217 results about "Tape casting" patented technology

The invention discloses a high-strength and high-toughness aluminum nitride ceramic and a preparation method thereof, and relates to the technical field of ceramics, a sol-gel method is adopted to coat the surface of aluminum nitride with a stable shell layer to form a core-shell structure, meanwhile, the low lattice mismatch rate of a core-shell interface is utilized to reduce thermal resistance, and toughness and thermal conductivity are both considered; according to the external magnetic field tape casting method, the magnetic dipole moment orientation principle is utilized, an external magnetic field is applied in the tape casting stage, the in-plane mechanical property is improved, and the fracture toughness is improved through the magnetism of aluminum nitride whiskers; a reinforcement is introduced to improve the mechanical property and corrosion resistance of the aluminum nitride ceramic material, multi-granularity powder is compounded, large-particle aluminum nitride powder is used as a sintering and heat-conducting framework material, and high activity provided by submicron particles is utilized to promote sintering, so that the sintering temperature of aluminum nitride can be remarkably reduced, and the performance is greatly improved; and the aluminum nitride substrate expands more application fields on a future packaging circuit.

The invention discloses a preparation method of a textured silicon nitride ceramic substrate, and belongs to the technical field of ceramic products. Beta-silicon nitride whiskers with the long diameter of 4-15 microns and the short diameter of 1-3 microns are added into silicon nitride ceramic slurry according to the design, and when the whiskers containing beta-silicon nitride pass through a scraper of a casting machine, the whiskers tend to be directionally arranged in the casting direction, so that a textured structure is generated in the silicon nitride ceramic substrate. The textured structure is beneficial to improving the three-point bending strength, the fracture toughness and the thermal conductivity in the horizontal direction of the ceramic substrate.

The invention discloses a high-interface-stability composite solid electrolyte membrane as well as a preparation method and application thereof. The composite solid electrolyte membrane comprises a gradient aperture three-dimensional porous skeleton formed by sintering inorganic solid electrolyte particles, a polymer electrolyte filled in a pore channel, and a plastic interface stable layer positioned between the electrolyte membrane and an electrode. The preparation method comprises the following steps: preparing a gradient aperture porous framework through a pore-forming agent template method and a tape casting technology, dipping and filling a polymer electrolyte precursor solution in a solution, accelerating in-situ polymerization by adopting electric induction, and performing hot-pressing treatment. The composite solid-state electrolyte membrane has high ionic conductivity, excellent interface compatibility and high mechanical strength, can effectively inhibit the growth of lithium dendrites, can be applied to solid-state batteries such as lithium metal batteries, lithium sulfur batteries and lithium air batteries, and can remarkably prolong the cycle life and improve the safety performance of the batteries, and the preparation process is suitable for large-scale production.

The invention provides a preparation method of a high-thermal-conductivity 99 aluminum oxide ceramic substrate, and belongs to the field of electronic ceramic materials. The method comprises the following steps: homogenizing and grinding a high-purity aluminum-containing compound and a modifier to obtain pretreated powder; mixing the pretreated powder with a carrier gas, and carrying out melt spheroidization to obtain a submicron spherical alumina precursor raw material; homogenizing and defoaming the submicron spherical aluminum oxide precursor raw material, an inorganic sintering aid, a dispersing agent, a binder, a plasticizer and a foam inhibitor in a solvent to obtain ceramic slurry; carrying out tape casting on the ceramic slurry to obtain an aluminum oxide green body; the alumina green body is subjected to rubber discharging, pre-sintering and sintering, and the 99 alumina ceramic substrate is obtained. The submicron spherical alumina powder is prepared through a melt spheroidizing process, the surface of the powder is smooth, particle size distribution is concentrated, grain boundary resistance between the powder is remarkably reduced, sintering densification is promoted, and therefore the technical problems that existing tape casting slurry is poor in stability and high in sintering temperature, and consequently microdefects are caused are solved.

