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1748 results about "Monopotassium phosphate" patented technology

Monopotassium phosphate, MKP, (also potassium dihydrogenphosphate, KDP, or monobasic potassium phosphate) is the inorganic compound with the formula KH₂PO₄. Together with dipotassium phosphate (K₂HPO₄·(H₂O)ₓ) it is often used as a fertilizer, food additive, and buffering agent. The salt often cocrystallizes with the dipotassium salt as well as with phosphoric acid.

Macroelement water-soluble fertilizer and preparation method thereof

The invention relates to the field of fertilizers, in particular to a macroelement water-soluble fertilizer and a preparation method thereof.The preparation method comprises the steps that a composite biochar material is prepared from biochar, loaded metal modified biochar and an iron metal material, and then the composite biochar material is compounded with tripotassium phosphate, monopotassium phosphate, disodium octoborate tetrahydrate, zinc sulfate monohydrate and the like; the finally prepared fertilizer can realize accurate fertilizer supply, the iron metal organic framework material efficiently converts nitrate nitrogen into ammonium nitrogen and cooperates with a large amount of trace elements such as tripotassium phosphate, the requirements of crops at all stages are met, nutrients in key periods are guaranteed, pores of the composite biochar material adsorb the nutrients, nutrient slow release is realized, root system interpenetration resistance is reduced, stress resistance is enhanced, and the yield of the crops is increased. The soil conditioner has the advantages of simple preparation process, reduction of growth hindrance, optimization of soil aggregates, increase of pores, reduction of volume weight, improvement of ventilation, water permeability and water and fertilizer retention capabilities, substantial agricultural economy energization, substantial yield increase of crops, and wide application prospects.
Owner:HUAIAN DAHUA BIO TECH

Intelligent control method and system for monopotassium phosphate

The invention relates to the technical field of intelligent control, in particular to a monopotassium phosphate intelligent control method and system.The method comprises the following steps that rhizosphere phosphorus and potassium concentration changes are obtained, whether the rhizosphere phosphorus and potassium concentration changes are in a critical rate interval or not is judged, an effective absorption time period identifier is generated, and an organ amplification ratio is analyzed to judge a cooperation period; and extracting a stalk concentration ratio, comparing the stalk concentration ratio with a reference interval to generate an application inhibition identifier, fusing information to judge a fertilization window, adjusting the concentration according to the root hair amplification and the water consumption rate, and generating a control instruction set. According to the method, the effective time period of phosphorus and potassium nutrient absorption of the crops is determined through crop rhizosphere phosphorus and potassium ion concentration difference calculation and average treatment, the objective interval of crop nutrient absorption rate indexes is defined, blind fertilization is avoided, the pertinence and accuracy of nutrient absorption and utilization of the crops are enhanced, the excessive application state of nutrient elements is dynamically identified, and the crop quality is improved. The risk of excessive nutrients caused by nutrient enrichment of crops is prevented, and resource waste and environmental burden are effectively reduced.
Owner:SHANDONG PROVINCE DINGXIN BIOLOGY TECH CO LTD

Microbial compound fertilizer for improving soil pollution as well as preparation method and application of microbial compound fertilizer

The invention discloses a microbial compound fertilizer for improving soil pollution, which is prepared by mixing a matrix fertilizer, alginic acid, cellulase, modified bentonite, biochar, a microbial agent, nano zero-valent iron and monopotassium phosphate according to a mass ratio of (30-40): (6-10): (5-8): (20-25): (15-20): (3-5): (4-6): (4-8), the microbial agent comprises pseudomonas, bacillus and silicate bacteria; heavy metal ions in soil can be effectively neutralized through the nanoscale zero-valent iron and the phosphate, pollutants in the soil can be effectively degraded through the microbial flora, meanwhile, nutrients needed by plant growth are provided, the modified bentonite is added, the soil structure can be changed, meanwhile, phosphorus and potassium fertilizers are provided for the soil, and the soil quality is improved. By adding alginic acid and cellulase, the activity of microorganisms is effectively enhanced, the fertility conversion efficiency of the microorganisms is improved, and soil improvement and remediation are achieved.
Owner:宁海县农业技术推广站 +1

Premature senility prevention management method for densely-planted double-layer truncated cone macadamia nut trees

