm and 3000 nm, preferably between 70 nm and 1500 nm, said stack of layers and said sol-gel layer having cracks or fissures.
Owner:SAINT GOBAIN VITRAGE SA

Physical vapor deposition equipment, electrochromic device and preparation method of electrochromic device

The invention discloses physical vapor deposition equipment, an electrochromic device and a preparation method of the electrochromic device, and relates to the technical field of electrochromic devices. The preparation method comprises the following steps: sputtering and depositing the WO3 electrochromic layer on the surface of the first ITO layer, wherein the oxygen content is any one of 42.5-52.5%; sputtering and depositing a tungsten oxide ion conducting layer with a preset thickness on the electrochromic layer, wherein the oxygen content of the corresponding chamber is any one of 35%-45%; sputtering and depositing an ion storage layer containing lithium ions on the ion conduction layer; a second ITO layer is deposited on the ion storage layer, and the electrochromic device is prepared after vacuum annealing treatment and cooling treatment; wherein the deposition temperature of the second ITO layer is any one value from 350 DEG C to 400 DEG C, and the annealing temperature of the vacuum annealing treatment is any one value from 450 DEG C to 500 DEG C. The electrochromic device prepared by the invention has the characteristics of high transmittance and low sheet resistance.
Owner:SUZHOU BEARSUNNY TECHNOLOGIES INC

A zirconium-based fuel cladding surface corrosion-resistant interface integrated Zr x O / SiC multilayer composite coating and preparation method thereof

The present invention discloses a zirconium-based fuel cladding surface corrosion-resistant interface integrated Zr x O / SiC multilayer composite coating and preparation method thereof, the method comprising: first, pre-oxidizing the zirconium-based fuel cladding to in-situ grow Zr x O oxide film; second, Ar plasma sputtering activation of the pre-oxidized zirconium-based fuel cladding; third, alternating deposition to form a multi-layered SiC composite coating. The present invention combines pre-oxidation with magnetron sputtering deposition, and constructs a Zr in situ growth from the matrix Zr x O and then to the gradient composite structure coating of the surface SiC composite coating, which reduces the thermal mismatch and interface thermal resistance between the base metal and the ceramic coating, enhances the interface adaptability between the base and the SiC composite coating, and with the help of the high corrosion resistance, high thermal conductivity and high hardness of the SiC composite coating, the surface corrosion resistance and wear resistance of the fuel cladding under normal and accident conditions are improved simultaneously, and the fault tolerance of the zirconium-based cladding under accident conditions is optimized.
Owner:NORTHWEST INSTITUTE FOR NONFERROUS METAL RESEARCH