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1218results about How to "Improve wettability" patented technology

Degradable epoxy resin system material and application thereof, body, composite material and recovery method thereof

The invention belongs to the technical field of recoverable epoxy resin, and relates to a degradable epoxy resin system material and application thereof, a body, a composite material and a recovery method thereof. The degradable epoxy resin system material comprises a first component and a second component, the first component comprises first epoxy resin and second epoxy resin, and the second component comprises a first curing agent, a second curing agent and an accelerant; the first epoxy resin is a mixture of one or more of glycidyl ether epoxy resin and glycidyl amine epoxy resin and accounts for 15-35% of the first component by mass, the second epoxy resin is selected from one or more of epoxy resin with the structure containing # imgabs0 #, and the second epoxy resin accounts for 60-80% of the first component by mass; the first curing agent is one or a mixture of more of alicyclic amines and accounts for 40%-60% of the second component by mass, the second curing agent is one or a mixture of more of polyether amines and accounts for 40%-60% of the second component by mass, and the accelerant accounts for 0.5%-3% of the second component by mass. The requirement for vacuum infusion of the wind power blade can be met.
Owner:TECHSTORM MATERIAL TECH SHANGHAI CO LTD

High-temperature-resistant carbon fiber reinforced phenolic resin composite material and preparation method thereof

The invention provides a high-temperature-resistant carbon fiber reinforced phenolic resin composite material and a preparation method thereof. The preparation method comprises the following steps: firstly, carrying out high-temperature oxidation treatment on carbon fibers; secondly, carrying out surface modification on the carbon fibers by using a chemical modifier; then mixing the modified carbon fiber, an antioxidant and a dispersing agent to prepare slurry; performing vacuum filtration on the prepared slurry, and drying to obtain a carbon fiber blank; preparing a phenolic resin infiltration solution, and impregnating the carbon fiber blank with the phenolic resin infiltration solution; and finally, carrying out mold pressing and curing to obtain the high-temperature-resistant carbon fiber reinforced phenolic resin composite The preparation method is simple in required equipment, convenient to operate, stable in process, high in production efficiency and suitable for large-scale industrial production. According to the high-temperature-resistant carbon fiber reinforced phenolic resin composite material prepared by the preparation method, the bonding property between the carbon fiber and the phenolic resin is improved, certain toughness and strength are provided, and meanwhile, the high-temperature-resistant carbon fiber reinforced phenolic resin composite material has the advantages of ablation resistance, good oxidation resistance in a high-temperature environment and the like.
Owner:ZHEJIANG SCI-TECH UNIV

Packing washing tower and washing method

The present invention discloses a filler washing tower and a washing method, the filler washing tower is used for washing treatment of VOCs waste gas, and the filler washing tower comprises: a washing liquid pipe which is arranged at the axis position of the washing tower in a penetrating manner, vertically extends and is used for receiving a washing liquid from the outside of the tower; the washing liquid pipe is provided with a rotatable pipe section at the corresponding position of the filler layer; the spraying pipe assembly is composed of a plurality of spraying pipes with different lengths and is communicated with the rotatable pipe section, and a spraying opening of each spraying pipe is formed in the tail end of the pipe; the spraying pipes are arranged at intervals in the circumferential direction of the rotatable pipe section and are tangent to the rotatable pipe section; the spraying pipes with different lengths drive the rotatable pipe section to rotate through counter-acting force when spraying out the washing liquid, and annular partition covering of the washing liquid on the packing layer is formed. Rotation of the spraying pipe is achieved through spraying of washing liquid, and through annular partition covering of spraying, water saving can be achieved while the gas-liquid mass transfer efficiency is guaranteed, and external power consumption is not needed.
Owner:CHINA PETROLEUM & CHEMICAL CORP +1

High-strength silver-free copper-based brazing filler metal

The invention discloses a high-strength silver-free copper-based brazing filler metal which is composed of P, Sn, Ni and Cu. The high-strength silver-free copper-based brazing filler metal is low in cost, safe, environmentally friendly and good in welding effect; through the adding of Sn and Ni, the melting point of brazing filler metal alloy is reduced, and the tensile strength and wettability of the brazing filler metal alloy are enhanced.
Owner:ANHUI HUAZHONG WELDING MATERIAL CO LTD

