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78results about How to "Good dispersion properties" patented technology

Preparation method of nanometer in situ composite reaction type organic silicone modified cationic water-based polyurethane and product thereof

The invention relates to a preparation method of nanometer in situ composite reaction type organic silicone modified cationic water-based polyurethane and a product thereof. The preparation method comprises the following steps: preparing raw materials of basic monomers, modified monomers and adjuvants; carrying out dewatering pretreatment on mixed polyether glycol; and carrying out pre-polymerization, chain extension, blocking, quaternization and emulsification. So the nanometer in situ composite reaction type organic silicone modified cationic water-based polyurethane is obtained. The method is easy to implement and control, and the nanometer in situ composite reaction type organic silicone modified cationic water-based polyurethane prepared by the method is in a microemulsion state, has a small and uniform emulsion particle size and a good dispersion, and combines merits of organic silicone, polyurethane and inorganic nanometer materials. So the polyurethane prepared in the invention, which can be used to improve the color fastness and pilling resistance of various dyed textiles, allows the textiles to have certain stain resistance, and soft feel of the textiles not to be damaged. Thereby the polyurethane has the advantages of good application performance, wide range of use, safety and environmental protection, and convenient usage.
Owner:清河羊绒产业技术研究院

Detecting method and dielectric particle containing magnetic material employed in the detecting method

The invention relates to a detecting method and a dielectric particle containing magnetic material employed in the detecting method. In order to improve the practical utility of detection methods that utilize localization of bound substances by magnetic particles. A magnetic binding substance (Bm), which is a first binding substance (B1) that specifically binds with a target substance (A), having magnet enveloping dielectric particles (B), which have magnetic particles (M) enveloped therein and surfaces modified with functional groups that exhibit polarity within a liquid sample, attached thereto, and a labeling binding substance (B0), which is a second binding substance (B2) that specifically binds with the target substance (A) having photoresponsive labels (O) attached thereto, are mixed with the liquid sample such that binding reactions occur. A magnetic field is generated within a sample cell (10), to draw the magnetic binding substance (Bm) to a local region. Excitation light is irradiated only onto a predetermined region including the local region while the magnetic binding substance (Bm) is drawn to the local region, causing the photoresponsive labels (O) present therein to generate optical signals. The optical signals are detected.
Owner:FUJIFILM CORP

Graphene/trimanganese tetraoxide composite nano lubricating additive and synthesis method thereof

The invention discloses a graphene/trimanganese tetraoxide composite nano lubricating additive and a synthesis method thereof. Specifically, the synthesis method includes: mixing graphite with concentrated sulfuric acid and potassium permanganate in a high mass ratio, and carrying out oxidation reaction to obtain a mixed solution containing graphite oxide and/or graphene oxide; adding hydrogen peroxide into the mixed solution to reduce unreacted potassium permanganate, and adding water for dilution, and conducting ultrasonic treatment for a predetermined period of time to obtain a graphene oxide mixed solution; adjusting the pH of the graphene oxide mixed solution to alkaline, and carrying out reaction to obtain trimanganese tetraoxide and loading it to graphene oxide, and evaporating or filtering the mixture to obtain a solid product; subjecting the solid product to reduction treatment at high temperature to obtain a graphene/trimanganese tetraoxide composite product; and cleaning thegraphene/trimanganese tetraoxide composite product, and then performing ball milling treatment, thus obtaining the graphene/trimanganese tetraoxide composite nano lubricating additive. The method issimple and efficient, and the prepared additive has excellent dispersibility and lubricity.
Owner:TSINGHUA UNIV +1

Dispersion method of nanoscale inorganic particles suitable for composite electrodeposition

The invention discloses a dispersion method of nanoscale inorganic particles suitable for composite electrodeposition and belongs to the field of nanoscale inorganic particle dispersion treatment. According to the dispersion method, firstly, the nanoscale inorganic particles are activated, and active sites of hydroxide radicals are increased on the surfaces of the nanoscale inorganic particles; then, the nanoscale inorganic particles with the surfaces containing the hydroxide radicals are subjected to pre-adsorption treatment in treating liquid A, so that nanoscale inorganic particles with thesurfaces containing the hydroxide radicals and nonionic long-chain groups simultaneously are obtained; and next, the obtained particles are subjected to secondary adsorption treatment in treating liquid B, so that nanoscale inorganic particles with the surfaces containing the nonionic long-chain groups and anionic surfactant long chains are obtained. According to the nanoscale inorganic particleswith the surfaces containing the nonionic long-chain groups and the anionic surfactant long chains, surface Zeta potential can reach -10mv to -40mv, the dispersity is good, the nanoscale inorganic particles applied to a composite coating obtained in composite electrodeposition are uniformly deposited, and the content of the nanoscale inorganic particles reaches more than 10%.
Owner:BEIHANG UNIV

Graphene aqueous dispersion liquid, graphene concrete and preparation methods of graphene aqueous dispersion liquid and graphene concrete

The invention provides a graphene aqueous dispersion liquid, graphene concrete and preparation methods of the graphene aqueous dispersion liquid and the graphene concrete. The graphene aqueous dispersion liquid is prepared from the following raw materials, in percentages by mass: 1-5% of graphene or graphene oxide, 0.5%-2% of sodium dodecylbenzenesulphonate, 0.5%-2% of polyvinylpyrrolidone, and the rest is water. The preparation method of the graphene aqueous dispersion liquid includes the following steps: taking the graphene or the graphene oxide, the sodium dodecylbenzenesulfonate, the polyvinylpyrrolidone and the water according to percentages by mass, and performing full mixing and dispersion to obtain the graphene aqueous dispersion liquid. The invention aims to provide the graphene aqueous dispersion liquid and the preparation method thereof, and the preparation method of the graphene concrete by using the graphene aqueous dispersion liquid. The graphene aqueous dispersion liquidprovided by the invention can improve the problem of settlement of graphene in an aqueous medium, realize the uniform and stable dispersion of graphene in cement concrete, and can be used to preparethe graphene concrete with excellent quality and performance.
Owner:GUANGXI UNIVERSITY OF TECHNOLOGY +2

