207 results about "Sintered ceramic" patented technology

The invention belongs to the technical field of ceramic slurry, and particularly relates to ceramic slurry and a preparation method and application thereof.The ceramic slurry comprises inorganic components and organic components, the inorganic components comprise inorganic additives and glass powder, the inorganic additives comprise Al2O3, ZrO2 and Y2O3, and the organic components comprise modified acrylic resin, organic solvent and auxiliaries. By controlling the relative content of carboxyl and ester groups in the modified acrylic resin and utilizing the polarity difference of functional groups, selective adsorption of inorganic powder is realized, so that the dispersion uniformity of the powder in the ceramic slurry is remarkably improved, segregation of yttrium oxide is effectively inhibited, and the service life of the ceramic slurry is prolonged. Therefore, monoclinic-phase zirconium oxide, tetragonal-phase zirconium oxide and cubic-phase zirconium oxide with a proper proportion can be formed in the sintered ceramic substrate, further the bending strength of the ceramic substrate is remarkably improved, and the ceramic substrate is particularly suitable for manufacturing miniaturized and thin electronic components.

The invention relates to the technical field of ceramics, and particularly discloses green special refractory ceramic slurry as well as a preparation method and application thereof. The green special refractory ceramic slurry is prepared from aluminum oxide, methyltrimethoxysilane-phosphoric acid modified polysiloxane, fluorocarbon emulsion, expanded vermiculite powder, silane coupling agent modified feldspar tailing powder, a dispersing agent, an organic silicon defoaming agent, a polyurethane curing agent and deionized water. After being sintered, the green special refractory ceramic slurry provided by the invention has excellent high-temperature stability, corrosion resistance, thermal shock resistance and mechanical strength, and solves the problems of low high-temperature-resistant upper limit and poor corrosion resistance of the traditional slurry, so that the sintered ceramic adapts to severe high-temperature working conditions such as steel plant converter liners and chemical high-temperature reaction kettle inner walls; and long-term protection requirements of industrial equipment are met.

The invention discloses a low-temperature sintered microwave dielectric ceramic material and a preparation method thereof, and belongs to the technical field of electronic materials. The composite material comprises the following raw materials: CaCO3, SrCO3, Bi2O3 and B2O3. The preparation method comprises the following steps: burdening and weighing according to a stoichiometric ratio CaxSr1-xBi2B2O7 (x is more than 0.1 and less than 0.9), then carrying out ball milling and mixing, pre-sintering to obtain pre-sintered ceramic powder, adding an organic material to prepare stable slurry, carrying out tape casting to obtain a green body, and sintering to obtain the low-temperature sintered microwave dielectric ceramic material. The sintering temperature of the ceramic material is 700-800 DEG C, the dielectric constant range is 4-8, the loss value is less than 0.00002, and the ceramic material has low dielectric constant and ultrahigh quality factor. The problems that an existing low-temperature sintering microwave dielectric ceramic material is high in water absorption and high in material cost are solved. The microwave ceramic dielectric is applied to the technical field of electronic components requiring low dielectric constant and low loss value microwave ceramic dielectric.

Proppant particles formed from slurry droplets and methods of use are disclosed herein. The proppant particles can include a sintered ceramic material and can have a size of about 80 mesh to about 10 mesh and an average largest pore size of less than about 20 microns. The methods of use can include injecting a hydraulic fluid into a subterranean formation at a rate and pressure sufficient to open a fracture therein and injecting a fluid containing a proppant particle into the fracture, the proppant particle including a sintered ceramic material, a size of about 80 mesh to about 10 mesh, and an average largest pore size of less than about 20 microns.

Disclosed is a pre-sintered ceramic block for a dental restoration, which has a low pre-sintering temperature, contains a silica main crystal phase, but does not contain or contains a small amount of lithium metasilicate crystal phase. The pre-sintered ceramic block has a low hardness, with a Vickers hardness of 0.5-3 GPa, which is significantly lower than that of a ceramic block containing a lithium metasilicate crystal phase, and same is suitable for dry machining and also wet machining when being machined into a dental restoration.