Reinforced liquid metal sliding bearing

The invention relates to the technical field of metal bearings, in particular to a reinforced liquid metal sliding bearing. The enhanced liquid metal sliding bearing comprises a rotor, a stator and liquid metal filled in an assembling gap between the rotor and the stator. The fixed positions of the rotor and the stator are provided with a spiral groove structure, a textured microstructure, an infiltration coating and a sealing coating. By adopting the enhanced liquid metal sliding bearing provided by the invention, the wettability and the wear resistance of a bearing rotating pair can be improved, and the problems of coating falling, wear, poor lubrication and the like of the enhanced liquid metal sliding bearing in a high-vacuum, high-temperature, high-pressure, high-speed and high-load use environment are effectively solved. High-pressure sealing is formed on the gaps between the stator and the rotor and between the limiting rings of the stator and the rotor, the liquid metal is kept in the bearing, the assembled bearing does not need a vacuum environment in the transfer process, meanwhile, external gas is prevented from entering the bearing structure, and the possibility that the liquid metal leaks or gets stuck is reduced.
Owner:SHANGHAI LEADING TECH CO LTD

Active brazing filler metal for sealing sapphire and kovar alloy and preparation method of active brazing filler metal

The invention discloses active brazing filler metal for sealing sapphire and kovar alloy and a preparation method of the active brazing filler metal. The active brazing filler metal comprises 25.0 wt%-27.5 wt% of Cu, 1.0 wt%-6.0 wt% of Ti, 1.0 wt%-5.0 wt% of Al, 0.1 wt%-1.0 wt% of B, 0.1 wt%-0.5 wt% of rare earth element RE, RE is one or more of La, Ce, Sc, Pr, Nd and Er, and the balance is Ag. The preparation method comprises the following steps: preparing silver-based pre-alloying powder by adopting a gas atomization method, mixing the alloy powder with additive element powder in a ball milling manner, sintering by utilizing vacuum pressure to obtain an alloy ingot blank, and carrying out rough rolling, intermediate annealing and finish rolling to obtain an active brazing filler metal strip with the thickness of 0.05-0.2 mm. The active brazing filler metal is well matched with the thermal expansion coefficient of sapphire, direct brazing of sapphire and Kovar alloy can be achieved, the brazing temperature is moderate, and a brazed joint is uniform in structure and free of defects such as air holes and cracks.
Owner:BEIJING INST OF NONFERROUS METALS & RARE EARTH

Battery and electric device

The invention discloses a battery and an electric device. The battery comprises an outer package, an electrode assembly and an electrolyte, the electrode assembly is arranged in the inner space of the outer package, and the electrolyte is filled in the inner space of the outer package; wherein the electrode assembly comprises a pole piece, the pole piece comprises a main body part and a plurality of convex parts, each convex part is formed by a part of the pole piece protruding towards one side of the main body part, and the center-to-center distance L between every two adjacent convex parts is larger than or equal to 0.5 mm and smaller than or equal to 4.0 mm; the viscosity of the electrolyte at 25 DEG C is eta, and 3.0 < = eta / L < = 7.0, so that the distance between two adjacent convex parts is matched with the viscosity of the electrolyte, the convex parts can provide enough support for the isolating membrane, the electrolyte can smoothly flow among the convex parts, better liquid storage is realized, the infiltration effect of the electrolyte is improved, local liquid shortage is prevented, and the service life of the isolating membrane is prolonged. And the transmission effect of ions between the pole piece and the diaphragm can be improved, the charge-discharge cycle performance of the battery can be improved, the adhesion between the pole piece and the diaphragm can be improved, and the overall interface consistency of the battery can be improved.
Owner:NINGDE AMPEREX TECHNOLOGY LTD

Lithium oxalate lithium supplement agent, preparation method thereof and lithium battery