The invention relates to the technical field of ceramic materials, in particular to a preparation method of a zirconium oxide toughened aluminum oxide ceramic substrate, which comprises the following steps: 1, pretreating a powder material; step 2, preparing slurry; step 3, tape casting; step 4, stamping and forming; and 5, sintering. Before the slurry is prepared, the aluminum oxide powder and the zirconium oxide powder are uniformly mixed and then subjected to plasma treatment, so that the surface activity of the mixed powder of the aluminum oxide and the zirconium oxide is improved, the grain structure of the mixed powder of the aluminum oxide and the zirconium oxide is changed, and the toughening effect of the zirconium oxide on the aluminum oxide ceramic substrate is improved.

The invention relates to the technical field of ceramic manufacturing processes, and particularly discloses a preparation method of a 96 aluminum oxide ceramic substrate, which comprises the following steps: slurry preparation: carrying out ball milling treatment on high-purity aluminum oxide powder, a sintering aid, a binder, a plasticizer, an organic solvent and a dispersing agent, and fully mixing to obtain tape casting slurry; forming a green body, coating a carrier film with the tape casting slurry through a tape casting machine with a wet film which is uniform in thickness and flat in surface, and drying the carrier film through a drying box in a partitioned manner to obtain a cured green body; and sintering densification treatment: carrying out glue removal treatment on the green body, and carrying out stepped heating sintering to obtain the 96 aluminum oxide ceramic substrate. According to the 96 aluminum oxide ceramic substrate prepared by the scheme, a large number of uniform crystal cores can be formed, small crystal grains can be dissolved, large crystal grains grow at a constant speed, and the uniformity of the crystal grain size is ensured, so that scattering of phonons on a crystal boundary can be reduced, and a structural foundation is laid for improvement of heat conductivity.

The invention relates to the field of aluminum nitride ceramic substrates, provides a preparation method of a high-thermal conductivity aluminum nitride substrate, and solves the defects of low thermal conductivity and insufficient mechanical strength of an aluminum nitride substrate obtained by adopting a preparation method in the prior art. Comprising the following preparation processes: (1) preparing raw materials and auxiliary materials; (2) mixing the raw materials and the auxiliary materials; (3) tape casting; (4) aging; (5) pre-flattening treatment; (6) sintering; and (7) post-treatment.

The invention relates to the technical field of polymer functional material processing, and particularly discloses a polyethylene waterproof breathable film using PTFE micro powder as an opening agent and a preparation method of the polyethylene waterproof breathable film. The waterproof breathable film is prepared from the following components in parts by weight: 50-70 parts of linear low-density polyethylene, 10-40 parts of PTFE (Polytetrafluoroethylene) micro powder, 3-8 parts of a modified compatilizer and an auxiliary agent. The preparation method comprises the following steps: S1, activating PTFE micro-powder by a silane coupling agent and coating the PTFE micro-powder with polyethylene wax to obtain modified micro-powder; s2, uniformly mixing all the components; s3, carrying out melt extrusion at 180-210 DEG C through a double-screw extruder, and carrying out tape casting to form a cast sheet; s4, the casting piece is heated to 90-115 DEG C for two-way stretching, and micropores are formed through interface stripping between the PTFE particles and the base body; and S5, carrying out heat setting at 120-130 DEG C, cooling, and rolling to form the film. Through the synergistic effect of the self-made compatilizer and the pretreatment process, the interface anchoring force is enhanced, the problems of powder falling and water leakage of highly-filled PTFE are solved, and meanwhile, high moisture permeability, high hydrostatic pressure resistance and high mechanical property are taken into account.