The invention discloses a high-durability multifunctional composite material for landscape architecture and a preparation method of the high-durability multifunctional composite material, and relates to the technical field of outdoor wood composite materials. Thermoplastic, plant fibers, a hydrophobic agent, a compatilizer and a composite antioxidant are blended to prepare a hydrophobic modified wood-plastic composite material, and the hydrophobic modified wood-plastic composite material is used as a core layer; the preparation method comprises the following steps: blending a wood unit, a low-temperature sintered ceramic precursor, nano titanium dioxide and an inorganic binder to prepare a photocatalyst-loaded microporous ceramic-wood composite material, and forming a functional surface layer of the photocatalyst-loaded microporous ceramic-wood composite material; according to the high-durability multifunctional composite material for the landscape architecture, synchronous co-extrusion is utilized, the surface of the core layer is coated with the functional surface layer, curing and shaping are conducted, and the high-durability multifunctional composite material for the landscape architecture is obtained and is a novel landscape material which integrates high durability, long service life, low maintenance, environment friendliness and aesthetic value and can actively keep the surface clean.

A method of manufacturing ceramic tape includes a step of directing a tape of partially-sintered ceramic into a furnace. The tape is partially-sintered such that grains of the ceramic are fused to one another yet the tape still includes at least 10% porosity by volume, where the porosity refers to volume of the tape unoccupied by the ceramic. The method further includes steps of conveying the tape through the furnace and further sintering the tape as the tape is conveyed through the furnace. The porosity of the tape decreases during the further sintering step.

The invention relates to a sintered ceramic body having a large size and a method for manufacturing the same. The method comprises the following process steps: providing a ceramic powder (5) within an internal volume of a spark plasma sintering tool (1), wherein the tool comprises: a mold (2); upper and lower punches (4, 4 ') creating a gap (3) between the punches and the inner wall when at least one of the punches moves within the internal volume; creating a vacuum condition within the interior volume; moving at least one of the punches to apply pressure to the ceramic powder while heating, and sintering; and reducing the temperature of the sintered ceramic body.

The invention provides a carbon ceramic vessel and a preparation method thereof.The preparation method of the carbon ceramic vessel comprises the steps that a ceramic body is subjected to first-time polishing treatment, and the polished ceramic body is obtained; carrying out sintering molding on the polished ceramic green body to obtain a sintered ceramic green body; carrying out liquid carburization and gas carburization on the sintered ceramic body to obtain a ceramic body of which at least part of pores contain a carbon film; and carrying out secondary polishing treatment on the ceramic green body containing the carbon film in at least part of pores to obtain the carbon ceramic vessel. According to the preparation method of the carbon ceramic vessel, through liquid carburization and gas carburization, a large number of carbon films can be formed in pores of the ceramic body, the water absorption rate of the ceramic body is greatly reduced, and the heat transfer performance is improved; and meanwhile, through two times of polishing treatment, the surface roughness and surface pores of the carbon ceramic ware can be reduced, and the carbon ceramic ware is glossy and better in appearance effect.

This invention discloses a selective roughening method for ceramic copper-clad laminates, comprising the following preparation steps: S1 printing an active solder layer between ceramic and copper foil; S2 preparing the ceramic copper-clad laminate; S3 etching copper onto the sintered ceramic copper-clad laminate; S4 removing unwanted solder layers; S5 cleaning, roughening, cleaning, acid washing, cleaning, immersion, and drying the patterned ceramic copper-clad laminate according to the following process, and filling it with nano-silicon and organosilane; S6 printing a thermosetting wet film to expose the area to be surface treated; S7 removing the surface roughening structure; S8 finally, subjecting the ceramic copper-clad laminate to nickel plating, chemical silvering, and then stripping to form the final structure. Compared with the prior art, this invention has the following beneficial effects: effectively avoiding the problem of solder voids caused by surface roughening pits, good surface weldability, and the concave structure of the welding area effectively prevents solder overflow during the welding process and reduces micropores in the chemical silver plating layer.

The invention provides a low-smoke halogen-free high-flame-retardant power cable and a preparation method thereof, and the low-smoke halogen-free high-flame-retardant power cable comprises a conductor, an insulating layer and a sheath layer. The sheath layer is prepared from the following raw materials: 25 to 40 parts of ethylene-vinyl acetate copolymer, 15 to 25 parts of linear low-density polyethylene, 5 to 15 parts of metallocene polyethylene, 8 to 15 parts of reactive phosphorus-nitrogen-silicon hybrid compatibilizer, 12 to 22 parts of low-temperature sintered ceramic composite powder, 30 to 45 parts of surface-treated magnesium hydroxide, 15 to 25 parts of surface-treated aluminum hydroxide, 3 to 6 parts of organic modified montmorillonite and 1.5 to 2.5 parts of triallyl isocyanurate. 1.0 to 2.0 parts of a composite antioxidant, 1.0 to 2.5 parts of a calcium-zinc stabilizer and 0.5 to 1.5 parts of silicone master batch. The prepared low-smoke halogen-free high-flame-retardant power cable has excellent flexibility, mechanical property, heat resistance and processability, is stable in flame retardant property and stable in size, and is suitable for safety protection of power cables.