ActiveCN120240220AFertilising methodsCultivating equipmentsPremature agingMacadamia integrifolia
The invention provides an anti-premature senility management method for closely-planted double-layer truncated cone macadamia nut trees, and belongs to the technical field of fruit tree cultivation. The premature senility prevention management method comprises layered nutrition supply and flower and fruit protection management. The layered nutrition supply comprises the following steps: deeply applying a calcium magnesium phosphate fertilizer to the lower layer of soil greater than 60cm, and covering a root controller; organic fertilizers and biological agents are applied to 30-60 cm soil of the middle layer; a macroelement, humic acid and seaweed extract water-soluble fertilizer is applied to the 0-30 cm soil of the upper layer; the flower and fruit protection management comprises the steps that ABA and paclobutrazol are sprayed in the flower bud differentiation period; brassinolide and fluid boron are sprayed in the full-bloom stage; spraying forchlorfenuron and amino acid in a young fruit stage; nAA and monopotassium phosphate are sprayed in the fruit swelling period. Layered nutrition supply and flower and fruit protection management are carried out on the densely-planted double-layer truncated cone macadamia nut trees, premature senility of the densely-planted macadamia nut trees is prevented, branch development of the lower layer is promoted, the tree vigor is balanced, and the high-yield level is maintained.
Owner:LINCANG ACAD OF FORESTRY SCI (LINCANG NUT SCI & TECH RES INST)

Demulsifier for eliminating oil-water interface emulsion layer in oilfield produced liquid treatment and preparation method thereof

The invention belongs to the technical field of sewage treatment, and particularly relates to a demulsifier for eliminating an oil-water interface emulsion layer in oilfield produced liquid treatment and a preparation method of the demulsifier. The preparation method comprises the following steps: adding acrylamide, 1-allyl-3-methylimidazolium bis (trifluoromethanesulfonyl) imine salt, allyl tributyl phosphonium chloride and deionized water into a first reactor, and heating and dissolving the acrylamide, the 1-allyl-3-methylimidazolium bis (trifluoromethanesulfonyl) imine salt, the allyl tributyl phosphonium chloride and the deionized water; adding allyl (diisopropylamino) dimethylsilane, butyl acrylate, deionized water, octylphenol polyoxyethylene ether-10, lauryl sodium sulfate and monopotassium phosphate into the second reactor, and stirring to obtain an emulsion; adding an initiator and sodium hydrogen sulfite into a second reactor, carrying out heating and heat preservation reaction, pouring the mixed solution in the first reactor, and continuously carrying out reaction, heating and heat preservation to obtain a viscous liquid; and drying and granulating the viscous liquid to obtain the demulsifier. The demulsifier provided by the invention has the characteristics of simple synthesis process and high demulsification rate.
Owner:DONGYING SPRING PETROLEUM ENG TECH

Culture solution and culture method for ganoderma lucidum

The invention discloses a ganoderma lucidum culture solution and a culture method thereof. Comprising the following raw materials in parts: 30-40 parts of water, 10-20 parts of corn flour, 1-5 parts of ammonium nitrate, 1-5 parts of monopotassium phosphate, 1-5 parts of potassium sulfate, 1-5 parts of boric acid, 1-5 parts of manganese sulfate, 1-5 parts of zinc sulfate, 1-5 parts of copper sulfate, 1-5 parts of ferric sulfate, 1-5 parts of a short-acting growth regulator, 1-5 parts of amino acid, 1-5 parts of vitamins, 1-5 parts of a seaweed extract, 1-5 parts of honey and 1-5 parts of peaches and oranges. The short-acting growth regulator is prepared from gibberellin, auxin and cytokinin according to the ratio of (2-5): (1-8): (2-9), and the amino acid is prepared by mixing isoleucine, lysine, methionine and phenylalanine according to the ratio of (1-5): (2-8): (4-9): (5-7). The nutrient purity of the culture solution can be greatly increased, the fatality rate is reduced, cell elongation and rooting are promoted, plant metabolism and growth can be greatly promoted, and the quality of ganoderma lucidum is improved.
Owner:任海博

Potassium fulvate chelated macroelement water-soluble fertilizer with stress resistance and growth promotion functions

The invention discloses a potassium fulvate chelated macroelement water-soluble fertilizer with stress resistance and growth promotion functions, and relates to the technical field of water-soluble fertilizers, the potassium fulvate chelated macroelement water-soluble fertilizer comprises the following raw materials by weight: 167-210 parts of mineral source potassium fulvate, 450-460 parts of potassium nitrate, 300-310 parts of urea, 150-160 parts of potassium dihydrogen phosphate, 30-40 parts of potassium sulfate, 15-25 parts of EDTA-disodium, and 5-15 parts of citric acid. 0.5 to 1.5 parts of brassinolide and 4 to 6 parts of polyaspartic acid; according to the potassium fulvate chelated macroelement water-soluble fertilizer with the stress-resistant and growth-promoting functions, through chelation cooperation of potassium fulvate and nitrogen, phosphorus and potassium, the solubility of the chelated phosphorus element in water is increased, and the chelated phosphorus element can be more uniformly distributed in soil; by adopting an EDTA-disodium and citric acid composite chelating system, volatilization and loss of nitrogen elements are reduced, the problem of precipitation of calcium, magnesium and phosphorus is solved, and the soil conditioner is suitable for hard water areas and especially has outstanding performance in saline-alkali soil and arid areas.
Owner:JILIN YIBO BIOTECHNOLOGY CO LTD