The invention provides a lithium oxalate lithium supplement agent, a preparation method thereof and a lithium battery, and belongs to the technical field of lithium batteries. The lithium oxalate lithium supplement agent comprises lithium oxalate, a conductive agent and a catalyst, wherein the catalyst is nonmetal doped manganese dioxide. The lithium oxalate, the non-metal doped manganese dioxide and the conductive agent are mixed in water, and then spray drying is performed to obtain the lithium oxalate lithium supplement agent. The nonmetal doped manganese dioxide catalyst has a nano flower cluster shape and can be in close contact with lithium oxalate to form homogeneous microspheres, efficient solid-solid catalysis is promoted, the decomposition voltage of a lithium oxalate lithium supplement agent can be reduced to 4.25 V from 4.8 V, and meanwhile good integrity and wettability are kept.
Owner:GANFENG LITHIUM CO LTD

Aqueous lithium battery positive electrode adhesive, preparation method and application

The invention discloses a water-based lithium battery positive electrode adhesive, a preparation method and application. The adhesive is of a single-layer or multi-layer shell core-shell structure formed by polar monomers such as acrylic acid, acrylate monomers, cross-linking monomers, self-emulsifying monomers and water through core-shell emulsion polymerization; by controlling the mass percent of acrylate monomers, polar groups and the like in the core layer structure and the shell layer structure and selecting proper types and dosages of cross-linking monomers and self-emulsifying monomers, the adhesive has proper surface tension, shows excellent adhesion and wettability to the current collector, has high peel strength, and is suitable for the current collector. According to the present invention, the lithium ion battery pole piece has the low glass-transition temperature so as to ensure the high toughness, the high surface density, the excellent electrolyte resistance, the excellent electrical property, the excellent coating property and the like of the pole piece, and the raw materials are all non-fluorine materials so as not to produce hydrogen fluoride and other harmful gases during the lithium battery recovery; water is used as a solvent, recycling is not needed, environment friendliness and low carbon are achieved, the manufacturing process is simplified, and the application range is widened.
Owner:CHENGDU CODYYA TECHNOLOGY CO LTD

Perovskite solar cell, preparation method thereof and photovoltaic module

The invention relates to the technical field of solar cells, in particular to a perovskite solar cell, a preparation method thereof and a photovoltaic module. The invention aims to solve the problem that the cell performance is influenced by non-uniform coverage of the perovskite layer on the hole transport layer. For the purpose, the preparation method of the perovskite solar cell comprises the steps of preparing a hole transport layer on a substrate, preparing an interface modification layer on the hole transport layer, preparing a perovskite layer on the interface modification layer, and sequentially preparing an electron transport layer and an electrode on the perovskite layer to obtain the perovskite cell, the wettability of the hole transport layer can be improved by introducing 3-hydroxyphenylboronic acid into the adjacent interface of the perovskite layer and the hole transport layer, so that the coverage rate of the perovskite layer is increased, meanwhile, the 3-hydroxyphenylboronic acid is coordinated with metal ions in the perovskite layer, non-radiative recombination between the hole transport layer and the perovskite layer interface can be reduced, and the hole transport efficiency is improved. And the carrier transmission efficiency is improved.
Owner:TRINA SOLAR CO LTD

Positive electrode slurry, positive electrode plate, lithium ion battery and electric device

The invention provides positive electrode slurry, a positive electrode plate, a lithium ion battery and a power utilization device, a positive electrode lithium supplement agent comprises a lithium iron phosphate main material, a binder, a conductive agent and a porous additive, the conductive agent comprises conductive carbon black with a high specific surface area, and the specific surface area of the conductive carbon black is greater than or equal to 130 m < 2 > / g. The space between the lithium iron phosphate particles in the positive electrode slurry provided by the invention is filled with the porous additive with the medium aperture and the conductive carbon black with the small aperture and the high specific surface area, so that a positive electrode plate applying the positive electrode slurry not only is small in internal pore spacing, but also forms gradient pore structure matching capable of reducing tortuosity of lithium ion transmission, and the lithium ion transmission efficiency is improved. And the technical effects of improving the electrolyte wettability of the electrode, improving the quick charge capacity, the cycle life, the low-temperature discharge capacity and the like of the battery are achieved.
Owner:ZHEJIANG ZEEKR INTELLIGENT TECH CO LTD +2