The invention relates to a preparation method of conductive ceramic Mg3Ga2GeO8 for an all-solid-state battery, and belongs to the technical field of all-solid-state batteries. The preparation method mainly comprises the following steps: roasting MgO, Ga2O3 and GeO2 powder in an air atmosphere, adding a solvent, and drying after ball milling; adding the primary sintered ceramic wafer and a binder into a solvent, grinding, drying, tabletting, and carrying out air burning at 1200-1400 DEG C to obtain a primary sintered ceramic wafer; and crushing and grinding the primarily sintered ceramic chip, taking powder, and repeatedly sintering for 2-3 times to obtain the Mg3Ga2GeO8 ceramic chip with a compact structure and a single phase. The ionic conductivity of the prepared ionic conductive oxide Mg3Ga2GeO8 is high, the ionic conductivity reaches 10 <-5 > S / cm at 25 DEG C, the activation energy is as low as 0.80 eV, the process is simple, and the method is suitable for industrial production.

The utility model relates to the technical field of vacuum arc extinguish chambers, in particular to a vacuum arc extinguish chamber shielding cylinder fixing structure which comprises a shell, a shielding cylinder and a plurality of movable parts, the shell is provided with a vacuum cavity, the cavity wall of the vacuum cavity is provided with a first protruding part, and the side wall of the shielding cylinder is provided with a second protruding part. The second protruding part abuts against one end of the first protruding part, and each movable part is in threaded connection with the shielding cylinder, extends out of the outer side wall of the shielding cylinder by a preset distance and abuts against the other end of the first protruding part. And the movable piece abuts against the first protruding part, so that the protrusion with the adjustable extending length is achieved, and the shielding cylinder is prevented from shaking and making abnormal sounds.

The application discloses a preparation method of a high-strength aluminum nitride substrate and relates to the technical field of aluminum nitride substrate preparation. The method comprises the following steps: preparing modified aluminum nitride powder; adding a non-oxygen composite sintering aid composed of fluorides and borides to the modified aluminum nitride powder to obtain a mixture; the adding amount of the composite sintering aid is 0.5wt%-5wt% of the total mass of the modified aluminum nitride powder; the mixture, a binder and a dispersant are mixed in a planetary ball mill to obtain a uniform slurry; the slurry is subjected to flow casting to form a green porcelain embryo, and then, glue removal treatment is performed under the protection of flowing inert gas to remove the binder; the green porcelain embryo after glue removal is placed in an atmosphere sintering furnace to perform a multi-stage temperature rising sintering procedure to form a ceramic body; and the sintered ceramic body is subjected to heat treatment and then cooled to obtain the aluminum nitride substrate. The application reduces the lattice thermal resistance of the aluminum nitride substrate and improves the mechanical strength of the aluminum nitride substrate.

This utility model discloses a demolding device for a pressing mold, including a pressure screw, a hollow demolding screw, and a screw support. The screw support includes a base, on which a hollow demolding screw support nut bracket and a pressure screw support nut bracket are fixedly installed. The hollow demolding screw is threadedly connected to the nut hole on the hollow demolding screw support nut bracket, and a pressure screw is threadedly connected to the nut hole on the pressure screw support nut bracket. A cylindrical cavity is formed in the center of the hollow demolding screw, through which the pressure screw passes. This demolding device for a pressing mold significantly reduces cracking damage to the ceramic blank after demolding. It has good demolding effects for both experiments with and without adhesive powder. The demolded blanks have high consistency and few defects, providing accurate and reliable performance evaluation of the sintered ceramic powder. Furthermore, it greatly improves the demolding success rate, efficiently obtaining high-quality blanks.

A method for enhancing mechanical properties of sintered, zirconia ceramic bodies and zirconia ceramic dental restorations is provided. A porous or pre-sintered stage of a ceramic body may be treated with a tantalum-containing composition prior to sintering. Alternatively, zirconia ceramic powder may be coated with a tantalum-containing composition prior to forming a shaped ceramic body. After sintering, the resulting ceramic bodies have enhanced mechanical properties, such as greater fracture toughness, without a significant decrease in optical properties.

Described is sintered zirconia-toughened alumina (ZTA), e.g., in the form of a sintered zirconia-toughened alumina body, and methods of preparing these sintered bodies, wherein the sintered ZTA includes silica to improve a machinability property of the sintered ZTA.