Microencapsulated animal drug and preparation method thereof

The invention discloses a microencapsulated animal drug which comprises the following synthesis raw materials in parts by weight: 9-29 parts of drug, 56-86 parts of wall material and 3-7 parts of an emulsifying agent. The invention further relates to a preparation method for the microencapsulated animal drug. The preparation method comprises the following steps: 1) preparing raw materials, 2), dissolving the wall material into water so as to obtain a water phase A; 3), dissolving the drug into a solvent, and adding the emulsifying agent so as to obtain an oil phase B; 4), under the condition of high shearing and high stirring, adding the oil phase B into the water phase A, stirring and emulsifying at a high speed and heating to remove the solvent so as to obtain microemulsion; 5), adding the obtained microemulsion into a spray granulation tower and mixing the microemulsion with corn starch or rice bran, and carrying out spray-drying, so as to obtain the microencapsulated animal drug granules or powder. The microencapsulated animal drug prepared through the preparation method disclosed by the invention is good in covering effect and good in flowing properties and the purposes of masking the smell, preventing dampness, and improving drug stability and drug bioavailability are realized.
Owner:GUANGDONG WENS DAHUANONG BIOTECH

Preparation method of hypocrellin-transferrin targeted drug delivery system and application of hypocrellin-transferrin targeted drug delivery system in photodynamic therapy

The invention discloses a preparation method of a hypocrellin-transferrin targeted drug delivery system and an application of the hypocrellin-transferrin targeted drug delivery system in photodynamic therapy. The method comprises the following steps: with holo-transferrin as a carrier, inactivating the holo-transferrin by urea and beta-mercaptoethanol, and making a three-dimensional structure loose to expose Fe-ion coordination sites; adding excessive hypocrellin, coordinating with Fe coordination sites, eliminating uncombined HA and urea through dialysis, and restoring the three-dimensional structure of holo-transferrin with beta-mercaptoethanol, thereby obtaining the hypocrellin-transferrin targeted drug delivery system. The method is simple in preparation and good in application prospect; the hypocrellin-transferrin targeted drug delivery system can be prepared into freeze-dried powder for storage, and the freeze-dried powder is prepared into a preparation suitable for intravenous injection after being dissolved. Due to the tumor targeting action of holo-transferrin in the system, the photosensitive anti-tumor activity of hypocrellin can be significantly strengthened by the targeted drug delivery system.
Owner:NANJING NORMAL UNIVERSITY

Photocuring 3D printing nanoparticle reinforced metal part and preparation method thereof

The invention relates to a photocuring 3D printing nanoparticle reinforced metal part and a preparation method thereof. The preparation method comprises the following steps that after amorphous powder and a coating agent are mixed, a coupling agent and metal powder are added into a mixture at the set temperature, and stirring is carried out for coating; post-treatment is carried out on a product obtained in the coating step, and an amorphous layer coated metal powder material is obtained; the amorphous layer coated metal powder material, photosensitive resin, an ultraviolet light initiator and a dispersing agent are prepared into a photocuring 3D printing slurry; a photocuring 3D printer is used for carrying out photocuring forming treatment on the photocuring 3D printing slurry, and a photocuring 3D printing biscuit is obtained; and degreasing and sintering treatment are carried out on the photocuring 3D printing biscuit, and the photocuring 3D printing nanoparticle reinforced metal part is obtained. According to the photocuring 3D printing nanoparticle reinforced metal part and the preparation method, the metal powder is prepared into the amorphous layer coated metal powder material with a powdery core-shell structure, so that the dispersity of the metal powder in the photosensitive resin slurry is improved, and the photocuring 3D printing nanoparticle reinforced metal part is prepared.
Owner:INST OF METAL RESEARCH - CHINESE ACAD OF SCI

Preparation method of organosilicon/hydroxyapatite composite adsorption fiber

InactiveCN110465270AGood dispersion propertiesSolve the problem of granular hard to useOther chemical processesWater contaminantsChemistryOrganosilicon
The invention discloses a preparation method of an organosilicon/hydroxyapatite composite adsorption fiber. The preparation method comprises the following steps: adding polyvinylpyrrolidone to anhydrous ethanol, and performing ultrasonic uniform stirring until the polyvinylpyrrolidone is completely dissolved in order to obtain a dispersed alcohol solution; carrying out wet ball-milling on the hydroxyapatite to form a fine powder, slowly adding the fine powder to the dispersed alcohol solution, and performing a low-temperature ultrasonic reaction for 2-3 h to obtain a first mixed solution; adding dichlorodimethylsilane to toluene, performing stirring until uniformity, then dropwise adding distilled water, and performing sealing stirring for 1-3 h to obtain a second mixed solution; slowly adding the first mixed solution to the second mixed medium, carrying out low-temperature and high-frequency ultrasonic dispersion for 30-60 min, and performing microwave oscillation for 1-2 h to obtaina pre-spinning solution; carrying out high-temperature electrostatic spinning on the pre-spinning solution to obtain single-fiber spun filament, twisting several strands of the single-fiber spin filaments to form twisted spun filaments, and bundling the twisted spun filaments to form a fiber web; and adding the fiber web an ethanol-water solution, carrying out a microwave oscillation reaction for30-60 min, and taking out and drying the fiber web to obtain the organosilicon/hydroxyapatite composite fiber material.
Owner:SHAOXING UNIVERSITY
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