Electrode assembly and battery

The invention discloses an electrode assembly and a battery. The electrode assembly comprises a plurality of pole pieces and an isolating membrane arranged between two pole pieces with opposite polarities, and at least one pole piece is provided with a plurality of first convex parts; the pole piece comprises a current collector and an active material layer arranged on the surface of the current collector, the first convex part is formed by bending a part of the current collector and a part of the active material layer towards the same side of the pole piece, the height of the first convex part is H1, and H1 is more than or equal to 20 microns and less than or equal to 80 microns; the active material layer comprises a softener, the softener is selected from at least one of organic silicon, fatty acid salt and quaternary ammonium salt, based on the total weight of the active material layer, the weight percentage of the softener is A, and A is larger than or equal to 0.01% and smaller than or equal to 0.4%. In the application, the softening agent is added into the active material layer to improve the overall flexibility of the pole piece 300, so that the active material layer at the first convex parts does not generate microcracks while the height of the first convex parts is higher, further, an electrode assembly capable of meeting the use requirements can be conveniently processed, and the electrolyte infiltration effect is improved.
Owner:NINGDE AMPEREX TECHNOLOGY LTD

Rare earth oxide modified high-entropy hard alloy and preparation method thereof

The invention discloses a rare earth oxide modified high-entropy hard alloy and a preparation method thereof. A high-entropy hard phase (high-temperature calcination), a high-entropy binding phase and rare earth oxide are adopted, grinding, pressing and air pressure sintering at the temperature of 1450-1550 DEG C are conducted, and the high-entropy hard phase is prepared from tungsten carbide, titanium carbide, zirconium carbide, yttrium carbide, manganese carbide, chromium carbide and molybdenum carbide; the high-entropy binding phase comprises the following components: cobalt and a CoCrFeNi-series high-entropy alloy; and the component of the rare earth oxide is Y2O3 or Nd2O3. The prepared rare earth oxide modified high-entropy hard alloy has the advantages of high strength, high compactness, high hardness, high wear resistance and the like.
Owner:SHANDONG SANZUAN CEMENTED CARBIDE CO LTD

Method for enhancing interface performance of carbon fiber composite coating through two-step chemical reaction synergistic modification, modified carbon fiber and application

The invention discloses a method for enhancing the interface performance of a carbon fiber composite coating through two-step chemical reaction synergistic modification, modified carbon fibers and application. The method comprises the following steps: carrying out silanization modification treatment and hyperbranched modification treatment on carbon fibers subjected to oxidation treatment to prepare the modified carbon fibers. The method for enhancing the interface performance of the carbon fiber composite coating through two-step chemical reaction synergistic modification is suitable for improving the interface performance of the carbon fiber composite coating, and the prepared modified carbon fiber is mixed with resin and a curing agent and cured; the obtained carbon fiber reinforced composite coating has excellent mechanical properties, wear resistance and erosive wear resistance, and can effectively reduce damages such as corrosion, erosive wear and the like of complex and harsh marine environments such as a spray splashing area and the like to steel structure facilities.
Owner:浙江科鑫重工有限公司 +1

Lead-free solder composition and preparation method thereof

The invention relates to the technical field of welding, in particular to a lead-free solder composition and a preparation method thereof. The composition comprises brazing filler metal and a brazing flux, wherein the brazing filler metal comprises 55 to 65 parts of copper, 30 to 40 parts of zinc, 0.5 to 1 part of silver, 0.1 to 1 part of tin, 0.1 to 0.5 part of nickel, 0.02 to 0.15 part of lanthanum, 0.03 to 0.15 part of cerium and 0.05 to 0.2 part of indium; the brazing flux comprises 18-22 parts of borax, 13-17 parts of boric acid, 25-32 parts of a potassium fluoride and potassium fluoborate compound, 3-5 parts of calcium fluoride, 12-16 parts of aluminum oxide and 8-11 parts of magnesium oxide. The lead-free solder composition does not contain toxic lead elements, pollution to the environment and the ecological system is little, the wettability, corrosion resistance, strength, stability and the like of the lead-free solder composition are improved, and the welding quality is comprehensively improved. According to the preparation method, uniform distribution and accurate control of the brazing filler metal and the brazing flux are guaranteed, stability and consistency of product quality are guaranteed, and the preparation method is easy and convenient to operate and suitable for mass production.
Owner:XINXIANG QIXING BRAZING TECH CO LTD

Method for strengthening coercive force of neodymium-iron-boron magnet through composite reduction grain boundary diffusion