The invention belongs to the technical field of photovoltaic packaging adhesive films, and particularly relates to an assistant precipitation resistant anti-slip POE packaging adhesive film and a preparation method thereof, and the preparation method comprises the following steps: S1, mixing raw materials, and uniformly stirring to obtain a micro-foaming layer raw material and a skeleton layer raw material; s2, performing melt extrusion, namely performing melt extrusion on the raw materials of the framework layer through a single-screw extruder, and controlling the extrusion temperature and the screw rotating speed to obtain the framework layer; s3, supercritical fluid micro-foaming extrusion is conducted, specifically, raw materials of a micro-foaming layer are subjected to melt extrusion through a co-rotating twin-screw extruder, the extrusion temperature and the screw rotating speed are controlled, supercritical fluid carbon dioxide is introduced in the extrusion process to serve as a foaming agent, then heating foaming is conducted, the adding amount of the foaming agent is 0.5%-2% of the mass of matrix resin, the foaming temperature is 160-200 DEG C, the foaming pressure is 10-20 MPa, and the foaming layer is obtained; a micro-foaming layer is obtained; and S4, tape casting: carrying out three-layer co-extrusion on the micro-foaming layer, the skeleton layer and the micro-foaming layer to form an ABA structural adhesive film, thereby obtaining the POE packaging adhesive film.

The invention relates to the technical field of high-temperature sintering, and particularly discloses a gradient composite kiln furniture based on spinel interface strengthening and a preparation method thereof. Wherein the kiln furniture sequentially comprises a mullite matrix layer, a silicon carbide enhancement layer and a zirconium oxide high-temperature-resistant layer from outside to inside, and the layers are chemically bonded through an in-situ generated MgAlO spinel interface layer. The preparation method comprises the following steps: carrying out layered tape casting on gradient slurry, carrying out isostatic pressing lamination molding, generating an MgSi transition phase at 1380-1420 DEG C through a stepped sintering process, and heating to 1600-1650 DEG C at a specific heating rate to form a continuous spinel interface. According to the kiln furniture, gradient component design cooperates with spinel interface strengthening, the problem of interface stripping caused by thermal expansion mutation of a traditional double-layer structure is solved, and the kiln furniture has excellent thermal shock stability and high-temperature strength retention rate. According to the preparation method, precise construction of the spinel interface is realized through staged reaction control.

The invention discloses an LTCC (Low Temperature Co-Fired Ceramic) green tape as well as a preparation method and application thereof, and the preparation method comprises the following steps: mixing LTCC formula powder and additive phase powder to obtain mixed powder; mixing the mixed powder, a dispersing agent and a solvent, and performing first ball milling treatment to obtain a first ball milling product; adding an adhesive and a plasticizer into the first ball-milling product, and carrying out second ball-milling treatment to obtain a second ball-milling product; filtering the second ball-milled product to obtain ceramic slurry for tape casting; drying the casting ceramic slurry to obtain an LTCC (Low Temperature Co-Fired Ceramic) green tape; wherein the weight ratio of the LTCC formula powder to the additive phase powder is (50-95): (5-50); the LTCC formula powder comprises ceramic powder and glass powder; the additive phase powder is at least one of hexagonal boron nitride, fluorophlogopite sheets, bismuthate-based tungsten bronze and phosphate glass. According to the LTCC green tape prepared by the preparation method disclosed by the invention, the technical problem that the machinability and the thermal conductivity of an LTCC green substrate prepared by an existing LTCC green tape are relatively poor can be solved.

The invention discloses a preparation method of a composite current collector base film based on flame-retardant and aging-resistant modified PP and a composite current collector, the method comprises the following steps: 1) preparation of a modified PP master batch: mixing 100 parts by weight of PP resin, 0.5-1.8 parts by weight of a lubricant and 10-25 parts by weight of a flame-retardant and aging-resistant composite filler, and stirring at 100-135 DEG C for 0.5-2 h to obtain the modified PP master batch; (2) carrying out melt extrusion, tape casting and sheet casting to obtain an intermediate sheet; 3) biaxial stretching; and 4) carrying out heat setting, rolling and slitting to obtain the composite current collector base film. The invention provides the PP base film with excellent flame-retardant and aging-resistant performance and good mechanical strength; furthermore, based on the PP base film, the composite current collector is obtained after copper layers are formed on the two surfaces of the PP base film by adopting a conventional water electroplating process, and the copper layers and the PP base film in the composite current collector have high bonding strength, so that the service life of the composite current collector can be effectively prolonged.

