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1407 results about "Spark plasma sintering" patented technology

Spark plasma sintering (SPS), also known as field assisted sintering technique (FAST) or pulsed electric current sintering (PECS), is a sintering technique. The main characteristic of SPS is that the pulsed or unpulsed DC or AC current directly passes through the graphite die, as well as the powder compact, in case of conductive samples. Joule heating has been found to play a dominant role in the densification of powder compacts, which results in achieving near theoretical density at lower sintering temperature compared to conventional sintering techniques. The heat generation is internal, in contrast to the conventional hot pressing, where the heat is provided by external heating elements. This facilitates a very high heating or cooling rate (up to 1000 K/min), hence the sintering process generally is very fast (within a few minutes). The general speed of the process ensures it has the potential of densifying powders with nanosize or nanostructure while avoiding coarsening which accompanies standard densification routes. This has made SPS a good method for preparation of ceramics based on nanoparticles with enhanced magnetic, magnetoelectric, piezoelectric, thermoelectric, optical or biomedical properties. SPS is also used for sintering of Carbon Nanotubes for development of field electron emission electrodes. While the term "spark plasma sintering" is commonly used, the term is misleading since neither a spark nor a plasma is present in the process. It has been experimentally verified that densification is facilitated by the use of a current.

Osseointegrative surgical implant

Embodiments of the present invention provide an osseointegrative implant and related tools, components and fabrication techniques for surgical bone fixation and dental restoration purposes. In one embodiment an all-ceramic single-stage threaded or press-fit implant is provided having finely detailed surface features formed by ceramic injection molding and/or spark plasma sintering of a powder compact or green body comprising finely powdered zirconia. In another embodiment a two-stage threaded implant is provided having an exterior shell or body formed substantially entirely of ceramic and/or CNT-reinforced ceramic composite material. The implant may include one or more frictionally anisotropic bone-engaging surfaces. In another embodiment a densely sintered ceramic implant is provided wherein, prior to sintering, the porous debound green body is exposed to ions and/or particles of silver, gold, titanium, zirconia, YSZ, α-tricalcium phosphate, hydroxyapatite, carbon, carbon nanotubes, and/or other particles which remain lodged in the implant surface after sintering. Optionally, at least the supragingival portions of an all-ceramic implant are configured to have high translucence in the visible light range. Optionally, at least the bone-engaging portions of an all-ceramic implant are coated with a fused layer of titanium oxide.
Owner:OSSEODYNE SURGICAL SOLUTIONS LLC

Refractory high-entropy alloy/titanium carbide composite and preparation method thereof

The invention discloses a refractory high-entropy alloy/titanium carbide composite. A refractory high-entropy alloy serves as a matrix phase, and titanium carbide serves as a wild phase; and elements in the refractory high-entropy alloy are selected from at least four kinds of elements of W, Mo, Ta, Nb, V, Ti, Zr, Hf and Cr. A preparation method of the refractory high-entropy alloy/titanium carbide composite comprises the steps that at least four kinds of carbonization metal powder in tungsten carbide, molybdenum carbide, tantalum carbide, niobium carbide, vanadium carbide, the titanium carbide, hafnium carbide, zirconium carbide and chromium carbide are selected and mixed according to the equal molar ratio or the ratio close to the equal molar ratio to form high-entropy matrix powder; and after the high-entropy matrix powder and titanium powder are mixed, alloy mechanization is carried out, then spark plasma sintering or hot-press sintering is carried out, and the refractory high-entropy alloy/titanium carbide composite is obtained. The density and cost of the composite are reduced while the hardness of the composite is improved, excellent high-temperature performance is achieved, and the requirement for manufacturing a high-temperature structural component is met.
Owner:江西咏泰粉末冶金有限公司

High-efficiency soft magnetic composite material and preparation method thereof

The invention discloses a high-efficiency soft magnetic composite material and a preparation method thereof. The material is in a nest wall structure composed of soft ferrite of high electrical resistivity; the ferrite in the nest wall structure completely isolates the soft magnetic metal in the nest or an alloy particle soft magnetic phase to cause the soft magnetic metal in the nest or the alloy particle soft magnetic phase to mutually isolate; the content of the soft magnetic metal or the alloy particle is 50-99wt%; and the balance is the soft ferrite. The preparation method comprises the following steps: mixing the soft magnetic metal or alloy particles and the soft ferrite powder at a ratio; causing the soft ferrite powder to completely and evenly coat the surface of the soft magnetic metal or the alloy particles; complexly sintering and shaping by spark plasma sintering densification; and finally, carrying out stress removal annealing heat treatment. The high-efficiency soft magnetic composite material has the characteristics of high-saturation induction density, high resistivity, high magnetic conductivity, low coercive force, low magnetic core loss and excellent comprehensive mechanical property. The high-efficiency soft magnetic composite material can be applied to occasions with higher working efficiency, high magnetic field and high stress. The preparation method issimple and the technological operation is convenient.
Owner:CHANGCHUN UNIV OF TECH
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