The invention provides a method for strengthening the coercive force of a neodymium-iron-boron magnet through composite reduction grain boundary diffusion, which comprises the following steps of: (1) mixing a reducing agent, a dispersing agent and a composite rare earth diffusion source to obtain mixed powder; the composite rare earth diffusion source comprises a multi-element rare earth compound diffusion source and / or a composite compound diffusion source; (2) coating the mixed powder obtained in the step (1) on the surface of a neodymium-iron-boron magnet to obtain a coating layer magnet; and (3) carrying out sectional composite reduction-grain boundary diffusion heat treatment and tempering treatment on the coated magnet in the step (2) to obtain the neodymium iron boron diffusion magnet. According to the method, the composite rare earth diffusion source is adopted, the preparation cost of the neodymium iron boron diffusion magnet is reduced, meanwhile, the grain boundary diffusion efficiency is improved, and the large-scale market application prospect is achieved.
Owner:GANJIANG INNOVATION ACAD CHINESE ACAD OF SCI

Chip heat dissipation assembly and vehicle

The embodiment of the invention provides a chip heat dissipation assembly and a vehicle, relates to the technical field of heat dissipation, and is used for reducing the stress borne by a chip while improving the heat dissipation capability of the chip heat dissipation assembly. The chip heat dissipation assembly comprises a circuit board, a chip, a heat dissipation structure and a heat-conducting medium. The chip is located on the circuit board. The heat dissipation structure covers the side, away from the circuit board, of the chip and is connected with the circuit board. The heat dissipation structure comprises a heat dissipation plate, a surrounding part and a boss part. The surrounding part and the boss part are located on the side, close to the chip, of the heat dissipation plate. The enclosure part and the boss part are both connected with the heat dissipation plate, and the enclosure part is arranged around the boss part; a closed space is defined by the heat dissipation plate, the enclosure part, the boss part and the chip, and a gap is formed between the boss part and the chip. The closed space is filled with the heat-conducting medium, the heat-conducting medium is in a solid state at a first temperature and is in a liquid state at a second temperature, and the second temperature is higher than the first temperature. The chip heat dissipation assembly is applied to a vehicle so as to improve the heat dissipation capacity of a chip in the vehicle.
Owner:YINWANG INTELLIGENT TECHNOLOGIES CO LTD

Battery and electric device

The invention discloses a battery and a power utilization device, the battery comprises a battery cell and an electrolyte, the battery cell comprises a negative plate and a diaphragm, the negative plate comprises a current collector and a negative active material layer, the negative active material layer comprises a silicon-based material, and the diaphragm comprises a base film and a coating; the mass percent of the silicon element in the negative electrode active material layer is a; the viscosity of the electrolyte is b, and the unit is cp; the percentage of the thickness of the coating to the thickness of the diaphragm is c; 0.037 < = a * b / c < = 5.625. By controlling the value of a * b / c within the range of 0.037-5.625, the infiltration effect of the electrolyte on the negative electrode and the fast charging performance of the battery can be effectively improved under the condition of ensuring the energy density of the battery.
Owner:CALB (JIANGMEN) CO LTD +1

Thin-layer high-density filler

The invention discloses a thin-layer high-density filler which is prepared by combining an optimized weaving method, weaving density and a bundling mode on the basis of a plain woven wire mesh filler. The novel weaving method enables the weft number of the thin-layer high-density filler to be larger than that of plain woven wire mesh filler under the condition of the same warp number, and the thin-layer high-density filler has the characteristics of high specific surface area, high mass transfer efficiency, low flow pressure drop and the like. A large number of micropores exist on the surface of the thin-layer high-density filler, the wettability is extremely good, the transverse diffusion effect of liquid in the filler can be greatly enhanced due to the fact that the weft density is large, the performance is particularly outstanding in the processes of large-spraying-density rectification and the like, and the pressure drop is about 30%-50% lower than that of a common plain woven filler. The filler provided by the invention mostly adopts stainless steel wires as raw materials, and has the advantages of low cost, large flux, stable performance and low metal exudation rate, so that the filler is difficult to replace in the field of heat pump rectification, high-purity electronic chemical separation, intermediate separation and isomerism separation production.
Owner:ZHEJIANG UNIV OF TECH +1

