3149results about How to "Uniform structure" patented technology

The invention discloses a method for preparing aerogel materials by combining hydrothermal synthesis technology and sol-gel technology. The prepared aerogel comprises one or more of alumina aerogel, silica aerogel, zirconia aerogel and titania aerogel. The method comprises the following steps: mixing a reactant and a structure-directing agent according to certain proportion, and adding a pH value control agent to adjust the pH value; sealing hydrothermal reaction equipment, heating the mixture to be between 50 and 280 DEG C, making the mixture stand for 0 to 72 hours, raising the temperature to be between 60 and 300 DEG C, and continuously reacting for 0.1 to 72 hours; and cooling gel, taking out the gel, drying the gel and obtaining the aerogel. Compared with the prior art, the method has low reaction temperature and pressure, small equipment investment and simple and controllable technology, reduces potential safety hazards, greatly improves the preparation speed of the aerogel, saves the production cost, and is favorable to realize commercial mass production.

The invention relates to a bamboo powder filling biodegradable compound material and a preparation method thereof. The bamboo powder filling biodegradable compound material comprises the following raw materials in part by mass: 30 to 80 parts of biodegradable resin, 20 to 70 parts of bamboo powder, 1 to 19 parts of plasticizer, 0.6 to 6 parts of interface modifier and 4 to 12 parts of aids. The preparation method comprises the following steps of: uniformly mixing the biodegradable resin, bamboo powder, plasticizer, interface modifier and auxiliary agent by using a mixer according to formula proportion; performing melt blending and granulation of the obtained mixture by using a screw extruder to obtain particles; and processing the particles by using an injection molding machine, a sheet extrusion forming machine, a blow molding machine or a film blowing machine, and molding in molds of different shapes to obtain the bamboo powder filling biodegradable compound materials of different shapes. The method has the advantages of high production efficiency and low cost; and the powder filling biodegradable compound material prepared by the method has the advantages of high environmentally-friendly property and economy and excellent usability.

The invention relates to a method for preparing spongy graphene oxide by using a freeze-drying method, which is in a loose and porous type and is in a spongy type in a macro-morphology. The method comprises the steps of: after an improved Hummers process is utilized to prepare graphite oxide, preparing graphite oxide into a solution with water or ethanol, and then carrying out quick-freezing and vacuumizing on the solution, and sublimating a solvent to obtain the graphene oxide. The graphene oxide is different from general blocky, film type or powdery graphene oxide. The obtained loose and porous graphene oxide provided by the invention is in a spongy type, is an excellent precursor for preparing graphene, and has a great application foreground in the field of an anti-flaming composite material, an adsorbent and the like. The method for preparing spongy graphene oxide by using a freeze-drying method is free from environmental pollution, convenient in technology and small damage to graphite oxide sheets, and completely strips graphite oxide; and the porosity of the graphene oxide is 20-90% and the pore distribution is uniform.

A method is disclosed to produce a heat pipe with a sintered powder wick formed inside the heat pipe. The method employs tape-casting technology to firstly produce thin sheets of powder and then these sheets are sintered to form the wick. In the tape casting procedure, a slurry of the powders necessary to construct said wick is cast onto a moving surface to form a slurry layer and then the slurry layer is dried to form a green tape. The green tape is rolled onto a mandrel and then is inserted into a hollow casing and sintered to cause the powders in the green tape to diffusion-bond together. Thus, the sintered powder wick is constructed.

The invention discloses low-cost green cellulose aerogel and a preparation method for hybrid aerogel thereof. The preparation method for the hybrid aerogel of the cellulose aerogel comprises the following steps that cellulose is dissolved into a zinc chloride aqueous solution, centrifugal deaeration is performed, and a uniform and transparent cellulose solution is obtained; the cellulose solution is formed, then the formed cellulose solution is placed into a coagulating bath to be regenerated, in addition, the regenerated cellulose solution is fully washed by use of a solvent, and cellulose solvent gel is obtained; the solvent in the cellulose solvent gel is removed by use of supercritical carbon dioxide drying or freeze drying, and the cellulose aerogel is obtained. Functional filler can be added into the cellulose solution to obtain the hybrid aerogel. By the adoption of different solution forming methods, the cellulose aerogel and the hybrid aerogel thereof in the shapes of sheets, fibers, particles and the like can be prepared. The preparation method is low in cost and is environmentally friendly, and the prepared aerogel is provided with a uniform nano-grade net porous structure.

