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999 results about "Ceramic sintering" patented technology

Sintering of ceramics. Sintering (Firing) of ceramic materials is the method involving consolidation of ceramic powder particles by heating the “green” compact part to a high temperature below the melting point, when the material of the separate particles difuse to the neghbouring powder particles.

Aluminum oxide ceramic substrate with high heat conductivity and preparation method thereof

The invention discloses an aluminum oxide ceramic substrate with high heat conductivity. The aluminum oxide ceramic substrate is prepared by steps of stirring a ceramic powder material, a binder, a plasticizer, a dispersant and a solvent uniformly, preparing a ceramic raw-ceramic substrate through a tape casting method, glue discharging and sintering. The aluminum oxide ceramic substrate is characterized in that the solvent is a mixture of butanol, isopropanol and butyl acetate, and the ceramic powder material comprises aluminium oxide powder and auxiliary agents. The invention also discloses a preparation method for the aluminum oxide ceramic substrate with the high heat conductivity. According to the aluminum oxide ceramic substrate and the preparation method, the solvent system which comprises the butanol, the isopropanol and the butyl acetate are used as the main solvent in place of traditional toluene, thus enhancing dissolution of PVB by the solvent, thereby guaranteeing uniformity of raw ceramic slurry, making physical properties of sintered ceramic stable, reducing environmental influences of the exhausted gas during production processes compared to traditional modes of production, contributing to energy conservation and emission reduction, and reducing the cost.
Owner:NANJING ZHONGJIANG NEW MATERIAL TECH

Method for preparing zirconium oxide refractory fibre

The present invention provides a method for preparing a zirconium oxide refractory fiber. The method adopts zirconium oxychloride, aqueous hydrogen peroxide solution, yttrium chloride or yttrium nitrate as raw material, the inorganic zirconium spinnable glue solution is made by reaction and compression, the gelatinous fiber can be obtained by centrifugal fiber forming, and after heat treating sintering the zirconium oxide refractory fiber which has the following advantages can be obtained: crystal phase composition with square phase and/or cubic phase zirconium oxide, purity up to 99.5% above, diameter around 5 mu m, length approximate continuous, soft and flexible property and without slag including sphere. The using temperature of the fiber is above 1600 DEG C, the material can be used as extreme temperature refractory, heat insulation material, protecting material, ablative material, satellite battery separator material and the like, used for the fields of aerospace, war industry and national defense, atomic energy and the like; the fiber can also be used as the flame-proof heat-insulating material of the extraordinary high-temperature electric furnace with temperature 1600 DEG C to 2200 DEG C, the oil or gas burning furnace and other extraordinary high-temperature heating mechanism, and is used for the fields of ceramic sintering, crystal growth, metal smelting, petroleum cracking, scientific researching and the like. The invention totally adopts the inorganic raw material, has the advantages of low cost, no pollution, simple technique and excellent effect.
Owner:山东红阳高温节能材料股份有限公司

Method for preparing Re:YAG polycrystalline transparent ceramic by using different molding modes

InactiveCN102060540ACeramic sinteringLiquid medium
The invention relates to a method for preparing Re:YAG polycrystalline transparent ceramic by using different molding modes, which adopts commercial high-purity Y2O3, Al2O3 and Re2O3 as raw materials, adopts MgO, CaO or TEOS (tetraethyl orthosilicate) as sintering additive, and prepares a raw blank by a cold isostatic pressing, slip casting or tape casting process to react and sinter the transparent polycrystalline Re:YAG ceramic. The method comprises the following steps: mixing and adding the oxides into a liquid medium; adding a certain amount of dispersant, adhesive, plasticizer, pressing agent and defoaming agent, carrying out ball milling, and mixing; treating the slurry under different conditions in different molding modes to obtain the raw blank; and sintering the degreased raw blank in a vacuum furnace. For the Re:YAG ceramic sintering body with thickness of 1.5mm, the transmission rate of straight light in the wavelength of 1064nm is not lower than 80% after the Re:YAG ceramic sintering body is subjected to double-sided polishing. For the raw blank which is prepared by different molding modes and is sintered for 10 hours at 1750 DEG C, sizes of ceramic grains are different, wherein regarding the raw blank prepared by cold isostatic pressing, the average grain of the ceramic is 13.5mu m; regarding the raw blank prepared by slip casting, the average grain of the ceramic is 3.5mu m; and regarding the raw blank prepared by tape casting, the average grain of the ceramic is 1.5mu m.
Owner:FUJIAN INST OF RES ON THE STRUCTURE OF MATTER CHINESE ACAD OF SCI

Bismuth scandate-lead titanate high-temperature piezoelectric ceramic material and preparation method thereof

The invention discloses a bismuth scandate-lead titanate high-temperature piezoelectric ceramic material. The bismuth scandate-lead titanate high-temperature piezoelectric ceramic material comprises a matrix with the chemical formula of xBiScO3-(1-x)PbTiO3 and bismuth trioxide (Bi2O3) in an amount which is less than 0.4 percent of the total weight of the matrix. The bismuth scandate-lead titanate high-temperature piezoelectric ceramic material is prepared by adding excess Bi2O3 into raw materials of Sc2O3, Bi2O3, Pb3O4 and TiO2 in the metering ratio according to the chemical formula of xBiScO3-(1-x)PbTiO3, wherein x is 0.35 to 0.38; and the using amount of the excess Bi2O3 is 0.1 to 0.4 percent of the total weight of the raw materials of Sc2O3, Bi2O3, Pb3O4 and TiO2 in the metering ratio according to the chemical formula of xBiScO3-(1-x)PbTiO3. The bismuth scandate-lead titanate high-temperature piezoelectric ceramic material solves the problems that ceramic sintering temperature is increased and piezoelectric and dielectric properties are reduced due to deviation of a stoichiometric ratio caused by bismuth volatilization in the sintering process of BSPT ceramic, and has high Curie temperature, excellent piezoelectric property and an actual application value in high-temperature electronic equipment. The invention also discloses a preparation method for the bismuth scandate-lead titanate high-temperature piezoelectric ceramic material. In the preparation method, the piezoelectric ceramic material is prepared by synthesizing and sintering at lower temperature, so production cost is reduced, process steps are simplified, and the material has actual application value.
Owner:MORNSUN GUANGZHOU SCI & TECH +1

Ceramic and carbon nano-fiber composite material and preparation method thereof

The invention relates to a ceramic and carbon nano-fiber composite material and a preparation method thereof. The preparation method has a principle of directly growing carbon nano-fiber in a ceramic hole which is formed in a ceramic body in the ceramic forming process to prepare the ceramic and composite material. The specific process comprises the following steps: mixing a metallic catalyst and ceramics; inputting carbonous gas to a system in an intermediate stage of preparing the ceramics by sintering or pyrogenation; directly growing the carbon nano-fiber in the hole by utilizing the metallic catalyst formed in the ceramic hole; and further rising the temperature and sintering or pyrolyzing the ceramics which grows the carbon nano-fiber to prepare the carbon nano-fiber and ceramic composite material. Through the in-situ preparation method, the ceramic composite material with the uniformly-distributed carbon nano-fiber can be prepared. As the growing of the carbon nano-fiber is completed by one step in the process of sintering or pyrolyzing the ceramics, the flow process is simple and controllable, and has the characteristics of low preparation temperature; the composite materials with different shapes and sizes can be prepared; and the flow process can be applied to the preparation of the high-performance fiber reinforced ceramic composite material and in an application field thereof.
Owner:TIANJIN UNIV
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