Fermentation medium for efficiently producing lipopeptide by bacillus subtilis, and application and method of fermentation medium

The invention provides a fermentation medium for efficiently producing lipopeptide by bacillus subtilis as well as application and a method of the fermentation medium. Each liter of the fermentation medium comprises 20-60g of a carbon source; 5-10 g of a nitrogen source; 1-5g of corn steep liquor dry powder; 1 to 5g of monopotassium phosphate; 1 to 5g of disodium hydrogen phosphate; 0.1 to 0.5 g of magnesium sulfate; 5 to 10 mg of calcium chloride; 5 to 10 mg of manganese sulfate; 5 to 10 mg of ferrous sulfate; and vegetable oil with a volume fraction of 1-5%. The carbon source is selected from at least one of glucose, maltodextrin and brown sugar; the nitrogen source is selected from at least one of diammonium hydrogen phosphate, sodium nitrate and urea; the vegetable oil is selected from at least one of soybean oil and corn oil. Bacillus subtilis with the volume fraction of 1-5% is inoculated into a fermentation culture medium for fermentation and fed-batch culture, and the yield of lipopeptide reaches 48.58 g / L. The method improves the lipopeptide production capability of the bacillus subtilis while eliminating foam, and is suitable for large-scale production and application.
Owner:BEIJING YINGHUIER BIOTECHNOLOGY CO LTD

Method for preparing amino acid-containing water-soluble fertilizer by using livestock and poultry slaughter blood

The invention relates to the field of preparation of amino acid water-soluble fertilizers, and discloses a method for preparing an amino acid-containing water-soluble fertilizer by using slaughtering blood of bred livestock and poultry, which comprises the following steps: collecting the blood of the bred livestock and poultry in a slaughter house through a blood collection container, and adding an anticoagulant to obtain an anticoagulant raw material; the preparation method comprises the following steps: heating and disinfecting an anticoagulant raw material, and then adding bacillus subtilis and monopotassium phosphate to carry out enzymolysis treatment, so as to obtain a feed liquid after enzymolysis; then filtering, complexing treatment, ultraviolet sterilization treatment and sterilization are carried out in sequence; carrying out amino acid detection on the sterilized material liquid subjected to enzymolysis, and adding other nutrients to form an organic liquid fertilizer containing amino acid; and finally, carrying out preservative treatment, packaging and warehousing, and storing in a shade place to complete the preparation process of the amino acid water-soluble fertilizer. The invention solves the problems that the existing amino acid water-soluble fertilizer preparation raw materials are less, the amino acid water-soluble fertilizer preparation process is longer, and the environment is polluted due to the discharge of livestock and poultry slaughtering blood waste.
Owner:JILIN ZENONG BIOTECHNOLOGY CO LTD

Water and fertilizer management method after transplanting of high-yield indica type two-line hybrid rice

The invention discloses a water and fertilizer management method for transplanted high-yield indica type two-line hybrid rice, and belongs to the technical field of rice cultivation. Comprising the following steps: (1) applying citric acid chelated calcium magnesium phosphate fertilizer to soil before transplanting; (2) applying coated controlled-release urea and a silicon-zinc fertilizer on the third day after transplanting; (3) when the tiller number reaches 2650,000-2750,000 plants / hm < 2 >, starting intermittent light field drying for three times, and deeply applying potassium magnesium sulphate before field drying; (4) laterally and deeply applying urea and a boron-humic acid chelate when tips of two inverted leaves are exposed; (5) spraying an aqueous solution in a full heading stage, wherein the aqueous solution comprises monopotassium phosphate, chelated zinc and brassinolide. Through staged precise fertilization, special chelating / controlled release fertilizer and water and fertilizer-field drying cooperation, the method has the advantages that the fertilizer utilization rate is increased, the nutritional requirements of rice in each growth period are precisely matched, and water and fertilizer cooperative management is optimized.
Owner:YIELEAD RICE IND

Cultivation material for cultivating selenium-rich black fungus and preparation method thereof