This invention describes the detection of atherosclerotic plaque or cancer cells by a light probe inside a blood vessel or internal to an elongate organ. In one embodiment, vessel wall is imaged by employing a scanning mechanism using one emitting and one receiving fiber, whereby light is directed at a spinning mirror, approximately normal to the vessel or elongate organ surface. The light is reflected circumferentially around the vessel or elongate organ surface as the mirror rotates and received by a low-numerical aperture (NA) fiber, which transmits it to a light detector, thereby generating a set of light amplitudes circumferentially around the vessel/elongate organ surface. Multiple rings are acquired by translating the probe within the vessel/elongate organ. In another embodiment, adding a piezoelectric transducer in proximity to the distal ends of the fibers permits simultaneous ultrasound and light images to be created.

The invention relates to a method for manufacturing a foamed aluminum sandwich plate, which belongs to the field of porous foam metal and laminar composite materials. The method comprises the following steps of: uniformly mixing aluminum-silicon alloy powder prepared by an atomization method, and foaming agent titanium hydride powder and metal magnesium powder in a certain ratio; filling the powder into a thin-wall steel (or aluminum alloy) tube with one sealed end; sealing the other end of the tube after powder filling and preparing a rolled blank; rolling and compounding at a slow speed on a cold rolling mill; trimming an obtained composite plate and cutting a foamed preformed blank according to the size of a foaming mold; foaming the preformed blank in a steel mold in a limited way; adjusting foaming temperature and foaming time as required; and foaming at a high temperature for a short period of time to obtain a high-quality foamed aluminum sandwich plate with a uniform foam structure in a core layer, good interface bonding, high thickness accuracy and excellent plate profile. The method has the outstanding characteristics of low equipment requirement, high plate profile accuracy of a product, high three-point bending strength and the like and is advantaged technology suitable for mass industrial production of foamed aluminum sandwich structural materials.

The invention discloses a method for coating micro/nano-metal powder by chemical vapor deposition, including: decomposing difluorocarbene precursor gas via a cracking pipe to generate difluorocarbene free radicals; contacting the generated difluorocarbene free radicals with micro/nano-metal powder, and due to polymerization between difluorocarbene free radicals, a compact polytetrafluoroethylene coating film is generated on the surface of micro/nano-metal powder. In allusion to disadvantages and defects of the application of micro/nano-metal powder in energy-containing materials, polytetrafluoroethylene is polymerized on the surface of metal powder by chemical vapor deposition in order to coat micro/nano-metal powder. In the invention, the ignition temperature of metal powder is effectively decreased, the ignition delay time is shortened, and the combustion speed of metal powder is improved; the surface of metal powder coated with polytetrafluoroethylene is highly hydrophobic, so that reactive metal powder can be effectively prevented from absorption of moisture and oxidation.

The invention relates to an ultrathin nanosheet array electro-catalytic material with a nano-porous structure and oxygen vacancies. The material is a cobaltosic oxide primary nanosheet array which grows vertically on a conductive substrate and is doped with a metal; an ultrathin nanosheet with oxygen vacancies and nanopores is obtained on each primary nanosheet; the conductive substrate is a titanium sheet or a foamed nickel sheet, and the doped metal is zinc, nickel or manganese; and the thickness of each cobaltosic oxide ultrathin nanosheet doped with the metal is 1.22 nm, nanosheets are in a three-dimensional porous structure, and the nano-pore diameter is 3-6 nm. The ultrathin nanosheet array electro-catalytic material with the nano-porous structure and oxygen vacancies has the following advantages: the material can effectively reduce the overpotential and the spike potential of an oxygen evolution reaction, increase the conversion rate of a single cobalt atom and work continuously and stably in an alkali environment; the steps of a preparation method of the material are simple, the operation is convenient, the cost is low, and the material is environmental-friendly; and new ideas and strategies are provided for the function-oriented design and the performance optimization of an oxygen evolution catalyst of a water electrolysis system.

