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1958 results about "Reduction rate" patented technology

Silicon-carbon composite negative pole material preparation method and lithium ion battery

The invention relates to a silicon-carbon composite negative pole material preparation method and a lithium ion battery. The preparation method comprises putting nanometer silicon and graphite micro-powder into a ball mill, carrying out ball milling uniform dispersion in an organic solvent environment, carrying out vacuum drying, putting the dried mixture and asphalt into a cone-type mixer, carrying out coarse mixing, putting the mixed powder subjected to coarse mixing into a mechanical fusion machine, carrying out mechanical fusion, carrying out heat treatment in an inert gas protective atmosphere and carrying out cooling to obtain the silicon-carbon composite negative pole material. The preparation method carries out asphalt softening coating on nanometer silicon so that silicon particle and electrolyte direct contact is avoided, a capacity reduction rate is delayed, a lithium ion diffusion path is shortened, an electrode material electron conduction loss is avoided, and first charge-discharge efficiency, a charge-discharge electric capacity and cycle performances are improved. Before coating, nanometer silicon is dispersed through graphite micro-powder so that it is avoided that in asphalt coating, nanometer silicon aggregation causes local capacity excess and nanometer silicon is uniformly dispersed.
Owner:浙江超恒动力科技有限公司

Preparation method and application of unsaturated polyether

The invention relates to a preparation method and application of unsaturated polyether. The preparation method comprises the following steps: (1) adding unsaturated alcohol and a catalyst into a first reactor, replacing with nitrogen, continuously adding epoxide with short branches and reacting to obtain an intermediate product A, wherein the unsaturated alcohol is one or a mixture of more than two of methyl allyl alcohol and isoamyl alcohol at any proportion and the mass ratio of the unsaturated alcohol to epoxide is 1.0:(0.1-5.0); and (2) putting the intermediate product A obtained in the step (1) and the catalyst into a second reactor, replacing with nitrogen, continuously introducing ethylene oxide and reacting to obtain polyether B, and neutralizing the pH value of the polyether B product to be 5-7 with a neutralizing reagent, wherein the mass ratio of the intermediate product A to ethylene oxide is 1.0:(15.0-51.0). The invention also provides the unsaturated polyether prepared by the preparation method, which is disclosed by the invention and application of unsaturated polyether in synthesis of polycarboxylic water reducer and the water reducer prepared from the unsaturated polyether synthesized by the method has the advantages of low doping amount, high water reduction rate, good slump-retaining agent and like.
Owner:HONGBAOLI GRP CO LTD

High-strength non-oriented electrical steel with high magnetic induction and manufacturing method thereof

InactiveCN102453838AHigh strengthSolve the problem of difficult rollingReduction rateElectrical steel
High-strength non-oriented electrical steel with high magnetic induction and a manufacturing method thereof. The method comprises the following steps of: 1) smelting and casting, wherein the electrical steel comprises the following components by weight: not more than 0.0040% of C, 2.50-4.00% of Si, 0.20%-0.80% of Al, 1.0-8.0% of Cr, 0.5-5.0% of Ni, not more than 0.50% of Mn, not more than 0.30% of P, not more than 0.0020% of S, not more than 0.0030% of N, not more than 0.0030% of Ti, not more than 0.010% of Nb, not more than 0.010% of V, not more than 0.010% of C+S+N+Ti, and the balance of Fe; smelting, RH vacuum treatment, casting; 2) hot rolling; 3) normalization at a temperature of 850-950 DEG C for 0.5-3 min, slow cooling to 650-750 DEG C with a speed of 5-15 DEG C / s, rapid cooling to below 100 DEG C with a speed of 20-70 DEG C; 4) pickling and cold rolling with a total reduction rate of not less than 70%; 5) annealing at 800-1000 DEG C for 5-60 seconds, slow cooling to 650-750 DEG C with a speed of 3-10 DEG C / s, rapid cooling to below 100 DEG C with a speed of 20-70 DEG C. The method of the invention produces non-oriented electrical steel with both high strength and high-efficient magnetic properties without the increase of manufacturing difficulties.
Owner:BAOSHAN IRON & STEEL CO LTD

Method for producing ferritic stainless steel bands with roughened surfaces through cold continuous rolling

