892 results about "Crystal system" patented technology

A piezoelectric body contains a ferroelectric substance phase having characteristics such that, in cases where an applied electric field is increased from the time free from electric field application, phase transition of the ferroelectric substance phase to a ferroelectric substance phase of a different crystal system occurs at least two times. The piezoelectric body should preferably be actuated under conditions such that a minimum applied electric field Emin and a maximum applied electric field Emax satisfy Formula (1):

Emin<E1<Emax   (1)

wherein the electric field E1 represents the electric field at which the first phase transition of the ferroelectric substance phase begins.

The invention relates to one solid electrolyte materials and its process method for fix lithium battery, which is characterized by the following: Li2S and other sulfur compound B/S and A/I according to certain mole proportion for compounds to form non-crystal system to provide space for lithium ion transmission to get higher ion conductive rate, wherein, the materials have wider heat stable range to provide one ideal electrolyte prepare materials for solid lithium ion battery.

The invention relates to one solid electrolyte materials and its process method for fix lithium battery, which is characterized by the following:four types of different sulfur compounds as Li2S:A/S:P2S5=6:0.1-4.0:1.5 for compound to form non-crystal system to provide more effective paths for lithium ion transmission to get higher ion conductive rate; the said A for Ag, Zn, Al or Zr with sample of Li2S-ZrS2-P2S5 with room ion battery conductive rate as 9.60X10-6S/cm and lower electron conductive rate under 150 degrees for 3.30X10-4S/cm.

An actuator device includes: a layer provided on a single crystal silicon (Si) substrate, and made of silicon dioxide (SiO₂); at least one buffer layer provided on the layer made of silicon dioxide (SiO₂); a base layer provided on the buffer layer, and made of lanthanum nickel oxide (LNO) having the (100) plane orientation; and a piezoelectric element. The piezoelectric element includes: a lower electrode provided on the base layer, and made of platinum (Pt) having the (100) plane orientation; a piezoelectric layer made of a ferroelectric layer whose plane orientation is the (100) orientation, the piezoelectric layer formed on the lower electrode by epitaxial growth where a crystal system of at least one kind selected from a group consisting of a tetragonal system, a monoclinic system and a rhombohedral system dominates the other crystal systems; and an upper electrode provided on the piezoelectric layer.

A piezoelectric body contains a ferroelectric substance phase having characteristics such that, in cases where an applied electric field is increased from the time free from electric field application, phase transition of the ferroelectric substance phase to a ferroelectric substance phase of a different crystal system occurs at least two times. The piezoelectric body should preferably be actuated under conditions such that a minimum applied electric field Emin and a maximum applied electric field Emax satisfy Formula (1)wherein the electric field E 1 represents the electric field at which the first phase transition of the ferroelectric substance phase begins.

High efficiency viscosity-reducing agent which is used on THE thermal oil extraction technology, which is formed by the following raw materials with percentage by weight, firstly phenyl benzene, fused ring aromatic hydrocarbon or fused ring aromatic hydrocarbon derivative which does not contain chlorine element and sulfur element, secondly liquid petroleum product whose aromatic hydrocarbons content is no more than 5%, petroleum resin which is liquid state under the constant temperature or hydrocarbons natural aggregation which is particle state under the constant temperature, thirdly water-soluble anionic surface active agent, water-soluble non-ionic surface active agent, oil solubility anionic surface active agent or oil solubility non-ionic surface active agent, fourthly fusel oil, fifthly alcohol ether, sixthly oil solubility or water-soluble polymer which respectively has nonpolar portion which has eutectic crystal with ceresin wax molecular and polar portion which can make wax crystal system twisty on main chain and or branch chain, seventhly hyperoxide, eighthly carbamide, ammonium carbonate, ammonium acid carbonate or ammonium nitrite and ninthly ketone. The high efficiency viscosity-reducing agent has strong suitability, strong viscosity-reducing ability, safety and reliability, can largely reduce extract cost and increase the yield of oil pump, and increases the final recovery efficiency of oil reservoir.

The method of measuring crystallographic orientations, crystal systems or the like of the surface of a specimen has steps of: irradiating the specimen with an ion beam; measuring tho secondary electrons generated by the irradiation of the ion beam; repeating the irradiation of the ion beam and the measurement of the secondary electrons with each variation in an angle of incidence of the ion beam with respect to the specimen; and determining the crystalline state based on the variation in the amount of the secondary electrons corresponding to the variation of the angle of incidence.

