Graphene fiber and method for manufacturing same
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example 1
Preparation of Solution of Graphene (RCCG) Chemically Converted by Reduction
[0044]In accordance with the method illustrated in FIG. 1, RCCG was dispersed in dimethylformamide (DMF) in the presence of an appropriate amount of triethylamine to obtain a stable graphene dispersion. Several grams of RCCG was obtained by reducing an aqueous dispersion of CCG with excess hydrazine at 95° C. over 2 h in accordance with previously reported methods (Li, D., Muller, M. B., Gilje, S., Kaner, R. B. & Wallace, G. G. Processable aqueous dispersions of graphene nanosheets. Nature Nanotech. 3, 101 (2008)). As a result of the reduction reaction, the graphene aggregated in the aqueous solution. The graphene aggregates were acidified with dilute sulfuric acid under vigorous stirring to a pH of 2 or less, and transferred to a sintered funnel. The aggregates were washed with a large amount of Milli-Q water on the funnel until the pH reached about 7. The filtered material was dried under vacuum at 70° C. ...
example 2
Production of Graphene Fiber
[0045]The solvent (DMF) of the graphene flake dispersion was exchanged with distilled water by centrifugation. The G / F aqueous solution was mixed with sodium dodecyl benzene sulfonate (SDBS) by ultrasonication.
[0046]The graphene dispersion was slowly injected into a coagulation bath containing PVA (molecular weight=89,000-124,000, degree of hydrolysis=˜99%) through a syringe (26 gauge) and wet spun to continuously produce a uniform graphene / PVA fiber.
[0047]The graphene / PVA was annealed at 600° C. to remove the PVA, leaving behind a porous fiber composed of graphene alone. The diameter of the graphene fiber was 28 μm.
experimental example
Characterization of the Graphene Fiber
[0048]The graphene fiber was sufficiently flexible and thus could be wound on a glass tube having a small diameter of 6.5 mm without mechanical damage, unlike graphene papers tending to be brittle (FIG. 1B). Complete knots of the graphene fiber were difficult to form, but the formation of sufficiently strong, flexible, small diameter knots of the graphene fiber was possible (FIG. 1C). Difficulty in the formation of complete knots was due to the small length of the graphene flakes and the frictional force of the rough surface of the graphene fiber composed of the graphene flakes (FIG. 2B). Several strands of the graphene fiber can also be woven into a fabric.
[0049]FIG. 2 shows SEM images of the surface and cross-sectional morphologies of the graphene fiber obtained by removing the PVA from the graphene / PVA composite fiber. After annealing at 600° C. for 1 h or treatment with 37% hydrochloric acid for 24 h, the graphene fiber had a rough surface b...
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