The invention relates to a nickel disulfide carbon nano composite material and a preparation method and an application thereof, wherein the composite material is formed by coating a nickel disulfide nanosheet with a carbon layer. The preparation method comprises the following steps of preparing a nickel hydroxide nanosheet precursor by a hydrothermal method, performing magnetic stirring and dispersing in deionized water to obtain a uniform dispersion liquid of the nickel hydroxide nanosheet precursor, adding a buffering agent tris(hydroxymethyl) aminomethane hydrochloride, and adjusting the pHvalue to be 8.5 by adopting an alkali solution with the pH value of 13, adding dopamine hydrochloride, and magnetically stirring at room temperature for in-situ polymerization, and carrying out washing and centrifugally drying to obtain a nickel hydroxide nanosheet precursor/polydopamine composite material, and carrying out heat treatment and vulcanization with sublimed sulfur powder in a tubularfurnace in nitrogen atmosphere at a certain temperature to obtain the composite material. The preparation process is simple, easy to operate, green and non-toxic and friendly in material preparationprocess; and the prepared nickel disulfide carbon nano composite material is stable in structure, uniform in morphology and high in dispersion. The obtained nickel disulfide carbon nano composite material can be an ideal electrode material of a high-performance lithium ion battery, a supercapacitor and other new energy devices.

The invention discloses a 2:17 type samarium-cobalt sintered magnet material and a preparation method thereof. The 2:17 type samarium-cobalt sintered magnet material comprises the following raw materials in percentage by mass: 10 to 25 percent of samarium, 45 to 55 percent of cobalt, 10 to 20 percent of iron, 3 to 9 percent of copper, 1 to 3 percent of zirconium and 5 to 15 percent of at least one heavy rear earth element. Due to the selection and the proportion of the raw materials and the innovation of the sintering process, a microstructure of the magnet material is optimized, and the aims of reducing the temperature coefficient of a magnet and simultaneously maintaining higher magnetic energy product of the magnet are fulfilled, wherein the magnetic energy product of the prepared magnet is 14 to 25 MGsOe, the residual magnetism temperature coefficient is about -0.005 to -0.03 percent per DEG C, and a lower magnetic flux temperature coefficient is maintained in an environment at the temperature of between -35 and 300 DEG C.

The invention discloses wear corrosion resistant castable prepared from a bauxite-based homogenous material and a preparation method thereof, which belong to the technical field of castable refractory. In the invention, by using the characteristics of the bauxite-based homogenous material, such as homogeneous chemical components and structure, stable performance, mulite main crystal phase, small linear change, high high-temperature strength and certain flexibility due to mutual insertion of micro crystals and the like, the shortcomings of low middle-temperature strength and poor wear resistance and alkali corrosion resistance of the conventional high-aluminum bauxite castable are overcome, and the problems of low middle-temperature strength, poor wear resistance and poor alkali, chloride and sulphur corrosion resistance of the conventional high-aluminum and corundum castable are effectively solved. The wear and corrosion resistant castable with high middle-temperature performance is prepared. The wear corrosion resistant castable and the preparation method thereof have the advantages of small fluctuation of water adding amount in construction, stable usability, reduction rate of partial corrosion, prolonged service life and wide application to a kiln hood, a grate cooler, a tertiary air duct and a decomposing furnace of a dry process cement kiln and relative parts of other ceramic and petrified thermo-technical kilns and the like.

The invention provides an opaque quartz crucible used in multicrystal silicon crystallization and a method for manufacturing the same. The crucible is of a regular square structure, and the compositions in mass ratio of the crucible are more than 99.7 Wt percent of silicon dioxide, less than 600ppm of aluminum oxide and less than 30ppm of ferric oxide. The method comprises the following steps: firstly, a raw material, i.e. high purity quartz is put into granulation equipment for wet method granulation, the grain size is controlled between 70 and 100mu m; then, slurry is fully stirred and then is fed into a gypsum mould under a pressure of between 2 and 3bar after being deposited for 24 to 48 hours; moreover, early grouting is assisted by slight vibration; the slurry is further settled for 5 to 8 hours, and is demoulded after fully dewatered; the slurry is dried inside a drier; and finally, a blank is put in a kiln for sintering so as to obtain the opaque quartz crucible. The proposal adopts grouting forming by a high-purity quartz material, and the sintered crucible has uniform inner structure; moreover, the crucible has excellent thermal shock stability and cracking resistance, and can meet the technological requirements for manufacturing multicrystal silicon cast ingots.

