The invention provides MAB-phase
ceramic powder as well as a preparation method and application thereof, and belongs to the technical field of
ceramic materials. Firstly, elementary
substance M powder and
boron powder serve as raw materials, and MB powder is prepared through ball milling treatment, tabletting, heat treatment and
grinding; the simple
substance M powder is selected from
transition metal powder; the preparation method comprises the following steps: by taking MB powder and aluminum powder as raw materials, carrying out wet ball-milling treatment,
compression molding, packaging and
sintering treatment to prepare MAB-phase
ceramic powder; the packaging is carried out by adopting
potassium bromide powder. According to the invention, an MS3-fused salt shielding synthesis /
sintering method is adopted, salt is used as a reaction medium and a salt
bed, the exterior of a sample is packaged with salt, so that a synthetic product is prevented from being oxidized during high-temperature synthesis in the air, and the preparation method has the characteristics of rapidness, high efficiency,
energy conservation,
environmental protection, low cost and the like, and is simple, convenient and feasible in the aspect of promotion of large-scale production.