A preparation method for bismuth(Bi)-tellurium(Te) nano-porous thermoelectric semiconductor material is disclosed, belonging to the technical field of the thermoelectric material. The preparation method comprises the following step: Bi-Te-based nano-powders Bi[2-x]Sb[x]Te[3-y]Se[y] (x=0-1.9, y=0-0.5) are placed in alcohol solution with a pore-forming agent sufficiently dissolved therein, in orderto be mixed by a method which combines ultrasonic wave with magnetic suspension agitation, the powders are sintered into bulk material by means of a discharge plasma sintering technology after being dried, and during the sintering, the pore-forming agent is utilized for sublimation and evaporation at the particular temperature so that the bulk material can form nano-sized pore structure therein inthe process of sintering in order to form the nano-porous material. The Bi-Te-based alloy belongs to rhombohedral crystal system structure. The preparation method has the advantages of simple preparation, easy operation, lower cost, accurate ingredient control, relatively uniform size and distribution of the nano pores and the like.

One embodiment of communication system comprises a crystal oscillator configured to output a reference clock; cellular radio frequency (RF) and baseband phase locked loops configured to receive the reference clock within a cellular module and compensate for calculated frequency errors between a received cellular downlink signal and a cellular local oscillator signal during operation of the cellular module; global positioning system (GPS) frequency compensation circuitry configured to receive the reference clock within a GPS module and compensate for calculated frequency errors during operation of the GPS module; and a temperature sensing circuit which includes a plurality of sensing resistors and is configured to output a signal corresponding to a temperature of a reference crystal which is translated to a frequency deviation, wherein the (GPS) frequency compensation circuitry is configured to offset the frequency deviation and output a temperate compensated signal to meet GPS clock frequency requirements.

The invention relates to a large size potassium strontium borate nonlinear optical crystal, the preparation and use thereof. The formula of the crystal is: KSr4B3O9, which belongs to rhombic system, the space group is Pna2(1), and the molecular weight is 566.01, and the crystal size is 10-60mmx10-60mmx10-60mm. The preparation contains the following steps of: evenly mixing the potassium strontium borate compound with a fusing assistant, heating, maintaining the constant temperature, cooling to the saturation temperature and obtaining a mixture solution, placing a seed crystal into the mixture solution, lowering the temperature to the saturation temperature to obtain the required crystal, and subsequently extracting the crystal from the liquid level, cooling to room temperature, and finally obtaining the large size potassium strontium borate nonlinear optical crystal. The nonlinear optical effect of the crystal is approximately the same as the KDP, the transparent optical band is 220nm-3000nm. The crystal is simple in operation, low in cost, large in crystal size, short in growth period, less in coating, high in laster damage threshold, good in mechanical property, firm, stable in physicochemical properties, uneasy to deliquescence, convenient for processing and storage, or the like. Accordingly, the nonlinear optical crystal of the invention can be abroadly applied in nonlinear optical devices such as frequency doubler, optical parametric oscillator or the like.

The invention provides a method for synthesizing a heteroatomic ZSM-5 molecular sieve. The method comprises the steps of (a) adding a gallium source and an aluminum source into a templating agent, then adding sodium hydroxide, and then mixing with a silicon source to form a sol-gel system; (2) crystallizing for 48-80 hours; (3) filtering, drying and roasting to remove the organic templating agent; and (4) carrying out ion exchange on molecular sieve powder by using an ammonium hydroxide solution to obtain the hydrogen-type molecular sieve. According to the synthesis method provided by the invention, the molecular sieve, which is synthesized directly from the inexpensive silicon source, gallium source, aluminum source, mineralizer and organic templating agent, is unnecessary to be subjected to subsequent micropore aperture adjustment. The synthesized heteroatomic ZSM-5 molecular sieve belongs to an MFI structure and no heterophase crystal systems appear. Compared with a conventional ZSM-5 molecular sieve, the heteroatomic ZSM-5 molecular sieve synthesized by the method provided by the invention has the advantages that biomass and polyethylene are rapidly pyrolyzed under the catalytic action of the heteroatomic ZSM-5 molecular sieve, the yield of monocyclic aromatic hydrocarbon is not reduced and the selectivity of benzene, toluene and p-xylene in aromatic hydrocarbon is improved by about 80%.