A method for producing ferritic stainless steel bands with roughened surfaces through cold continuous rolling comprises that (1), a five-rack serial type cold continuous rolling is performed, a five-rack serial type cold continuous rolling unit is adopted, the diameter of a working roll of each rolling mill is 300-500mm, and endless rolling is performed; the roughness degrees of the rolls of the first rack to the fourth rack are in a range of 0.5-1.0mum and decrease sequentially; the working roll of the fifth rack is subjected to roughening and chromium plating treatment; an emulsion lubrication rolling mode is adopted, the temperature of an emulsion is 50-60DEG C, the emulsion is sprayed to roll gaps for cooling and lubricating, the temperature of cold-rolled band steel is controlled below 150DEG C; the accumulated reduction rate of the first rack to the fourth rack is larger than 60%, the reduction rate of the fifth rack is in a range of 4-10%, and the roughness of the cold-rolled band steel is controlled in a range of 0.5-1.0mum; (2), the cold-rolled band steel is subjected to annealing acid picking treatment, heating and annealing are performed in a continuous horizontal gas furnace, the annealing temperature is in a range of 800-1000DEG C, and recrystallization of the band steel is finished; finished surfaces are obtained finally through electrolytic picking by Na2SO4 and H2SO4 solutions and soaking picking by a nitric acid and hydrofluoric acid mixed acid solution sequentially after annealing.
Owner:BAOSTEEL DESHENG STAINLESS STEEL

Ultrafine grained hot rolled dual-phase steel with tensile strength of above 750MPa and manufacturing method of plate thereof

The invention relates to ultrafine grained hot rolled dual-phase steel with tensile strength of above 750MPa and a manufacturing method of a plate thereof, belonging to the technical field of steel rolling, and the dual-phase steel comprises the following chemical components by weight percentage: 0.06-0.16% of C, 0.10-0.50% of Si, 1.00-2.00% of Mn, 0.02-0.06% of Al, 0.01-0.08% of Nb, 0-0.03% of Ti, not more than 0.1 of P, not more than 0.05 of S and the balance of Fe. The manufacturing method of the dual-phase steel comprises the following steps: 1) heating, heating a plate blank with the thickness of not less than 60mm to 1100-1250 DEG C, and keeping the temperature for 1-4h; 2) rolling and adopting the two-stage controlled rolling, wherein the reduction rate in a recrystallization zone is larger than 60%, the reduction rate in a non-recrystallization zone is larger than 70%, the initial rolling temperature of the recrystallization zone is 1100-1150 DEG C, the initial rolling temperature of the non-recrystallization zone is 880-940 DEG C, and the final rolling temperature is 770-860 DEG C; and 3) cooling, and adopting the continuous cooling after final rolling, wherein the cooling rate is 30-40 DEG C/s, the coiling temperature is lower than 350 DEG C, and the thickness of a finished product is 2-10mm. The manufacturing method can obtain the high-performance steel plate with high strength, low yield-strength ratio and good extension property, and the steel plate can be suitable for forming processing of high-strength automobiles, other industrial mechanical parts and the like.
Owner:NORTHEASTERN UNIV

Wear and corrosion resistant castable prepared from bauxite-based homogenous material and preparation method thereof

ActiveCN101885617AUniform structureSmall fluctuations in water addition during constructionPliabilityCement kiln
The invention discloses wear corrosion resistant castable prepared from a bauxite-based homogenous material and a preparation method thereof, which belong to the technical field of castable refractory. In the invention, by using the characteristics of the bauxite-based homogenous material, such as homogeneous chemical components and structure, stable performance, mulite main crystal phase, small linear change, high high-temperature strength and certain flexibility due to mutual insertion of micro crystals and the like, the shortcomings of low middle-temperature strength and poor wear resistance and alkali corrosion resistance of the conventional high-aluminum bauxite castable are overcome, and the problems of low middle-temperature strength, poor wear resistance and poor alkali, chloride and sulphur corrosion resistance of the conventional high-aluminum and corundum castable are effectively solved. The wear and corrosion resistant castable with high middle-temperature performance is prepared. The wear corrosion resistant castable and the preparation method thereof have the advantages of small fluctuation of water adding amount in construction, stable usability, reduction rate of partial corrosion, prolonged service life and wide application to a kiln hood, a grate cooler, a tertiary air duct and a decomposing furnace of a dry process cement kiln and relative parts of other ceramic and petrified thermo-technical kilns and the like.
Owner:YANGQUAN JINYU TONGDA HIGH TEMPERATURE MATERIALS +1

Fire-resistant and earthquake-resistant steel for construction and production method thereof