Hole transport material, preparation method thereof and perovskite solar cell

The invention provides a hole transport material, a preparation method thereof and a perovskite solar cell. The chemical structural formula of the hole transport material is # imgabs0 #, wherein each A is independently a heteroatom. A thiophene-methoxy triphenylamine group and a thiophene-methylthio triphenylamine group are introduced into an acridine phosphate side chain, and a series of novel hole transport materials are provided. The hole transport material has higher decomposition temperature, better thermal stability and higher hole mobility, thereby being beneficial to hole extraction and transport. The hole transport material has a deep HOMO energy level matched with perovskite, and can be used in a perovskite solar cell without doping any additive, so that the perovskite solar cell has higher photoelectric conversion efficiency, photovoltaic performance and stability, and the material has repeatability.
Owner:JINKO SOLAR (SHANGRAO) CO LTD +1

Quick-drying water-based ink and preparation method thereof

ActiveCN119490772AAchieve quick dryingAchieving wear resistanceInksPolyesterPolymer science
The invention discloses quick-dry water-based ink and a preparation method thereof, and relates to the technical field of ink. The preparation method comprises the following steps: firstly, enabling 4, 6-bis (allyloxy)-n-butyl-1, 3, 5-thiazine-2-amine and vinyl sulfonamide to participate in a polymerization reaction of acrylic acid and butyl acrylate, and preparing 4, 6-bis (allyloxy)-n-butyl-1, 3, 5-thiazine-2-amine and vinyl sulfonamide through a two-step emulsion polymerization method; the core-shell structure modified polyester emulsion with 2, 5-thiazine-2-amine and vinyl sulfonamide as soft shells and acrylic acid and butyl acrylate as hard cores improves the wear resistance and durability of the ink. Then allyl polyether reacts with 2-(p-chlorphenyl) ethylene oxide, so that the drying time is shortened, and the wear resistance of the ink is improved; then through addition reaction of reactants, bis (2-ethoxyl) dimethyl ammonium chloride and hydrogen-containing silicone oil, the epoxy-amino-polyether combined modified silicone oil flatting agent is formed, the flatting agent has hydrophilicity and hydrophobicity, the drying speed is increased, and the wear-resistant effect is improved.
Owner:HUBEI YUELONG PACKAGING CO LTD

Water-based binder, preparation method thereof and carbon-coated aluminum foil

The invention relates to the technical field of battery binders, in particular to a water-based binder, a preparation method of the water-based binder and a carbon-coated aluminum foil. The water-based binder comprises a water-soluble monomer, an oil-soluble monomer, an amphiphilic monomer, a functional monomer, an initiator and a neutralizer, the amphiphilic monomer is prepared from at least one of sodium vinyl sulfonate, sodium p-styrenesulfonate, 2-acrylamide-2-methylpropanesulfonic acid and N-vinyl pyrrolidone; the functional monomer comprises at least one of divinylbenzene, pyrrole, phenylacetylene and 3, 4-ethylenedioxythiophene. According to the water-based binder, the water-soluble monomer, the oil-soluble monomer, the amphiphilic monomer and the functional monomer are compounded in proportion, the conductivity of the binder, the wettability to a conductive carbon material and an aluminum foil, the adhesion to the aluminum foil and the like are improved, the prepared battery has excellent cycle stability, and the service life of the battery is prolonged.
Owner:GUANGZHOU LUSHAN NEW MATERIALS

Ultrathin liquid metal thermal interface material based on dynamic infiltration regulation and preparation method

The invention provides an ultrathin liquid metal thermal interface material based on dynamic infiltration regulation and a preparation method, the ultrathin liquid metal thermal interface material is composed of a high-purity liquid metal main body and liquid metal dynamic infiltration adhesion layers connected to the two sides of the high-purity liquid metal main body, the material of the liquid metal dynamic infiltration adhesion layer is the same as that of the high-purity liquid metal main body, and the liquid metal dynamic infiltration adhesion layer is spread on the surface of the heating substrate and the surface of the heat dissipation substrate respectively. According to the method, the ultrathin metal liquid layer formed through dynamic infiltration is directly used as a heat transfer medium, molecular-level seamless attachment between the liquid metal and the substrate material interface is achieved, the ultrathin thermal interface with the minimum thickness of only nanoscale 1-1000 nm can be obtained, the contact thermal resistance is greatly reduced, the actually measured interface thermal conductivity can reach 25.9-47.1 W / m <-1 >. K <-1 >, and the thermal conductivity of the interface is greatly improved. The measured value far exceeds the measured value of the current commercial thermal interface material; the dynamic infiltration regulation and control means provided by the invention has universality and can be widely applied to various different heating and heat dissipation substrate materials.
Owner:BEIJING INST OF FUTURE SCI & TECH ON BIOINSPIRED INTERFACE