A ferroelectric capacitor includes a lower electrode, a ferroelectric film provided over the lower electrode and having a perovskite-type structure and an upper electrode provided over the ferroelectric film. The ferroelectric film includes a first ferroelectric film part having a first crystal system and formed along at least one interface with at least one of the lower electrode and the upper electrode and a second ferroelectric film part having a second crystal system that is different from the first crystal system.

The invention belongs to the technical field of a microporous metal-organic framework material and particularly relates to a microporous metal-organic framework material based on isophthalic acid derivatives as well as a preparation method and an application thereof. The chemical formula of the microporous metal-organic framework material provided by the invention has a chemical formula of Zn(pybdc), wherein pybdc<2-> is deprotonated 5-(1-pyrrolidyl)-1,3-phthalic acid and n represents an infinite link of the structural unit. The metal-organic framework material provided by the invention is crystallized in a trigonal system and the space group is R-3m; the metal Zn<2+> is located in the center of a tetrahedron and is tetrachordinate. The microporous metal-organic framework material provided by the invention has a one-dimensional porous channel structure along the direction of axis c and a methylene group of a pentary pyrrole ring stretches into the porous channel; the window of the porous channel is about 4 angstroms and the porosity is 18.6%. The structure of the material provided by the invention has the porous channel, so that the material can be used for safely storing gas or solvent molecules.

Provided is a manufacturing method for preferentially-oriented oxide ceramics having a high degree of crystal orientation. The manufacturing method includes: obtaining slurry containing an oxide crystal B having magnetic anisotropy; applying a magnetic field to the oxide crystal B, and obtaining a compact of the oxide crystal B; and subjecting the compact to oxidation treatment to obtain preferentially-oriented oxide ceramics including a compact of an oxide crystal C having a crystal system that is different from a crystal system of one of a part and a whole of the oxide crystal B. By (1) reacting raw materials, (2) reducing the oxide crystal A, or (3) keeping the oxide crystal A at high temperature and quenching the oxide crystal A, the oxide crystal B is obtained to be used in the slurry.

The present invention relates to positive electrode active substance particles comprising a compound having at least a crystal system belonging to a space group of R−3m and a crystal system belonging to a space group of C2/m, and boron, wherein the compound is a composite oxide comprising at least Li, Mn, and Co and/or Ni; a relative intensity ratio [(a)/(b)] of a maximum diffraction peak intensity (a) observed at 2θ=20.8±1° in a powder X-ray diffraction pattern of the positive electrode active substance as measured using a Cu-Ka ray to a maximum diffraction peak intensity (b) observed at 2θ=18.6±1° in the powder X-ray diffraction pattern, is 0.02 to 0.5; a content of Mn in the positive electrode active substance particles is controlled such that a molar ratio of Mn/(Ni+Co+Mn) therein is not less than 0.55; and the positive electrode active substance particles comprise the boron in an amount of 0.001 to 3% by weight. The positive electrode active substance particles of the present invention are produced by calcining a mixture comprising precursor particles comprising Mn, and Ni and/or Co, a lithium compound and a boron compound at a temperature of 500 to 1500° C. The positive electrode active substance particles of the present invention can provide a secondary battery which can be improved in charge/discharge capacity and cycle characteristics.

The invention discloses a near blue fluorescent material and a preparation method thereof. The material is prepared through chemical reactions of quinoline carboxylic acid and 4,4'-bipyridine with conjugated extended pi bonds, and zinc ions with optical activity. The fluorescent material is a zinc quinoline carboxylic crystal with a molecular formula of C84H56N8O8Zn2. The crystal belongs to a crystal system of triclinic system, and a space group of P-1. Cell parameters of the crystal are that: alpha= 91.357 DEG, gamma=106.573 DEG, and beta=101.953DEG. The zinc ions have two coordination modes, one is a square pyramid coordination mode, wherein two nitrogen coordinating atoms come from two different 4,4'-bipyridines, and three oxygen coordinating atoms come from two different quinoline carboxylic acid ligands; the other is a octahedral coordination mode, wherein two nitrogen coordinating atoms come from two different 4,4'-bipyridines, and four oxygen coordinating atoms come from two different quinoline carboxylic acid ligands. The material is advantaged in that: the fluorescent material contains abundant optically active Zn (II) ions and conjugated extended bonds, and has good near blue light emission performance.