The invention relates to a method for slitting, striking and redrying tobacco, which is technically characterized by comprising the following step of: cutting tobacco lead bases with minimum tensile strength, poorest physical processing resistance and poorer perception smoke panel test quality and appearance quality in the tobacco for singly cutting, striking and redrying. The method has the mainadvantages that remained non leaf base tobacco leaves are crushed to be smaller when leaves and stems are separated singly after the tobacco leaf bases are cut for being singly processed, the leaf structures are more uniform after the leaves are separated from the stems, the green and impurity content in the tobacco is reduced, thus the large-medium leaf ratio after the striking is improved, the crushing generated when the leaves are separated from the stems is reduced, the leaf yield is improved, and the purity of the tobacco is increased. After the tobacco is processed by using a slitting, striking and redrying method of the invention, the leaf base smoking quality is better, the fragrance quantity is improved, the smoke explosive force is increased, the smoking comfort is enhanced, andthe impurity gases are reduced, thus the use value of the tobacco can be improved.

The invention discloses a preparation method of a spinel-type magnetic MFe2O4/graphene composite material. The preparation method utilizes a water-soluble metal M<2+> salt and a Fe<3+> salt as precursors and graphite oxide as a matrix and comprises the following steps of carrying out ultrasonic dispersion of graphite oxide in ethanol or water as a solvent to obtain a graphene oxide dispersion, adding a M<2+> salt and Fe<3+> salt-containing aqueous solution having a M<2+>/Fe<3+> mole ratio of 1: 2 into the graphene oxide dispersion, fully stirring to obtain a mixed solution, adjusting a pH value of the mixed solution to a value more than 10 by an alkali liquor, adding a reducing agent into the mixed solution, stirring at a temperature of 80 to 150 DEG C for a reaction lasting for 4 to 10 hours, after the reaction is finished, carrying out separation, washing, drying and grinding, and carrying out calcination of the grinded powder at a temperature of 300 DEG C in a nitrogen or argon atmosphere for 2 to 10 hours. Magnetic MFe2O4 nano particles of the spinel-type magnetic MFe2O4/graphene composite material have high loading capacity, stable structures, good uniformity, good dispersibility and strong adhesion with graphene. The spinel-type magnetic MFe2O4/graphene composite material can be widely used in the fields of magnetic targeting materials and other related function materials.

A three-dimensionally structured fibrous fabric having elevations and depressions occurring regularly in alternation in relation to the surface plane, includes at least one nonwoven fabric layer and a shrunk fabric bonded thereto. In this context, the nonwoven fabric layer and the shrunk fabric were bonded by heat sealing performed at least perpendicular to the direction of the greatest shrinkage of the shrunk fabric in the form of lines. The fabric may be used as filter materials, in hygiene articles or as the mechanically sticking part of Velcro fasteners.

The invention relates to a novel preparation technology of polyoxymethylene fiber, in particular to the novel preparation technology of the polyoxymethylene fiber via multi-stage slow cooling and three-stage drawing with different media, which comprises the following steps: vacuum-drying polyoxymethylene granular materials, heating and melting via a screw extruder, melting and extruding by a spinneret, leading small melt flow to pass through the multi-stage slow cooling, carrying out high-speed traction, passing through a moistening and oiling cluster, winding, then obtaining as-spun fiber, carrying out hot air drawing and two times of drawing with different types of solvent, then carrying out hot molding and finally preparing the polyoxymethylene fiber. The novel prepration technology can solve the problems of matching between the multiple sections of atmosphere and temperature and the spinning process control and the control of the drawing with multiple media and make up for the deficiencies that the single atmosphere and temperature and the single medium drawing of the prior art lead the structure to be difficult to stable and uniform.