The invention relates to a fire-resistant and earthquake-resistant steel for construction. The steel comprises the following components by weight percent: 0.1-0.18 % of C, 0.1-0.50 % of Si, 1-1.80 % of Mn, less than or equal to 0.025 % of P, less than or equal to 0.015 % of S, less than or equal to 0.50 % of Cr, less than or equal to 0.30 % of Mo, less than or equal to 0.04 % of Al, less than or equal to 0.007 % of N, less than or equal to 0.006 % of Ca, one or two or more of less than or equal to 0.050 % of Nb, less than or equal to 0.055 % of V and less than or equal to 0.035 % of Ti, with Nb+V+Ti being <= 0.055 %, and the balance being Fe and unavoidable impurities. A production method comprises heating under a temperature of 1180 DEG C, insulating for 3 hours, rolling with a starting temperature of not less than 1180 DEG C, an accumulated reduction rate of last three controlled rolling being not less than 35 %, and a terminating temperature of 860 to 900 DEG C, and then directly air-cooling to a room temperature or cooling with a rate of 5 to 15 DEG C per second to the room temperature. The obtained steel is excellent in fire resistance, low in yield ratio (Rp0.2/Rm <= 0.75), and good in earthquake-resistance performance, with Rp0.2 (yield strength at 600 DEG C) / Rp0.2 (yield strength at the room temperature) >= 2/3.
Owner:BAOSHAN IRON & STEEL CO LTD +1

High crack-arresting toughness steel plate with yield strength of 500MPa and production method thereof

The invention provides a high crack-arresting toughness steel plate with yield strength of 500MPa and a production method thereof. The chemical components of steel comprises the following components in percentage by weight: 0.04-0.08% of C, 0.10-0.5% of Si, 0.8-1.6% of Mn, not more than 0.02% of P, not more than 0.01% of S, 0.03-0.065% of Al, not more than 0.005% of N, 0.005-0.05% of Nb, 0.005-0.03% of Ti, 0.0005-0.003% of B, not more than 0.004% of Ca, and the balance of Fe and avoidless impurities. The preparation method comprises the steps of roughing in an austenite re-crystalline region in a first stage, wherein the rolling temperature is 1000-1130 DEG C, the total reduction rate in the re-crystalline region is greater than or equal to 50%; cooling a rolled steel plate quickly to 580-530 DEG C at a rate of 10 DEG C/s; rolling in a non-re-crystalline region in a second stage when the temperature of the surface of the steel plate is 720-770 DEG C, wherein the accumulated deformation is greater than or equal to 50%, the finish rolling temperature is 700-740 DEG C; and water-cooling after rolling, wherein the cooling rate is 5-15 DEG C/s, and the final cooling temperature is 460-560 DEG C. The high crack-arresting toughness steel plate provided by the invention has the characteristics of high strength, high toughness, inhibition of crack formation and expansion and the like, and meets the performance requirements of special part members of large container ships.
Owner:ANGANG STEEL CO LTD

Phosphates adhesive and preparation method thereof

The present invention discloses a phosphate adhesive and a preparation method thereof, which relate to an adhesive and a preparation method thereof. The present invention resolves the problem that the curing and heat-resisting capabilities of the prior phosphate adhesive are impaired under the room temperature. The phosphate adhesive of the present invention is prepared with phosphoric acid solution, aluminum hydroxide powder, aluminum oxide powder, zirconium oxide powder and zinc oxide powder or aluminum nitride powder. The preparation method includes the following steps: (1) the materials are weighed out; (2) the phosphoric acid solution is mixed with the aluminum hydroxide powder so that aluminum dihydrogen phosphate matrix resin can be made; (3) the aluminum oxide powder, the zirconium oxide powder and the zinc oxide powder or the aluminum nitride powder are mixed together so that curing agent is prepared; (4) the aluminum dihydrogen phosphate matrix resin and the curing agent are mixed together, and after being cured under the room temperature, the phosphate adhesive is prepared. The phosphate adhesive of the present invention can be cured under the room temperature and can resist a temperature up to 1580 DEG C, moreover, the water-resisting property of the phosphate adhesive of the present invention is good, and after the phosphate adhesive is soaked in tap water under the room temperature for 100 days, the reduction rate of the adhering strength of the phosphate adhesive is less than 10 percent.
Owner:INST OF PETROCHEM HEILONGJIANG ACADEMY OF SCI

Fluidized low-temperature reduction device and reduction method for powdery manganese oxide ores