The invention relates to a preparation method of a cultivation material for cultivating selenium-rich black fungus, which comprises the following steps: respectively preparing a slow-release sodium chlorate composite material and a slow-release selenium-containing mineral material, and then mixing with carbon nutrition, nitrogen nutrition and mineral nutrition to obtain the cultivation material. The slow-release selenium mineral material is a polymer-coated slow-release selenium mineral material prepared by the following steps: preparing a selenium mineral core material from selenium powder, gypsum, calcium superphosphate, monopotassium phosphate, calcium sulfate, diatomite, nano silicon dioxide and a surfactant OP-10, preparing a coating material, adding the selenium mineral core material, and soaking with a Bis-Tris buffer solution. Sodium chlorate and selenium are respectively prepared into specific slow release systems, and are slowly released in the cultivation material to react to generate a seleninic acid component which can be easily absorbed and utilized by the black fungus, so that the concentration of seleninic acid in the cultivation material is regulated, the growth of the black fungus is promoted, the yield of the black fungus is increased, the quality of the black fungus is remarkably improved, and the cultivation cost is reduced. The selenium content and the amino acid content in the black fungus are obviously increased.
Owner:YANBIAN ACADEMY OF AGRI SCI +2

Fermentation medium for regulating and controlling target product of clostridium aerovorans and fermentation method of fermentation medium

The invention discloses a fermentation medium for regulating and controlling a clostridium aerovorans target product and a fermentation method of the clostridium aerovorans target product. The medium comprises a basic component and a regulating component, the basic components comprise ammonium chloride, potassium chloride, magnesium sulfate heptahydrate, sodium chloride, monopotassium phosphate, yeast powder, calcium chloride dihydrate, sodium selenite, nickel chloride hexahydrate, biotin, folic acid, pyridoxine hydrochloride, thiamine, riboflavin, nicotinic acid, D-calcium pantothenate, cobalamin, para aminobenzoic acid and lipoic acid; the adjusting component comprises sodium tungstate, ferrous sulfate and sodium molybdate, sodium tungstate and ferrous sulfate have a forward adjusting effect on increasing the yield of acetic acid, ethanol and butanol in the target product, and sodium molybdate has a reverse adjusting effect on the target product. By optimizing the proportion of trace elements in the culture medium, the clostridium metabolism efficiency is improved, synthesis of a target product is regulated and controlled, and the method is particularly suitable for industrial production of acetic acid, ethanol, butanol and the like.
Owner:NANJING SHIQI BIOCHEMICAL TECH CO LTD

Formitamidine thiosulfate second-order nonlinear optical crystal and preparation and application thereof

The invention relates to a formamidine thiosulfate second-order nonlinear optical crystal and preparation and application thereof, the chemical formula of the crystal material is [CH (NH2) 2] 2SO3S, the molecular weight is 203.27, the crystal material belongs to an orthorhombic crystal system, the space group is P212121, the unit cell parameter is # imgabs 0 # alpha = beta = gamma = 90 degrees, Z = 4, and the unit cell volume is # imgabs 1 #. Under 1064nm laser irradiation, the frequency doubling intensity of the powder is about two times that of monopotassium phosphate crystals, and phase matching can be realized. In addition, the crystal material has a wide light transmission wave band, the ultraviolet absorption cut-off edge is 253 nm, the optical band gap is 4.90 eV, and the crystal material is easy to grow. The wavelength range of the coherent light source can be expanded by using optical frequency conversion technologies such as second harmonic generation and optical parametric amplification. Therefore, the crystal material has important application value in the fields of laser frequency conversion, photoelectric information storage and the like.
Owner:TONGJI UNIV

Soil structure improver containing compound microbial agent and preparation method thereof

The invention discloses a soil structure improver containing a compound microbial agent and a preparation method of the soil structure improver. The soil structure improver containing the compound microbial agent is prepared from the following raw materials in percentage by mass: humic acid, the compound microbial agent, vermiculite powder, a seaweed extract, diatomite, polydextrose, pectin, monopotassium phosphate, an organic zinc chelate, a medium trace element supplement and bentonite, wherein the humic acid, the compound microbial agent, the vermiculite powder, the seaweed extract, the diatomite, the polydextrose, the pectin, the monopotassium phosphate, the organic zinc chelate, the medium trace element supplement and the bentonite are matched. According to the soil structure improver disclosed by the invention, through the synergistic effect of the compound microbial agent, the proportion of a soil aggregate structure is effectively increased, the stability and the anti-scouring capability of soil are enhanced, the air permeability and the water-retaining property of the soil are improved, an ideal environment is created for the growth of crop roots, and the microbial agent can be colonized in the soil, so that the soil structure is improved. A good microbial community structure is formed, the biological diversity of the soil is enhanced, the self-repairing capability of the soil is improved, and a healthy soil ecological system can be constructed.
Owner:江苏维福优生物科技有限公司