The invention discloses a preparation method of a high-strength aluminum oxide ceramic substrate, which comprises the following steps: firstly, modifying aluminum oxide powder by a liquid phase method, and coating a layer of nano magnesium oxide on the surface of the aluminum oxide powder; then carrying out ball milling treatment on the modified powder, rare earth metal oxide, metal oxide, an organic solvent, a binder, a plasticizer and a dispersing agent together, then carrying out defoaming, tape casting, drying and laminated hot pressing to obtain a ceramic green body, and finally carrying out sintering molding in an air atmosphere to obtain the ceramic. The nano magnesium oxide active coating layer constructed in situ and the added exogenous sintering aid act together, so that uniform growth of isometric crystals is promoted, development of a small amount of dominant oriented grains is directionally induced, a composite enhanced microstructure is formed, atomic scale super-uniform distribution and optimal interface combination of the nano magnesium oxide and the exogenous sintering aid are realized, and the nano magnesium oxide / exogenous sintering aid composite material is prepared. The bending strength of the obtained alumina ceramic can reach up to 881 MPa.

The invention discloses a manufacturing method of a grinding wheel for a high-uniformity and easy-to-sharpen grinding single crystal diamond cutter, and belongs to the field of superhard materials and products in machining, the manufacturing method mainly comprises the steps of wet mixing, tape casting, laser cutting, lamination, matrix surface treatment, integrated sintering, size processing, sharpening and the like, and finally the grinding wheel with the total thickness of an abrasive layer being 7-15 mm is formed. The grinding wheel layer is formed by intersecting and laminating a piece a and a piece b, the height of diamonds at the junction of the piece a and the piece b tends to be consistent, the diamond exposure height and smoothness are better compared with direct feeding sintering, meanwhile, the piece a can be designed to be of a porous structure through proper binder selection, and therefore the dressing efficiency is further improved, and the dressing effect is better. And higher processing quality and efficiency of the diamond cutter are indirectly improved.

The invention relates to the technical field of silicon nitride ceramic chips, in particular to a reactive sintering silicon nitride ceramic chip processing method which comprises the following steps: S1, adding spherical boron nitride powder and a dispersing agent into a solvent, and mixing to obtain a spherical boron nitride solution; s2, mixing the spherical boron nitride solution and the yttrium solution to obtain a mixed solution; s3, a sintering aid, silicon powder and the mixed solution are put into a ball mill for pulping, and slurry is obtained; s4, the slurry is subjected to tape casting through a tape casting machine, and a tape casting green body is prepared; s5, the tape-casting green body is placed on a powder coating machine for powder coating, and the tape-casting green body coated with the powder is obtained; s6, the green bodies coated with the powder are laminated and then put into a hot air glue discharging furnace to be subjected to glue discharging treatment, and laminated green bodies are obtained; and S7, sintering the laminated green body to obtain the silicon nitride ceramic chip. The yttrium-containing substance is locally coated with the spherical boron nitride powder, the invention provides a method for processing the reactive sintering silicon nitride ceramic chip, and the prepared silicon nitride ceramic chip is compact in structure and excellent in bending strength.

The invention provides an LTCC raw material belt with a high thermal expansion coefficient, an LTCC substrate and a preparation method of the LTCC substrate, the LTCC raw material belt with a smooth surface and a uniform thickness is obtained through tape casting by adjusting the proportion of silicon dioxide ceramic powder, MgTiO3 ceramic, SrTiO3 ceramic, Li2MgSiO4 ceramic, BCBS, ZABS and LASP microcrystalline glass powder, the LTCC raw material belt is sintered in a nitrogen furnace at 880-940 DEG C for 1-3 h, and the LTCC raw material belt can be co-fired with low-cost copper electrode slurry to be flat and tightly attached to the low-cost copper electrode slurry. The LTCC substrate with the thermal expansion coefficient larger than 11 ppm / DEG C is prepared, under the test frequency of 5 GHz, the dielectric constant of the LTCC substrate ranges from 5.1 to 6.1, the dielectric loss ranges from 0.0025 to 0.004, the bending strength ranges from 170 MPa to 230 MPa, the thermal expansion coefficient at the temperature ranging from 30 DEG C to 400 DEG C ranges from 11.0 ppm / DEG C to 13.0 ppm / DEG C, and acid resistance is good.