ActiveCN102363837ALow thermal decomposition rateAvoid formingCombustion chamberRetention time
The invention relates to a fluidized low-temperature reduction device and a fluidized low-temperature reduction method for powdery manganese oxide ores. The device comprises a feeding unit, a preheating unit, a reduction roasting unit and a cooling unit which are connected from top down, wherein the reduction roasting unit is connected with a combustion chamber; and the combustion chamber is connected below the preheating unit. In the reduction method, tail gas formed in the reduction process enters the combustion chamber combusts with supplementary gas and air to form flue gas; and the flue gas is subjected to countercurrent heat exchange with the manganese oxide ores. The fluidized low-temperature reduction device and the reduction method have the advantages that: the gas can be used as a reducer and also can be used as fuel; and the utilization rate of the gas is 100 percent. In the reduction device, the reduction temperature of the manganese oxide ores is low, so a manganese-containing phase which is insoluble to sulfuric acid is avoided, and heat carried by the manganese oxide ores is reduced by over 30 percent. The manganese oxide ores in a fluidized reduction roasting furnace are in the bubbling fluidized state, the heat transfer efficiency, the mass transfer efficiency and the reaction efficiency are high, the distribution of retention time is uniform, and the reduction rate of the manganese oxide is more than 98 percent.
Owner:深圳中科九台资源科技有限公司

Method for rolling liquid core under heavy reduction rate by virtue of online thickness regulating roll by utilizing continuous casting machine

The invention relates to a method for rolling a liquid core under heavy reduction rate by virtue of an online thickness regulating roll by utilizing a continuous casting machine. The method comprises the following steps of: when two rolling mills are loaded, setting a target thickness, feeding back the thickness value in real time and detecting oil pressure, carrying out conversion on a rolling force to judge whether the rolling force is higher than a limit value, if the rolling force is lower than the limit value, stabilizing rolling until the rolling is finished; if the rolling force is higher than the limit value, regulating and judging the rolling force again; if the target thickness is changed in the rolling process, calculating thickness variation by virtue of a rolling process computer, regulating roll gap of the two rolling mills to be the target thickness, and judging whether the rolling force is higher than the limit value again. In the method provided by the invention, a rolling signal can be changed to change the target thickness in the rolling process, and a wedge-shaped blank is rolled. By applying the method provided by the invention, the quality of a continuous casting can be better improved, the continuous casting and the wedge-shaped blank can be rolled, and the time of a process is reduced while the yield is improved; meanwhile, structure of equipment is simple, investment is less, control is simple, reliability is high, and energy can be greatly saved, thus the method has a good popularization and application prospect.
Owner:SHEN KAN QINHUANGDAO GENERAL ENG DESIGN & RES INST CORP MCC

High intensity and high ductility -50 DEG C low-temperature steel and manufacturing method thereof

InactiveCN101381841AHigh strengthStable and excellent low temperature toughnessReduction rateChemical composition
The invention discloses high-strength high-toughness low-temperature steel at 50 DEG C below zero and a manufacturing method thereof, and belongs to the manufacturing field of low alloy steel. The low-temperature steel comprises chemical compositions in percentage by weight: 0.12 to 0.20 percent of C, 0.15 to 0.50 percent of Si, 1.20 to 1.70 percent of Mn, less than or equal to 0.015 percent of P, less than or equal to 0.010 percent of S, 0.30 to 1.00 percent of Ni, 0.005 to 0.050 percent of Ti, 0.005 to 0.10 percent of Al, 0.010 to 0.050 percent of Nb, one or more than one of less than or equal to 0.10 percent of V, less than or equal to 1.0 percent of Cu, less than or equal to 0.50 percent of Mo, less than or equal to 0.040 percent of Zr, and less than or equal to 0.20 percent of RE, and the balance being Fe. The manufacturing method for the steel comprises the following steps: the heating temperature of steel billets is between 1, 150 and 1, 280 DEG C, the heating rate is between 8 and 14 minute/centimeter, the initial rolling temperature of the steel is more than or equal to 1, 100 DEG C, the accumulated reduction rate of control rolling is more than or equal to 60 percent, the reduction rate of each of final three passes is more than or equal to 10 percent, and the final rolling temperature is between 780 and 860 DEG C; and the normalizing heat treatment is adopted, the keeping temperature of the normalization is between 850 and 930 DEG C, and the keeping time is 30-50 minutes+plate thickness (millimeters) x 1 minute/millimeter.
Owner:武汉钢铁有限公司

Sustained-release polycarboxylic high-performance water reducing agent and preparation method thereof