Culture medium formula for improving vibrio inhibition capability of bacillus

PendingCN120098818ABacteriaMicroorganism based processesBiotechnologyVibrio inhibens
The invention provides a culture medium formula capable of effectively improving vibrio inhibition capability of bacillus. The culture medium formula comprises 10-20 g of corn starch, 2-10 g of yeast powder, 2-10 g of malt extract, 5-20 g of glycerin, 0.5-1 g of L-aspartic acid, 1 g of dipotassium phosphate, 0.3 g of monopotassium phosphate, 0.5 g of magnesium sulfate, 1 g of calcium carbonate and 1000 mL of distilled water. When the culture medium is used for culturing bacillus capable of naturally inhibiting vibrio, the obtained culture has a better vibrio inhibiting effect.
Owner:QINGDAO INST OF TECH PHYSICS OF SCI & TECH OF CHINA

Electrode foil, preparation method thereof and aluminum electrolytic capacitor

The invention belongs to the technical field of electrode foil formation treatment, and particularly relates to an electrode foil and a preparation method thereof and an aluminum electrolytic capacitor, the preparation method of the electrode foil comprises the steps of performing multi-stage formation treatment on a corrosion foil, the number of stages of the formation treatment is at least two, and the formation treatment at least comprises first-stage formation and second-stage formation, first heat treatment is carried out after the second-stage formation; a formation liquid used in the second-stage formation is a mixed solution containing adipate and monopotassium phosphate. According to the preparation method provided by the invention, the formation liquid used in secondary formation is the mixed solution containing adipate and monopotassium phosphate, the limitation of traditional single formation liquid is broken through, and synchronous optimization of the structure, hydration resistance and electrochemical performance of the aluminum oxide film is realized through multi-stage formation, mixed solution synergy and the synergistic effect of formation and heat treatment; meanwhile, production cost is reduced, and environmental load is relieved.
Owner:DONGGUAN DONGYANG SOLAR SCI RES & DEV CO LTD

Method for detecting related substances in landiolol hydrochloride for injection

The invention belongs to the technical field of pharmaceutical analysis, and particularly relates to a method for detecting related substances in landiolol hydrochloride for injection. According to the method, an HPLC (High Performance Liquid Chromatography) method is adopted, octadecylsilane chemically bonded silica is taken as a filler, and a mobile phase A (the volume ratio of a monopotassium phosphate solution containing pentafluoropropionic acid to methanol is 58: 42-62: 38) and a mobile phase B (the volume ratio of the monopotassium phosphate solution containing pentafluoropropionic acid to methanol is 28: 72-32: 68) are used for gradient elution to detect the related substances in landiolol hydrochloride for injection. The detection method is high in specificity, high in sensitivity, good in accuracy and convenient to operate, the medicine quality can be effectively controlled, the technical blank of detection of the landiolol hydrochloride related substances for injection is filled, a reference standard is provided for quality control of landiolol hydrochloride for injection, and therefore the safety and reliability of clinical medication are guaranteed.
Owner:ZHEJIANG HEMUKANG PHARM TECH CO LTD

Management and control method for reducing malformed fruits caused by non-development of pineapple fruits

The invention relates to the technical field of pineapple planting, in particular to a management and control method for reducing malformed fruits caused by non-development of pineapple kernels. The management and control method comprises the steps of regulating and controlling nutrition before a flowering period, optimizing a microenvironment in a flowering period, strengthening management in a young fruit period and comprehensively preventing and controlling diseases and insect pests. The operation of regulating and controlling the nutrition before the flowering stage comprises the following steps: supplying a water-dispersible slow-release fertilizer by adopting a drip irrigation system from a seedling stage to a flowering accelerating stage; the mass ratio of nitrogen to phosphorus to potassium in the water dispersible slow-release fertilizer is 1: (1.1-1.3): (1.4-1.6); the operation of optimizing the microenvironment in the flower forcing period comprises the following steps: forcing flowers in cloudy days at the temperature of 18-25 DEG C or at dusk; after the inflorescence develops, a mixed solution of ethephon and gibberellic acid is adopted for core filling; the operation of strengthening young fruit stage management comprises the following steps: in a young fruit stage, spraying a mixed aqueous solution of sugar alcohol calcium and monopotassium phosphate to leaf surfaces; the operation of comprehensively preventing and controlling diseases and insect pests comprises the following steps: covering with breathable insect-preventing fruit bags 20 days after flowers wither, and releasing natural enemies to control the cardinal number of pests.
Owner:HAINAN BETTER ECO LEISURE AGRI TECH CO LTD

Medium-temperature semitransparent glaze for steel plate enamel without fluoride salt and nitrate as well as preparation method and application of medium-temperature semitransparent glaze

