241 results about "Spark plasma sintering" patented technology

Spark plasma sintering (SPS), also known as field assisted sintering technique (FAST) or pulsed electric current sintering (PECS), is a sintering technique. The main characteristic of SPS is that the pulsed or unpulsed DC or AC current directly passes through the graphite die, as well as the powder compact, in case of conductive samples. Joule heating has been found to play a dominant role in the densification of powder compacts, which results in achieving near theoretical density at lower sintering temperature compared to conventional sintering techniques. The heat generation is internal, in contrast to the conventional hot pressing, where the heat is provided by external heating elements. This facilitates a very high heating or cooling rate (up to 1000 K/min), hence the sintering process generally is very fast (within a few minutes). The general speed of the process ensures it has the potential of densifying powders with nanosize or nanostructure while avoiding coarsening which accompanies standard densification routes. This has made SPS a good method for preparation of ceramics based on nanoparticles with enhanced magnetic, magnetoelectric, piezoelectric, thermoelectric, optical or biomedical properties. SPS is also used for sintering of Carbon Nanotubes for development of field electron emission electrodes. While the term "spark plasma sintering" is commonly used, the term is misleading since neither a spark nor a plasma is present in the process. It has been experimentally verified that densification is facilitated by the use of a current.