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Preparation method and device of metal foam material

A metal foam and metal aluminum technology, which is applied in the field of the preparation of closed-cell metal foam materials, can solve the problems of poor product reproducibility, prolonged cooling time, and reduced product yield, etc. The effect of reducing pore size gradient and improving mechanical properties

Active Publication Date: 2012-03-14
NORTHEASTERN UNIV
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  • Summary
  • Abstract
  • Description
  • Claims
  • Application Information

AI Technical Summary

Problems solved by technology

[0006] It can be seen from the preparation process of the above-mentioned foam material that both the melt stirring casting method and the powder metallurgy method contain two main steps, one is the preparation of the preform, and the other is the heating and expansion process of the preform. The formation of foam plays a vital role; but there are shortcomings in its technology, this is because the heating and foaming process in the existing technology is carried out in a well-type or box-type resistance furnace, using convection and heat radiation. Heat transfer makes the foaming process take a long time. At the same time, because the prepared foam is mostly in the shape of a block, the heat insulation effect of the unique porous structure of the foam material will also cause the cooling time to be prolonged, and finally due to gravity. The obtained aluminum foam contains a thicker solid metal layer, which greatly reduces the yield of the product. In addition, the heating and foaming and cooling time prolongation also make the cell evolution of the foam difficult to control, and the pore size gradient from the outside to the inside is relatively small. Large, and it is easy to form internal defects in the process, which makes the control of process conditions more difficult and the reproducibility of products is poor

Method used

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  • Preparation method and device of metal foam material
  • Preparation method and device of metal foam material
  • Preparation method and device of metal foam material

Examples

Experimental program
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Effect test

Embodiment 1

[0046] Embodiment 1: a kind of preparation method of metal foam material is as follows:

[0047] Take 850g of pure aluminum and melt it at 800°C-850°C, add 120g of metal silicon and 30g of metal calcium respectively to prepare Al-12%Si-3%Ca alloy melt, stir evenly and cool down to 600°C-650°C, add Titanium hydride accounting for 0.5-1.5% of the mass of the aluminum alloy melt and stirred evenly, the particle size of titanium hydride is 250-300 mesh and oxidized at 500°C for 1 hour, the stirring speed is 1000-3000r / min, and the stirring time is 3-5min. The aluminum alloy melt containing titanium hydride is poured into a flat ingot and cut into a 5mm thick plate, which is the foamable precursor 5, and the output voltage of the thyristor in the temperature control device is adjusted to change the temperature of the infrared radiator. Transmit power so that the temperature between the upper and lower heating mantles is at a certain temperature between 800°C and 1100°C, the distanc...

Embodiment 2

[0048] Embodiment 2: a kind of preparation method of metal foam material is as follows:

[0049] Take 497.5g of aluminum powder and 2.5g of magnesium powder for preliminary mixing, then take titanium hydride powder with a mass fraction of 0.5-1.0% of the mixed powder and pour them into the mixing tank together, seal the mixing tank and place it in the electric mixing tank Rotate and mix on the rollers of the machine, the mixing time is 0.5-1.5h, then pour the uniformly mixed material into the mold and compress it axially, the pressure is 300-500MPa, and the green body obtained is cut into thicknesses of 5mm foamable precursor 5, adjust the output voltage of the thyristor in the temperature control device and then change the emission power of the infrared radiator, so that the temperature between the upper and lower heating mantles is at a certain temperature between 800°C and 1100°C Next, the distance between the two heating mantles is 60 mm, and the prepared precursor 5 is pl...

Embodiment 3

[0050] Embodiment 3: a kind of preparation method of metal foam material is as follows:

[0051] Take a total of 500g of titanium hydride powder and aluminum powder accounting for 0.6 to 1.2% of the total mass and pour them into the mixing tank together, seal the mixing tank and place it on the rollers of the electric mixer for rotation and mixing. The mixing time is 0.5~1.5h, then pour the uniformly mixed material into the mold for cold pressing, the pressure is 200~300MPa, then heat the obtained cold compact at 300~500℃ and extrude, the pressure is 200~400MPa, finally Cut the obtained columnar green body into a foamable precursor 5 with a thickness of 5 mm, adjust the output voltage of the thyristor in the temperature control device and then change the emission power of the infrared radiator, so that the temperature between the upper and lower heating covers is at 800 Under a certain temperature between ℃~1100℃, the distance between two heating mantles is 60mm. Place the pr...

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Abstract

The invention discloses a preparation method and a device of a metal foam material. The preparation method comprises the following steps: mixing 93-99 wt% of aluminium matrix, 0.5-5 wt% of additive and 0.5-2 wt% of foaming agent uniformly to form a shaped foamable precursor material, putting the foamable precursor material in a foaming furnace with infrared heating to foam the foamable precursor material fast under infrared radiation, then taking the foam material out from the foaming furnace and cooling, wherein, the aluminium matrix is pure aluminium, aluminium powder or aluminium alloy, the foaming agent is titanium hydride, zirconium hydride, or calcium carbonate, and the additive is calcium, carborundum powder, or alumina powder. The device is a foaming furnace with infrared heating,has the advantages of fast foaming the precursor material, eliminating the hole gradient, easily controlling the foaming and cooling process, making the product have reproducibility and maneuverability, and improving cellular uniformity. According to the invention, metal foam sandwich panels can be prepared directly, and the mechanical properties of the aluminium-based foam material are improved.

Description

technical field [0001] The invention relates to a method for preparing a metal foam material, in particular to a method and a device for preparing a closed-cell metal foam material. Background technique [0002] Closed-cell metal foam is a new multifunctional structural material, which has the characteristics of low relative density, large specific surface area, high specific mechanical properties, and good damping and shock absorption performance. It can be widely used in aerospace, military industry, ships, and rail trains. , automobiles and construction, machinery and many other fields; [0003] The preparation methods of closed-cell metal foam mainly include melt stirring casting method and powder metallurgy method. [0004] The melt stirring casting method first melts aluminum at a certain temperature, and adds additives that can increase the viscosity of the melt to the aluminum melt, and then adds a foaming agent to the aluminum melt and disperses it evenly by stirri...

Claims

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Application Information

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IPC IPC(8): C22C1/08C22C21/00
Inventor 罗洪杰姚广春刘宜汉张晓明曹卓坤吴林丽
Owner NORTHEASTERN UNIV
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