The invention relates to a sustained-release polycarboxylic high-performance water reducing agent and a preparation method thereof. The water reducing agent comprises: 0.13mol of monomer methyl alkenyl polyoxyethelene or allyl polyoxyethylene ether or polyoxypropylene ether, 0.32mol of monomer acrylic acid or methacrylic acid, 0.01mol of monomer sodium methallyl sulfonate, 0.12mol of monomer acrylamide or 2-acrylamide-methylpropanesulfonic acid, and 0.05mol of monomer ethyl acetate or styrene. Deionized water is adopted as a reaction medium, and the materials are subjected to a reaction with an initiating agent and a chain transfer agent for 4-6h with a maintained temperature of 58-62 DEG C. Copolymerization is carried out, such that a polymer with a molecular weight of 50000-120000 is obtained; the temperature is reduced to below 40 DEG C, and an alkali solution is added for regulating the pH of the system to 6-8, such that the water reducing agent is obtained. The sustained-release polycarboxylic high-performance water reducing agent provided by the invention has high water reduction rate. When an equivalent solid dosage is 0.2%, a water reduction rate can reach 35%. A slump performance is good. Concrete slump and extension degree have no loss in 3h. The water reducing agent is widely adaptable with concrete raw materials.
Owner:广西云鹰新材料科技有限公司

Manganese ore reduction calcination method and apparatus

InactiveCN101413056AFeeding is automatic and uniformEasy to overflowReduction rateLower grade
The invention discloses a method and a device for reducing and roasting manganese dioxide into manganese monoxide in electrolytic manganese industry. The method comprises the following steps: dried manganese dioxide mineral powder is ground, well mixed with reducing powder and conveyed to a feeding bin on the top of a roasting furnace, and then enters hermetic roasting devices; a plurality of burners are arranged among the hermetic roasting devices; fuel is burnt so as to roast manganese dioxide ore; the manganese dioxide ore and the reducing powder are heated and roasted to 900 to 970 DEG C in the hermetic roasting devices with no oxygen supplement; under the circumstance of oxygen-free contact after reaction in the lower ends in the hermetic roasting devices, the temperature of roasted manganese ore is lowered, so as to recover heat and cool the manganese ore; and finally, the manganese ore is discharged out of a furnace by an automatic discharging device and then is subjected to a subsequent process. The method and the device can reduce and roast the high/low-grade manganese dioxide ore, have the advantages of low production cost, simple process and convenient operation, can control the reduction rate of manganese dioxide and other metals through the automatic discharging device, and improve the quality of final products.
Owner:朱军

Austenitic stainless steel with excellent polishing performance and manufacturing method thereof

The invention discloses an austenitic stainless steel with excellent polishing performance. The austenitic stainless steel comprises the following chemical components in percentage by weight: 16 to 20 percent of Cr, 7 to 15 percent of Ni, less than or equal to 2 percent of Mn, 0.2 to 2 percent of Cu, less than or equal to 0.05 percent of Al, less than or equal to 0.5 percent of Si, 0.03 to 0.1 percent of C, less than or equal to 0.05 percent of N, 0.01 to 0.06 percent of P, 0.003 to 0.05 percent of S, 0.05 to 0.5 percent of V, and the balance of iron and inevitable impurities. A manufacturing method for an austenitic stainless steel cold-rolled plate comprises the following steps of: heating a continuous cast plate blank to the temperature of between 1,100 and 1,300 DEG C; performing rough rolling at the temperature of between 1,000 and 1,250 DEG C; performing final rolling at the temperature of between 950 and 1,100 DEG C; performing quick cooling; coiling at the temperature of less than 700 DEG C; performing hot rolling to form a hot-rolled plate of the required specification; annealing the hot-rolled plate at the temperature of between 950 and 1,200 DEG C; removing oxide skin by adopting a continuous acid washing process of phosphorus breakage, shot blasting, electrolysis and mixed acid washing; performing cold rolling, wherein the overall reduction rate is more than 50 percent; and performing continuous annealing at the temperature of between 950 and 1,200 DEG C, or performing full-hydrogen bright annealing at the temperature of between 950 and 1,200 DEG C. The austenitic stainless steel cold-rolled plate has completely improved grinding performance and surface polishing performance, and is particularly suitable for the industries of building decoration, plastic dies, food sanitation, electronics and the like with strict polishing performance requirements.
Owner:BAOSHAN IRON & STEEL CO LTD
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