The invention provides a high-strength high-thermal-conductivity reaction-sintered SiC ceramic material and a preparation method thereof.The preparation method comprises the following steps that silicon carbide powder and carbon source powder are mixed and then subjected to ball milling treatment, and mixed powder is obtained; mixing the mixed powder with a binder, a plasticizer and a lubricant, and carrying out high-speed centrifugal stirring and rolling homogenization treatment to obtain a silicon carbide mud blank for injection molding; putting the silicon carbide mud blank for injection molding into a mold, carrying out hot-press injection molding, demolding to obtain a silicon carbide prefabricated body, and carrying out glue removal treatment to obtain a silicon carbide biscuit; and paving silicon particles on the silicon carbide biscuit, carrying out vacuum high-temperature infiltration, and cooling. According to the preparation method, the plastic deformation capacity of the silicon carbide mud blank is optimized by regulating and controlling the component proportion, in the preparation process, the movement rearrangement effect among particles is enhanced by applying reinforced shearing centrifugal stirring and rolling treatment to a mixed system, the density of a biscuit is effectively improved, residual silicon is promoted to be uniformly distributed, and the content and size of the residual silicon are reduced; and the overall performance of the material is improved.

The present invention describes a method for deforming sintered ceramic (3) by reheating it to a deformable state and adapting it to a shape (1) by means of self-gravity. The method offers an efficient and controlled method for producing complex ceramic parts such as washbasins and represents a significant improvement over conventional methods.

Disclosed is a multilayer sintered ceramic body comprising at least one first layer comprising polycrystalline YAG, wherein the at least one first layer has at least one surface; and at least one second layer comprising magnesium aluminate spinel, wherein the at least one surface of the at least one first layer comprises pores wherein the pores have a maximum size of from 0.1 to 5 pm as measured by SEM, and wherein each of the at least one first layer and the at least one second layer has a coefficient of thermal expansion (GTE), wherein the GTE of the at least one first layer and the GTE of the at least one second layer differ from 0 to 0.6×10−6 / ° C. Methods of making are also disclosed.

This ceramic sintered compact contains: zirconia crystal particles containing yttria; and alumina crystal particles. The ratio ({Y / (Zr+Y) × 100} between elemental yttrium (Y) and elemental zirconium (Zr) contained in the zirconia crystal particles is 1.5-20 at%.

The invention discloses a magnetorheological elastomer self-adaptive clamping mechanism for ceramic body machining, and relates to the technical field of ceramic machining. The device comprises a base, symmetrical clamping arms, a linear driver, a self-adaptive clamping plate assembly and a main control unit, a magneto-rheological elastomer column and a micro vortex vacuum pump are arranged in the self-adaptive clamping plate assembly, and the main control unit achieves clamping force closed-loop control with + / -0.02 N precision through a PID algorithm; the miniature vortex vacuum pump forms stable pressure difference adsorption in a 5Pa vacuum environment, and the friction force of the miniature vortex vacuum pump, the nanometer silica gel anti-skid layer and the clamping force of the magnetorheological elastomer form triple synergistic fixation. The technical problems of clamping damage and adsorption failure of the ceramic green body in the vacuum environment are solved, and the vacuum spraying device is suitable for machining procedures such as vacuum spraying and fettling of the unsintered / semi-sintered ceramic green body.

The invention belongs to the technical field of fluorescent ceramic preparation, and relates to an enhanced near-infrared luminescence MgAl2O4: Cr < 3 + > fluorescent ceramic and a preparation method thereof, and the preparation method comprises the following steps: dissolving Mg (NO3) 2.6 H2O, Al (NO3) 3.9 H2O and Cr (NO3) 3.9 H2O in deionized water, then adding urea, stirring and dissolving; transferring the mixed solution into a reaction kettle for hydrothermal reaction to obtain MgAl2O4: Cr < 3 + > powder; adding a sintering aid CaF2 into the MgAl2O4: Cr < 3 + > powder, and carrying out ball milling and mixing; the ball-milled powder is poured into a mold to be compacted and then put into an SPS sintering furnace to be sintered; the sintered ceramic is subjected to annealing treatment; the surface of the annealed ceramic is sequentially subjected to coarse grinding and polishing operation, and the MgAl2O4: Cr < 3 + > fluorescent ceramic is obtained. According to the method, the luminescent property of Cr < 3 + > is remarkably promoted, and meanwhile, the high density and excellent mechanical property of the ceramic are guaranteed.

Provided is a method whereby a ceramic powder can be more evenly mixed with a sintering aid. This method for producing a mixed ceramic powder includes: a step in which a sintering aid comprising granules of a sintering-aid powder is prepared; and a step in which a ceramic powder serving as a base material is mixed with at least one such sintering aid to produce a mixed ceramic powder.