The invention discloses fluoride-salt-free and nitrate-free medium-temperature semitransparent glaze for steel plate enamel as well as a preparation method and application of the medium-temperature semitransparent glaze, and belongs to the technical field of enamel. The semitransparent glaze is prepared from quartz, potassium feldspar, anhydrous borax, sodium carbonate, titanium dioxide, monopotassium phosphate and zinc oxide according to a specific mass ratio. The preparation method comprises the steps of raw material mixing, high-temperature melting under a pure oxygen condition, wiredrawing detection, quenching and the like. The semitransparent glaze is completely free of fluoride salt and nitrate, the problems of fluoride emission and environmental protection equipment blockage are avoided from the source, the fluorine content of the product is not detected through detection, the product meets the requirements of European Union REACH regulations, meanwhile, the product has good porcelain surface, luster and firing adaptability, is suitable for a steel plate matrix, has the firing temperature of 800-840 DEG C and the firing time of 20-30 minutes, and is suitable for a steel plate. The method can be used for producing green and environment-friendly enamel products.
Owner:SINOPIGMENT & ENAMEL CHEM

Microbial agent for improving yield and quality of strawberries as well as preparation method and application of microbial agent

The invention discloses a microbial agent for improving the yield and quality of strawberries and a preparation method and application thereof, and belongs to the technical field of microorganisms. The microbial agent comprises the following raw materials in parts by weight: 40-50 parts of a compound microbial agent, 0.3-0.5 part of xanthan gum, 1.5-2 parts of glycerol, 4-5 parts of a citric acid-sodium citrate buffer solution, 1-1.5 parts of potassium humate, 0.3-0.5 part of monopotassium phosphate, 0.2-0.3 part of chelated calcium magnesium and the balance of water, wherein the total parts by weight of the raw materials are 100; the compound microbial agent is prepared from arthrobacter Xinjiang, linear Prussella bursa-pastoris and bacillus coagulans. The microbial agent disclosed by the invention can be used for effectively preventing and treating strawberry diseases, including root rot, fusarium wilt, gray mold and anthracnose; through the synergistic effects of hormone secretion, nutrient activation, disease inhibition and the like, the microbial agent comprehensively promotes root development and nutrient absorption of strawberry plants, promotes strawberry growth, remarkably improves the strawberry yield and fruit quality, and meanwhile remarkably reduces the strawberry storage rotting rate.
Owner:HUBEI MAOSHENG BIOLOGY CO LTD

Determination method of tandospirone and salt intermediate thereof

The invention relates to the field of pharmaceutical analytical chemistry, in particular to a method for determining tandospirone and salt intermediates thereof, high performance liquid chromatography is adopted, and chromatographic conditions include that a chromatographic column with octadecylsilane chemically bonded silica as a filler is adopted, and gradient elution is performed by a mobile phase A and a mobile phase B; wherein the mobile phase A consists of a first water phase and acetonitrile; the mobile phase B is composed of a second water phase and acetonitrile; the first water phase is a water solution containing monopotassium phosphate and sodium hexanesulfonate, and the pH value of the first water phase is 3.0-3.8; the second water phase is an aqueous solution containing monopotassium phosphate and sodium hexanesulfonate, and the pH value of the second water phase is 1.8-2.6. The testing method disclosed by the invention has good specificity, accuracy and repeatability, and can be used for monitoring the quality of the tandospirone raw material medicine.
Owner:SHENYANG HUATAI MEDICATION RES CO LTD

Planting method of selenium-rich apricots

The invention provides a selenium-rich apricot planting method, and belongs to the technical field of fruit tree planting. The planting method comprises the following steps: soil preparation and fertilization management; performing planting; fertilization: respectively carrying out topdressing before flowering, in a flower bud differentiation period and in a fruit expansion period; and harvesting. A fertilizer for topdressing is a selenium-rich fertilizer, and the selenium-rich fertilizer is composed of a microbial fertilizer, animal manure, waste plant rhizomes, monopotassium phosphate, urea and a substance containing a selenium element; the microbial fertilizer is prepared from saline-alkaline tolerant bacillus, pseudomonas and arbuscular mycorrhizal fungi. According to the selenium-rich fertilizer disclosed by the invention, the saline-alkaline tolerant bacillus, the pseudomonas and the arbuscular mycorrhizal fungi are added into the selenium-rich fertilizer, and the enrichment effect of apricot trees on selenium in soil is improved through the synergistic effect of the saline-alkaline tolerant bacillus, the pseudomonas and the arbuscular mycorrhizal fungi, so that the content of selenium in apricots is greatly increased.
Owner:QINGHAI UNIVERSITY +1

Growth-promoting macroelement water-soluble fertilizer as well as preparation method and application thereof