The invention relates to the technical field of ceramic materials, in particular to a preparation method of a low-temperature sintered high-thermal-conductivity 99 ceramic aluminum oxide ceramic substrate, which comprises the following steps of: 1, preparing slurry; step 2, tape casting; step 3, stamping and forming; 4, performing warm isostatic pressing treatment; step 5, performing main firing to obtain porcelain; and 6, inspecting a finished product. By regulating the particle size of the alumina powder, adopting the specific sintering aid of the solid solution and the liquid phase forming agent, introducing trace La2O3 into the system and combining low-temperature co-firing, the problem that the 99 ceramic alumina ceramic substrate is easy to crack in the processing process is improved while the sintering temperature of the 99 ceramic alumina ceramic substrate is remarkably reduced.

The invention discloses a high-reliability packaging quality assessment method and system based on multi-source process data, and relates to the technical field of quality assessment, and the method achieves the online sensing of the orientation consistency of casting ceramic particles through the nondestructive scanning of an unsintered green tape by adopting a terahertz spectrum. Material waste and procedure interruption caused by destructive detection are avoided; secondly, the cutting edge morphology is synchronously collected in the scribing process, geometric feature quantification is carried out, the recognition of the edge breakage state is improved from subjective qualitative judgment to objective quantitative characterization, and the detection consistency and precision are remarkably improved; the frequency spectrum coding data reflecting the internal quality and the shape coding data reflecting the external defects are associated point by point, and a two-dimensional mapping relation of the internal process parameters and the external processing results is constructed, so that whether the cutting edge breakage is derived from potential abnormity in a tape casting stage or not can be accurately traced; and a data closed loop is provided for backtracking optimization of process parameters.

The invention discloses a preparation method of a zirconium oxide toughened aluminum oxide ceramic substrate, which comprises the following steps: respectively carrying out surface modification on aluminum oxide powder and zirconium oxide powder by adopting a coupling agent, a catalyst and a cross-linking agent, then mixing the two modified powder with a rare earth sintering aid, a dispersing agent, a binder and a plasticizer, and carrying out ball milling treatment, thereby obtaining the zirconium oxide toughened aluminum oxide ceramic substrate. Carrying out tape casting and sintering processes to obtain a target ceramic substrate; the preparation method is simple, the process is easy to control, the bending strength of the prepared zirconium oxide toughened aluminum oxide ceramic substrate can reach 847 MPa at most, and the fracture toughness can reach 7.6 MPa.m < 1 / 2 > at most.

The invention relates to a high-strength light waist protection cushion and a preparation method thereof, and relates to the technical field of waist protection cushions, the high-strength light waist protection cushion comprises an upper outer surface coating material, a lower outer surface coating material and an inner container connected between the upper outer surface coating material and the lower outer surface coating material, the upper outer surface coating material and the lower outer surface coating material are integrally formed, the upper outer surface coating material and the lower outer surface coating material form an accommodating space for filling the inner container; the high-density outer surface coating material is prepared from high-density raw materials in a tape casting or spraying forming mode, the process is simple and efficient, an exoskeleton structure formed by the outer surface coating material can guarantee the appearance integrity of a seat product, the hardness of the seat product is improved, and the service life of the seat product is prolonged. The inner container is formed by injecting the high-temperature low-density raw material into the outer surface coating material, the inner container can provide additional support for the upper outer surface coating layer, the structural stability of a seat product is improved, and a product structure which cannot be manufactured through a traditional technology can be manufactured through the mode.