The invention relates to a functional ceramic phase-nanopore resin ablation-resistant composite material and a preparation method thereof, and belongs to the technical field of ceramic-based thermal protection materials. The preparation method comprises the following steps: mixing ablation-resistant ceramic powder, sintering-assistant ceramic powder and high-emissivity ceramic powder in proportion, and carrying out ball milling to obtain mixed powder; adding the mixed powder into a dispersing agent to obtain ceramic slurry; after fiber roughening pretreatment, ceramic slurry is applied to the upper surface of a fiber preform, then the slurry is promoted to uniformly permeate into the fiber through auxiliary oscillation, and a fiber preform loaded with a functional ceramic phase is obtained; putting the fiber preform into a mold, injecting resin sol into the mold by adopting an RTM (Resin Transfer Molding) process, sealing the mold, curing and drying at normal pressure to prepare the functional ceramic phase-nanopore resin ablation-resistant composite material. The obtained composite material not only has lower density and lower thermal conductivity, but also has higher ablation resistance.

Ceramic particles for use in a solar power tower and methods for making and using the ceramic particles are disclosed. The ceramic particle can include a sintered ceramic material formed from a mixture of a ceramic raw material and a darkening component comprising MnO as Mn2+. The ceramic particle can have a size from about 8 mesh to about 170 mesh and a density of less than 4 g / cc.

The utility model belongs to the technical field of ceramic sintering, and particularly relates to a ceramic product sintering device which comprises a furnace body, the front face of the furnace body is provided with a gate in a hinged mode, and a containing table is movably arranged in the furnace body. The heating part is arranged above the placing table and is used for heating the ceramic; wherein a dust collecting structure is arranged on the side edge of the placing table, and the dust collecting structure can collect smoke dust generated in the ceramic sintering process. And the effects that the smoke dust in the furnace body can be treated, and the production quality of the ceramic products can be improved are achieved.

This application relates to a relaxor ferroelectric piezoelectric ceramic material, its preparation method, and its application, belonging to the field of piezoelectric ceramic technology. The method includes: obtaining a ceramic precursor powder after pre-firing, grinding, and drying; preparing the ceramic precursor powder into a casting slurry to form a ceramic green sheet; printing internal electrodes on the ceramic green sheet and performing lamination pressing to obtain a laminated green sheet; hot-cutting the ceramic green sheet to obtain the ceramic green sheet, wherein the internal electrode is an Ag-Pd-Cu ternary metal system, with Ag at 80-90 wt%, Pd at 5-15 wt%, and Cu at 3-8 wt%; performing staged atmosphere co-firing treatment; and performing electrode connection and polarization treatment on the sintered ceramic to obtain a laminated piezoelectric ceramic device. This application synergistically controls the composition of the internal electrode and the sintering atmosphere path, improving the bonding performance of the ceramic-electrode interface, reducing thermal stress concentration, and enhancing the stability and reliability of the laminated piezoelectric ceramic during polarization and use.

A spark plasma sintering tool (1) is provided. The tool includes a die (2) including an inner wall having a diameter defining an internal volume configured to receive ceramic powder (5) and an upper punch (4) and a lower punch (4') operably coupled with the die, wherein each of the upper punch and the lower punch has an outer wall defining a diameter that is smaller than the diameter of the inner wall of the die, whereby when at least one of the punches moves within the internal volume of the die, a gap of 10-100 pm wide is created between each of the punches and the inner wall of the die. Also disclosed is a method of using the tool to produce a large sintered ceramic body and a computer readable medium storing processor executable instructions adapted to cause one or more computing devices to operate the tool.

The invention relates to a heat-sensitive material with a high lift-to-drag ratio and a preparation method thereof, and belongs to the technical field of preparation of electronic ceramic elements. The preparation method comprises the following steps: mixing nano barium titanate powder and donor-doped barium titanate powder, molding, and sintering to obtain the barium titanate-based thermal sensitive ceramic, the nano barium titanate powder is acceptor doped nano barium titanate powder or undoped nano barium titanate powder; the sintering is carried out under the condition of 1000 to 1500 DEG C for 0.5 to 10 hours. According to the invention, high density and low room temperature resistance are realized, effective oxidation of ceramic grain boundaries can be realized, acceptor doping is realized at the grain boundaries, and the thermal sensitive ceramic has obviously improved thermal sensitive performance. The two-step sintering method preferably adopted by the invention can effectively improve the density of the sintered ceramic and reduce the grain size, is beneficial to improving the performance stability of the thermal sensitive ceramic, and is beneficial to miniaturization of a thermistor with a multi-layer chip structure.