The invention belongs to the technical field of novel fertilizers, and particularly relates to a growth promoting type macroelement water-soluble fertilizer and a preparation method and application thereof.The fertilizer is prepared from, by weight, 4-6 parts of tertiary amine synergist, 220-230 parts of monopotassium phosphate, 350-360 parts of urea, 3-5 parts of compound amino acid, 3-5 parts of sorbitol and 15-20 parts of ethylene glycol, the invention relates to N, N '-tetra (2-fluorobenzyl diamido) diphenyl ether. The invention aims at innovating a macroelement water-soluble fertilizer product to prepare the novel tertiary amine synergist, so that the additional value and the use effect of the macroelement water-soluble fertilizer can be effectively improved, and a new direction and a new idea are provided for development and use of a new functional macroelement water-soluble fertilizer technology.
Owner:LIAONING PROVINCE DONGBEIFENGZHUANYONGFEI CO LTD

Steel plate enamel low-temperature matte glaze free of fluoride salt and nitrate as well as preparation method and application of steel plate enamel low-temperature matte glaze

ActiveCN121159098AMolten stateSilicic acid
The invention discloses fluoride salt-free and nitrate-free low-temperature matte glaze for steel plate enamel as well as a preparation method and application of the low-temperature matte glaze, and belongs to the technical field of enamel. The matte glaze is prepared from quartz, borax pentahydrate, sodium carbonate, titanium dioxide, magnesium oxide, monopotassium phosphate, calcium carbonate, zinc oxide, magnesium carbonate, lithium carbonate, aluminum oxide and zirconium silicate according to a specific mass ratio. The preparation method comprises the following steps: mixing the raw materials, melting at 1300 + / -10 DEG C in a pure oxygen environment, and quenching after wiredrawing to detect a molten state. The matte glaze completely avoids the use of fluoride salt and nitrate, the problems of fluoride emission and environmental protection equipment blockage are eliminated from the source, the fluorine content of the product is not detected through detection, and the limit value requirements of European Union REACH regulations are met. Zinc oxide and ZnO / TiO2 are added, so that the liquid phase viscosity is reduced, ion diffusion is accelerated, and the opacity (opacification performance) and gloss of the porcelain glaze are enhanced.
Owner:SINOPIGMENT & ENAMEL CHEM

Bacteria enrichment nutrient solution for fermentation and preparation method thereof

The invention relates to the technical field of bacterium enrichment nutrient solutions, in particular to a bacterium enrichment nutrient solution for fermentation and a preparation method of the bacterium enrichment nutrient solution. The culture medium is prepared from the following raw materials in parts by weight: maltodextrin, crystalline glucose, low-pigment yeast extract powder, refined soy peptone, dipotassium phosphate, monopotassium phosphate, magnesium sulfate heptahydrate, sodium chloride, phytic acid, L-ascorbic acid, manganese sulfate monohydrate, biotin, thiamine hydrochloride and choline chloride. Through a double-carbon-source structure, maltodextrin and crystalline glucose cooperate, metabolic oscillation is avoided, and the energy utilization rate is increased; the low-pigment yeast extract powder and the refined soy peptone are complementary, so that the rapid growth requirement of thalli is met; phytic acid is chelated with metal ions to prevent precipitation, L-ascorbic acid is used for resisting oxidation, and biotin and thiamine activate a coenzyme pathway to realize accurate regulation and control of a metabolic network.
Owner:SHANDONG YANGGU RUNXIN BIOPRODUCTS CO LTD

Double-liquid magnesium phosphate early-strength high-strength grouting material and preparation method thereof

The invention discloses a double-liquid magnesium phosphate early-strength high-strength grouting material and a preparation method thereof.The grouting material is composed of a liquid A and a liquid B. The liquid A is composed of powder A and water in parts by weight and comprises dead burned magnesia powder, a defoaming agent, steel slag powder, a retarder I and water, and the liquid B is composed of powder B and water in parts by weight and comprises powder B and water in parts by weight. Wherein the monopotassium phosphate, the superfine powder, the polymer rubber powder, the retarder II and the water have the advantages that the stirring time is shortened, the setting time is controllable, the flowability is good, the repair requirement can be met more quickly, the construction period is shortened, and the cane sugar and the borax are used as the retarders, so that the setting time can be controlled, and the early strength can be improved; surplus phosphate in a grouting material matrix is consumed by using the steel slag powder, so that some amorphous gel products can be generated, and the mechanical property is improved; the redispersible latex powder is utilized to form a polymer film in the slurry to wrap a hydration product, so that the water resistance is improved, and the synergistic modification effect is achieved.
Owner:ZHENGZHOU UNIV

Clay stabilizer for oil field as well as preparation method and application of clay stabilizer