The invention discloses a high-bending-resistance and low-dielectric-loss LTCC substrate preparation method and an LTCC substrate, and the method comprises the steps: mixing inorganic powder, an organic system and a solvent through ball milling, dissolving and stirring, and preparing a green ceramic chip through a tape casting technology; carrying out lamination, warm isostatic pressing, cutting, glue discharging and sintering on the green ceramic chip to obtain the LTCC substrate; the inorganic powder comprises sodium borosilicate glass, aluminum oxide and mullite whiskers. According to the invention, the sodium borosilicate glass is used as a glass phase, the mullite whisker and the alumina powder are used as ceramic phases, and the excellent mechanical properties and extremely low dielectric loss of the mullite whisker are utilized to modify the sodium borosilicate glass-alumina composite material. The problems that an existing sodium borosilicate glass-aluminum oxide LTCC composite material is low in bending strength and high in dielectric loss are solved.

A porous titanium sheet configured to function as an anode side gas diffusion layer of a proton exchange membrane (PEM) electrolyzer is formed by a powder technique, such as tape casting or powder metallurgy.

This invention relates to the field of ceramic casting technology and discloses a ceramic casting slurry and its preparation method. The ceramic casting slurry contains a main agent and auxiliary agents. Based on the total mass of the ceramic casting slurry, the main agent includes 49wt%-61wt% of calcined ceramic powder, 9wt%-20wt% of alcohol compounds, 15wt%-26wt% of non-alcoholic organic solvents, and 0.3wt%-0.8wt% of dispersant. The non-alcoholic organic solvents consist of organic solvent I and organic solvent II in a mass ratio of (0.6-3):1. Organic solvent I is selected from C4-C7 organic solvents, and organic solvent II is selected from C6-C8 organic solvents. The ceramic casting slurry provided by this invention has good stability, high solid content, and good powder dispersion, which is beneficial for improving the strength of the cast sheets and ceramics, and solves the problem that large-particle calcined ceramic powder cannot be directly used in casting production.

The application belongs to the field of solid oxide electrolysis cells, and discloses a method for preparing a solid oxide electrolysis cell by continuous roll-to-roll aqueous flow casting. The method comprises the following steps: mixing an oxygen electrode powder, a barrier layer powder, an electrolyte powder, a hydrogen electrode powder and a support body powder respectively with a dispersant, a binder, a plasticizer, a defoaming agent and a solvent, and defoaming to obtain an aqueous flow casting oxygen electrode slurry, an aqueous flow casting barrier layer slurry, an aqueous flow casting electrolyte slurry, an aqueous flow casting hydrogen electrode slurry and an aqueous flow casting support body slurry respectively; sequentially casting the above slurries to obtain a five-layer thin film green body; and performing integrated devolatilization-sintering heat treatment on the obtained five-layer thin film green body to obtain a solid oxide electrolysis cell. The method is easy to industrialize and implement in roll-to-roll continuous production, avoids the conventional hot pressing, lamination and multi-step sintering process flow, simplifies the preparation process and reduces energy consumption cost, and the prepared solid oxide electrolysis cell has good electrochemical performance.

The invention discloses a plasma corrosion resistant silicon nitride ceramic composition, tape casting slurry, a tape casting sheet, a green body sheet, a green body block, a ceramic, a preparation method, an electrostatic chuck and a semiconductor equipment part, and belongs to the technical field of semiconductor ceramic materials. The plasma corrosion-resistant silicon nitride ceramic composition provided by the invention comprises the following raw materials in parts by mole: 85-95 parts of silicon nitride and 5-15 parts of a sintering aid, wherein the sintering aid comprises a metal fluoride sintering aid. By introducing the fluorine-containing and / or nitrogen-containing compound sintering aid, a stable grain boundary phase is formed in a fluorine-containing plasma environment, synergistic protection is realized, different plasma environments are adapted, the corrosion resistance of the Si3N4 ceramic is improved, the defect of poor plasma corrosion resistance is overcome, sufficient liquid phase sintering is ensured by optimizing the ratio of the aid, and the service life of the Si3N4 ceramic is prolonged. Meanwhile, the grain boundary is prevented from being too thick; and the thermal expansion coefficient is stabilized at 2.6-3.1 * 10 <-6 > / DEG C, and is highly matched with a silicon wafer.