Polyarylamine hole transport material, synthetic method thereof and perovskite solar cell

The invention discloses a polyarylamine hole transport material, a synthesis method thereof and a perovskite solar cell, and belongs to the field of chemical and energy materials. The synthesis method comprises the following steps: mixing arylamine, aryl halide, a palladium catalyst, a phosphine ligand and organic alkali, carrying out a reflux reaction, and then adding an end-capping reagent to terminate the reaction; and settling the product in methanol, carrying out suction filtration to obtain a solid, and then carrying out Soxhlet extraction. By adjusting the activity of the reaction intermediate, two continuous C-N cross-coupling catalytic cycles are achieved, in the first catalytic cycle, high-reaction-activity arylamine and aromatic halide are coupled to generate a low-activity bifunctional secondary arylamine intermediate, the intermediate is kept in a dormant state in the first catalytic cycle, and after primary arylamine is completely consumed, the intermediate is separated from the primary arylamine, and the secondary arylamine is separated from the primary arylamine. And the secondary arylamine intermediate and the aromatic halide are subjected to coupling polymerization, so that accurate synthesis of a series of polyarylamine with narrow molecular weight distribution is realized. The polyarylamine can be used as a hole transport material to construct a perovskite solar cell, adjust interface hole extraction and promote perovskite growth.
Owner:ZHEJIANG UNIV

System and method for regulating and controlling metal wetting behavior in vacuum brazing process

The invention relates to the technical field of brazing, in particular to a metal wetting behavior regulation and control system and method in the vacuum brazing process. The pretreated hard alloy, the pretreated base body and the pretreated mixed brazing filler metal are loaded into a vacuum brazing furnace, a heating and temperature control system is started, and heating is conducted according to a preset heating curve; in the heating process, according to a feedback result monitored in real time, the wetting behavior of the brazing filler metal is regulated and controlled; and the heating system is closed, so that the brazed part is naturally cooled in the vacuum environment. The hard alloy and the substrate are subjected to surface pretreatment, so that surface oxides, oil stains and other impurities are effectively removed, the wettability of the surface of the substrate is improved, and favorable conditions are provided for uniform wetting of the brazing filler metal. And a proper amount of active elements are added into the prepared mixed brazing filler metal, so that the wettability of the brazing filler metal on the hard alloy is improved. Therefore, the problem that metal wetting is not uniform in the traditional vacuum brazing process is solved.
Owner:同济大学浙江学院

Hole transport layer, perovskite solar cell and preparation method

The invention belongs to the field of solar cells, and particularly relates to a hole transport layer, a perovskite solar cell and a preparation method. The hole transport layer comprises a NiOx layer and a self-assembly molecular layer, wherein the self-assembly molecular layer comprises a self-assembly molecular material and a surfactant. The perovskite solar cell comprising the hole transport layer has the advantages of high efficiency, high stability, low production cost and simple preparation process.
Owner:TRINA SOLAR CO LTD

Preparation method and application of PET (Polyethylene Terephthalate) enhanced bi-crosslinking polyion liquid composite solid electrolyte