ActiveCN119143926AHigh anti-expansion ratewashableDrilling compositionMeth-Ethyl group
The invention belongs to the technical field of oil exploitation, and particularly relates to a clay stabilizer for an oil field as well as a preparation method and application thereof. The preparation method comprises the following specific steps: adding lauryl amine, ethanol and allyl chloride into a reactor, introducing nitrogen, heating, controlling the temperature at 50-60 DEG C, and maintaining the pH value at 7-8; the preparation method comprises the following steps: adding 2-(allyldimethylsilyl) pyridine, 3-(methacrylamido) propyl dimethyl (3-sulfopropyl) ammonium inner salt, 1-vinyl-3-ethylimidazolium bromide, monopotassium phosphate and deionized water in sequence, adjusting the pH value to 7-8, and uniformly stirring; dropwise adding an initiator, heating to 65-70 DEG C when the mixed solution becomes thick after dropwise adding is finished, continuing to react for 4-8 hours, cooling to 30 DEG C or below, adding ethanol, precipitating, filtering and drying overnight to obtain a product, namely the clay stabilizer. The clay stabilizer disclosed by the invention has the advantages of high anti-swelling rate and washing resistance.
Owner:DONGYING ZHONGYUE PETROLEUM TECH CO LTD

Formula of sample eluent

The invention provides a formula of a sample eluent. The eluent comprises a surfactant, peptone with a concentration of 9 to 12 g / L, normal saline with a concentration of 7.2 to 9.6 g / L, tween-80 with a concentration of 0.8 to 1.2 g / L, disodium hydrogen phosphate with a concentration of 2.75 to 2.97 g / L and potassium dihydrogen phosphate with a concentration of 1.12 to 1.64 g / L. The eluent can effectively improve the sample recovery rate, and at least 90% of target substances can be successfully recovered after the eluent is treated by specific steps. In the use process, a dry and pollution-free sampling brush head needs to be completely immersed in the prepared eluent, then oscillation is carried out under set conditions to promote a target substance to be dissolved in the liquid, and finally the eluent is collected for subsequent analysis. The method is simple and convenient to operate, high in efficiency and very suitable for extracting and detecting various biological samples.
Owner:SHANGHAI JIANCAI MEDICAL EQUIP CO LTD

Method for converting livestock and poultry manure into organic fertilizer through microbial fermentation

The invention discloses a method for converting livestock and poultry manure into an organic fertilizer through microbial fermentation, and belongs to the technical field of livestock and poultry manure conversion. The method comprises the steps that firstly, the livestock and poultry manure is subjected to physical sorting, lime or monopotassium phosphate is added according to the pH value detection result, and the pH value is adjusted to 6.5-7.5; after determining nutrient components of the feces, adding soluble salt trace elements such as zinc sulfate and mixed carbohydrates of cane sugar and glucose; traditional strains of bacillus, lactic acid bacteria, saccharomycetes and actinomycetes are mixed with novel strains separated from the periphery of a livestock and poultry farm, optimized culture is conducted through a two-step culture method, and plant extracts such as lily extracts or livestock and poultry intestinal metabolites such as short-chain fatty acid are added in the culture process. The fermentation process adopts a rotatable fermentation tank body, and comprises three stages of fermentation of rapid heating, high-temperature stabilization and cooling decomposition. And finally, low-temperature vacuum drying, crushing, granulation and addition of a coating material are performed to prepare the organic fertilizer, so that efficient resource utilization of the livestock and poultry manure is realized.
Owner:CHINA AGRI UNIV

High-molecular polymer thickening agent as well as synthesis method and application thereof

The invention belongs to the technical field of oil exploitation, and particularly relates to a high-molecular polymer thickening agent as well as a synthesis method and application thereof. The synthesis method comprises the following steps: sequentially adding 4-trifluoromethyl cinnamic acid, deionized water, hydroxyethyl cellulose, TX-10 and monopotassium phosphate into a reactor, uniformly stirring, and adjusting the pH value to 7-8; 4, 4 '-diaminostilbene-2, 2'-disulfonic acid, 2-allyloxymethyl-2-methylolpropane-1, 3-diol and deionized water are added into a second reactor and stirred to be uniform, and the pH is adjusted to be 7-8; adding an initiator into a high-position dropwise adding tank, dropwise adding the initiator into the first reactor, continuously stirring, adding the mixed liquid in the second reactor when the viscosity begins to rise, continuously stirring, and then heating and carrying out heat preservation reaction to obtain viscous liquid; and drying and granulating to obtain the product thickening agent. The invention has the advantages of simple synthesis, high apparent viscosity, strong shear resistance, and good salt resistance and hardness resistance.
Owner:DONGYING SPRING PETROLEUM ENG TECH