The application discloses an LLZO electrolyte and a casting forming method thereof, and belongs to the technical field of solid electrolyte material preparation. The application improves the storage period of the casting slurry to more than 15 days through surface modification; a composite binder-composite plasticizer synergic system is constructed, and a 20-micron ultra-thin defect-free green film can be stably prepared; in combination with Li3BO3-LiF composite sintering aids and a gradient sintering process, high densification of the LLZO film is realized at less than or equal to 1150 DEG C, the relative density of the prepared electrolyte film is greater than or equal to 97%, the room-temperature lithium ion conductivity is greater than or equal to 5*10 ‑4 S / cm, and the interface stability with lithium metal is excellent. The application has the advantages of simple and controllable process, good batch stability, adaptation to industrialized continuous production, and extremely high application value in the field of high-energy-density all-solid-state lithium batteries.

The invention relates to the field of high polymer materials, in particular to a high-definition perspective TPEE film, a preparation method and application. The invention discloses a high-definition perspective TPEE film which is prepared from the following components in percentage by weight: basic resin TPEE, a high-definition additive, a weather-resistant stabilizer, an antioxidant, an antistatic agent, an anti-scraping agent and a compatilizer, and further provides a preparation method of the TPEE film, the preparation method comprises the following steps: pre-mixing the components, performing melt blending through a twin-screw extruder, and finally forming the film through a tape casting method or a film blowing method, so as to obtain the high-definition perspective TPEE film. Meanwhile, the invention discloses application of the TPEE film in a high-definition display screen, a high-end packaging material or special optical equipment. The prepared TPEE film has high-definition perspective performance, the film thickness is 50-200 microns, the light transmittance is larger than or equal to 91%, the haze is smaller than or equal to 1.2%, the yellowing index delta b is smaller than or equal to 0.6, and the TPEE film has the effects of weather resistance, oxidation resistance, static electricity resistance, scraping resistance and the like.

The invention relates to high-solid-content AlN ceramic slurry for tape casting, a substrate and a preparation method of the substrate, and belongs to the field of ceramic substrates. The ceramic slurry is prepared from the following components in percentage by mass: 60 to 68 weight percent of high-purity AlN powder, 3 to 6 weight percent of dispersing agent, 3 to 5 weight percent of binding agent, 4 to 6 weight percent of plasticizer, 3 to 6 weight percent of sintering aid and 32 to 45 weight percent of solvent, the mass ratio of the plasticizer to the binder ranges from 3: 5 to 4: 5. By regulating and controlling the proportion of the dispersing agent in the AlN ceramic slurry and the solid content of the high-purity AlN powder, the slurry has excellent flowability, dispersity and stability while maintaining high solid content, and is suitable for a tape casting process. The AlN ceramic substrate prepared through sintering is high in density and excellent in heat conductivity, and engineering application can be achieved.

The invention relates to a bone-like layered calcium silicate / tricalcium phosphate heterogeneous biological ceramic as well as a preparation method and application thereof. The preparation method of the bone-imitating layered calcium silicate / tricalcium phosphate heterogeneous biological ceramic comprises the following steps: (1) mixing calcium silicate powder, an additive and a solvent to obtain calcium silicate tape casting slurry; mixing the tricalcium phosphate powder, an additive and a solvent to obtain tricalcium phosphate tape casting slurry; (2) respectively carrying out tape casting on the calcium silicate tape casting slurry and the tricalcium phosphate tape casting slurry to obtain a calcium silicate green tape and a tricalcium phosphate green tape; (3) alternately laminating the calcium silicate green tape and the tricalcium phosphate green tape, and performing pressurization treatment to obtain a composite ceramic body; and (4) degumming and sintering the composite ceramic green body to obtain the bone-like layered calcium silicate / tricalcium phosphate heterogeneous biological ceramic.

The invention relates to the field of electronic ceramic substrates, provides a preparation method of a black aluminum oxide substrate, and solves the defects of low heat conductivity and low mechanical strength of the existing black aluminum oxide substrate due to the defects of a preparation process. The preparation method comprises the following steps: (1) preparing raw materials; (2) preparing slurry; (3) tape casting; (4) discharging glue; (5) sintering; (6) annealing; and (7) surface treatment.