The preparation method comprises the following steps: preparing PET non-woven fabric raw paper, preparing a nano-zinc oxide particle dispersion liquid, dipping the PET non-woven fabric raw paper in a solution, carrying out heat treatment to form a functional PET non-woven fabric, preparing a functional alkenyl ionic liquid, carrying out heat treatment to form a PET non-woven fabric, and carrying out heat treatment to form the PET reinforced bi-crosslinked polyionic liquid composite solid electrolyte. Adding a cross-linking agent, a lithium salt, a plasticizer and a photoinitiator to prepare an electrolyte precursor solution; the functional PET non-woven fabric is placed in the electrolyte precursor solution, standing and dipping are carried out under the vacuum condition, then thermal polymerization and photopolymerization are carried out, and the solid electrolyte is prepared and applied to the solid polymer lithium ion battery; the zinc oxide particles are compounded into the PET non-woven fabric to form the non-woven fabric which is thin in thickness, high in tensile strength and appropriate in porosity, and the non-woven fabric is cross-linked with the functionalized alkenyl ionic liquid and the electrolyte precursor solution step by step, so that the ionic conductivity, the electrochemical window and the thermal stability of the solid electrolyte and the safety performance of the battery in use are improved.
Owner:GUANGDONG GUANHAO NEW MATERIALS R&D CO LTD +2

Preparation method of silicon carbide reinforced aluminum-based composite material for electronic packaging

The invention relates to the technical field of metal-based composite materials, and discloses a preparation method of a silicon carbide reinforced aluminum-based composite material for electronic packaging, the method that pre-oxidation is conducted on the surfaces of silicon carbide particles first and then vacuum micro-evaporation titanium plating is conducted is adopted, the wettability with an Al matrix is obviously improved, generation of an interface reaction brittle product Al4C3 is inhibited, and the performance of the silicon carbide reinforced aluminum-based composite material is improved. Defects such as gaps in the composite material are reduced, and the mechanical property of the composite material is improved; the silicon carbide reinforced aluminum-based composite material is prepared by adopting a non-pressure infiltration method, so that the production time is obviously shortened, infiltration can be successful by taking a small amount of time, and the process is stable; the interface phase TiC / Ti5Si3-Al coating not only improves the electrical conductivity and thermal conductivity of the silicon carbide powder, but also enhances the adhesive force of the silicon carbide powder and an aluminum base; al2O3 is gradually adsorbed and deposited on the surface of the material by adopting a micro-arc oxidation process, so that the corrosion resistance of the aluminum silicon carbide composite material is enhanced, and the requirements of a contemporary packaging material on high heat dissipation and corrosion resistance can be met.
Owner:SUZHOU HATENG TECH CO LTD

Ni3Al-based alloy, test bar, turbine disc and preparation method of Ni3Al-based alloy

The invention relates to the technical field of alloys, in particular to a Ni3Al-based alloy, a test bar, a turbine disc and a preparation method of the Ni3Al-based alloy. The invention discloses a Ni3Al-based alloy which comprises the following components in percentage by mass: 7%-9% of Al, 7%-8.5% of Cr, 0.13%-0.24% of C, 0.5%-2% of Ti, 3%-6% of Mo, 1%-3% of W, 1%-2% of Hf, 0.005%-0.03% of B and the balance of Ni. According to the Ni3Al-based alloy disclosed by the invention, all the elements are coordinated and matched, so that the Ni3Al-based alloy has a long-range ordered crystal structure, a stable high-temperature phase structure and excellent oxidation resistance, mechanical property and high-temperature property.
Owner:GAONA AERO MATERIAL CO LTD

Water-based silicon-carbon negative electrode binder for lithium battery as well as preparation and application of water-based silicon-carbon negative electrode binder

The invention belongs to the technical field of polymers and lithium battery materials, and discloses a water-based silicon-carbon negative electrode binder for a lithium battery as well as preparation and application of the water-based silicon-carbon negative electrode binder. The water-based silicon-carbon negative electrode binder is obtained by copolymerizing the following monomers in percentage by mass: 30-50% of a hydrophilic monomer, 20-40% of a hydrophobic monomer and 10-30% of a functional monomer, the hydrophilic monomer is an unsaturated monomer containing carboxylic acid, amide and sulfonic acid groups; the hydrophobic monomer is at least one of acrylonitrile, methacrylonitrile, acrylate and methacrylate; the functional monomer is at least one of vinyl polysiloxane, sodium allysulfonate, sodium methallyl sulfonate, sodium p-styrenesulfonate and N-vinyl pyrrolidone. The water-based silicon-carbon negative electrode binder disclosed by the invention can enhance the binding force between silicon particles on the surface of a silicon-based negative electrode material and a current collector; meanwhile, the volume expansion of the silicon negative electrode material can be inhibited; the cycle performance is improved.
Owner:GUANGZHOU TINCI MATERIALS TECH