The invention discloses a convenient method for directionally cutting any crystal face of crystal, belonging to the technical field of crystal material cutting processing. The method is implemented by cutting out a plane arbitrarily to be as the reference plane, then determining longitudinal, transverse and normal indexes of the reference plane by using electron backscattered diffraction (EBSD) technology, then calculating the needed included angle between the reference plane and any crystal face, and finally regulating the crystal cutting direction to obtain the crystal face satisfying requirements by once cutting processing. With the EBSD technology adopted, the EBSD instrument and the traditional crystal material cutting device are combined, thus the crystal of any crystal system can be cut out any crystal face in directional way, namely, the needed crystal face is a high index diffraction face or an extinction face, the invention is especially suitable to the crystal with unknown reference plane orientation and larger crystal orientation deviation, and the bearing accuracy is high, the operation is simple and convenient and the crystal consumption is reduced.

The invention discloses a high magnetic-energy-product M type calcium series permanent magnetic ferrite material and a preparation method thereof. The high magnetic-energy-product M type calcium series permanent magnetic ferrite material is a hexagonal crystal system, and the chemical structural formula is R1-x-yCaxLayO.nFe(12-z)/nCoz/nO3, wherein x is greater than or equal to 0.001 and smaller than or equal to 0.4, y is greater than or equal to 0.001 and smaller than or equal to 0.5, z is greater than or equal to 0.01 and smaller than or equal to 2.0, 1-x-y is greater than 0.2 and smaller than or equal to 0.998, n is greater than or equal to 5.0 and smaller than or equal to 6.5. R is Sr or adopts Sr as the main component, and also contains one, two or three of Ba, lanthanide series Ce, Pr, La, Nd and Sm. When R is Sr and Ba, the content of Sr and Ba is less than or equal to 0.998. In addition to high residual magnetism and intrinsic coercivity, the high magnetic-energy-product M type calcium series permanent magnetic ferrite material provided by the invention also has higher magnetic induction coercivity and maximum magnetic energy product, and is particularly in favor of miniaturization of permanent magnetic ferrite devices.

The invention relates to a process for preparing calcium carbonate with different crystal forms by employing chitosan, which belongs to the biomimetic materials field. The steps of the invention comprise adding chitosan in water solution with calcium chloride and urea according to a certain proportion and controlling modality of chitosan molecular chain to hydro-thermally synthesize calcium carbonate with different crystal form via changing pH of reaction solution. The invention realizes the method of synthesizing calcium carbonate with different crystal forms by manual work, and is expected to be applied to the biomineralization process and synthesis of biomineralization materials.

The invention provides novel non-linear optical crystal gallium germanium barium sulfide, and a growing method and application thereof. The chemical formula is BaGa2GeS6 (short for BGGS). The novel non-linear optical crystal gallium germanium barium sulfide has the chemical formula of BaGa2GeS6, has an asymmetrical center structure and belongs to a trigonal crystal system, wherein the space group is R3; and cell parameters are that: a=9.5967(5) Angstrom, b=9.5967(5) Angstrom, c=8.6712(7) Angstrom, alpha=90 degrees, beta=90 degrees, gamma=120 degrees, Z=1, and V=691.62 Angstrom3. The clock multiplier factor of the BaGa2GeS6 is 0.8 time that of AgGaS2. The BGGS compound is obtained by sintering at high temperature through a solid phase synthesis method. The BGGS monocrystal can grow successfully by a crucible descending method. The BaGa2GeS6 has a non-linear optical effect, is not dissolved in dilute acid, has high chemical stability, can be widely applied in various non-linear optical fields, and can develop non-linear optical application of a middle infrared band.

Provided is a deposited film containing microcrystalline silicon by plasma CVD, which includes changing at least one of conditions selected from a high frequency power density, a bias voltage with respect to an interelectrode distance, a bias current with respect to an electrode area, a high frequency power with respect to a source gas flow rate, a ratio of a diluting gas flow rate to a source gas flow rate, a substrate temperature, a pressure, and an interelectrode distance, between conditions for forming a deposited film of a microcrystalline region and conditions for forming a deposited film of an amorphous region; and forming a deposited film under conditions within a predetermined range in the vicinity of boundary conditions under which the crystal system of the deposited film substantially changes between a amorphous state and a microcrystalline state.