This application discloses a method for preparing a
graphene /
carbon nanotube composite
slurry and its application, relating to the field of electrochemical sensing. The method includes: S1, placing multi-walled carbon nanotubes in concentrated
sulfuric acid, reacting, washing with deionized water until neutral, and
drying to obtain carboxylated carbon nanotubes; S2, adding the carboxylated carbon nanotubes to
thionyl chloride, stirring the reaction, rinsing with
tetrahydrofuran, and
drying to obtain
acyl chloride-based carbon nanotubes; S3, mixing the following components: 4.0-6.0% multi-walled carbon nanotubes,
graphene microsheets... 0.2-1.0%, dispersant 0.5-1.0%,
melamine 3.0-6.0%, balance NMP; S4, add
graphene oxide /
carbon nanotube filter material to dilute
hydrochloric acid solution for
acid washing and purge with
nitrogen bubbles, stir evenly, filter, dry, and repeat 4 times. Mix and disperse each component in N-methylpyrrolidone to improve the uniformity of the mixture. Carbon nanotubes and graphene microsheets are uniformly dispersed in NMP to reduce the possibility of agglomeration and break up the already agglomerated groups.