1269 results about "Polyacrylic acid" patented technology

The invention provides a solid electrolyte slurry, an electrode slurry, a solid electrolyte sheet, an electrode sheet, a solid battery monomer, a battery device and a power utilization device.The solid electrolyte slurry comprises a sulfide solid electrolyte material, a solvent and a binder dissolved in the solvent, and the solvent is a non-polar solvent, a weak-polar solvent or a mixed solvent of the non-polar solvent and the weak-polar solvent; the binding agent comprises a polyacrylate binding agent and a non-polar polyolefin binding agent. The slurry disclosed by the invention has high dispersity, high suspension property and good cohesiveness, and can enable the solid-state battery monomer to have high initial coulombic efficiency when being used in the solid-state battery monomer.

The invention discloses a method for synthesizing electronic-grade ethyl acetate through catalytic esterification of acidic ion exchange resin, and belongs to the technical field of ethyl acetate preparation. The method comprises the following steps: mixing crosslinked polystyrene white balls and a swelling agent, and dropwise adding concentrated sulfuric acid for reaction to obtain S-PS resin; mixing an EDTA disodium salt saturated solution and a polyacrylic acid solution, adding a cross-linking agent and an emulsifier, and carrying out a cross-linking curing reaction to obtain EDTA microcapsules; the preparation method comprises the following steps: dispersing S-PS resin in a solvent, adding EDTA microcapsules, a dehydration condensation agent and a catalyst, reacting under the protection of inert gas, and filtering and recovering after the reaction is finished to obtain S-PS-EDTA resin; mixing glacial acetic acid, absolute ethyl alcohol and S-PS (at) EDTA resin for reaction, and filtering and collecting liquid after the reaction is finished; and rectifying the collected liquid to obtain the product. According to the method provided by the invention, metal impurities can be chelated in the synthesis process, and the electronic-grade ethyl acetate with high purity and low impurity content is produced.

The invention relates to environment-friendly hydrophobic ink and a preparation method thereof, and belongs to the technical field of water-based ink. A copolymerization modifier capable of being combined in a water-based polyacrylate emulsion in an initiation polymerization mode in the stage of preparing the modified water-based polyacrylate emulsion is prepared, and an o-hydroxy aromatic ketone structure in the copolymerization modifier can endow water-based ink with lasting ultraviolet absorption performance; the trifluoromethyl structure can reduce the surface energy of the water-based ink, and the benzimidazole ring structure can form stable coordinate bonds with metal ions, so that the bonding performance of the water-based ink and a metal substrate is enhanced; when the copolymerization modifier is used for modifying the water-based polyacrylate emulsion, the long-term performance, the hydrophobic and oil-resistant performance and the adhesion performance on the surface of a metal base material of the finished water-based ink can be effectively improved.

The invention discloses a dynamic borate bond-based self-healing polyacrylic acid binder and a preparation method thereof. The dynamic borate bond-based self-healing polyacrylic acid binder comprises a polymer main chain and a dynamic cross-linking agent, the dynamic cross-linking agent is a polyol compound containing at least two pairs of ortho-hydroxyl groups; the polymer main chain is formed by copolymerizing the following monomers: an acrylic structural monomer, the molar fraction of which accounts for 85-94% of the total monomer; a functional monomer containing a boric acid group, wherein the molar fraction of the functional monomer accounts for 3-8% of the total monomer; the mole fraction of the flexible monomer containing the acrylate group accounts for 3-8% of the total monomer. Various stresses generated by different negative electrode materials in circulation can be effectively adapted and buffered through a network formed by dynamic boric acid ester bonds and reversible fracture and combination of the boric acid ester bonds, so that the service life of the battery is generally prolonged, the working temperature range of the battery can be remarkably widened, the low-temperature discharge capacity can be remarkably increased, and the high-temperature cycle life can be prolonged.

The invention discloses a preparation method and application of a ceramic glaze layer protecting and repairing material, and belongs to the technical field of cultural relic protection. The preparation method comprises preparation of a core-shell self-repairing nanocapsule, and the preparation of the core-shell self-repairing nanocapsule comprises the following steps: reacting a calcium chloride solution with a sodium hydroxide solution, then adding sodium polyacrylate and nano ZnO, and carrying out dispersion, centrifugation, washing and other operations to prepare the nano Ca (OH) 2-ZnO composite material. The nano Ca (OH) 2-ZnO composite material of the core-shell self-repairing nanocapsule can be rapidly released through the 3.5 nm aperture of the mesoporous SiO2 shell, glaze layer cracks are physically filled and react with CO2 in air to generate CaCO3 crystals, crack plugging is achieved, meanwhile, dynamic disulfide bonds of a PU layer are broken and recombined under stress stimulation, a crack interface is repaired through chemical bonding, and the performance of the core-shell self-repairing nanocapsule is improved. The 24-hour crack repair rate is greater than or equal to 96%, and the limitation of'one-time repair 'of a traditional material is solved.

The application belongs to the field of concrete, and discloses a low-carbon and environment-friendly ultra-high performance concrete and a preparation method thereof.The low-carbon and environment-friendly ultra-high performance concrete comprises the following raw materials in parts by weight: 13-23 parts of water, 50-70 parts of cement, 5-15 parts of silica ash, 100-138 parts of fine aggregate, 20-50 parts of quartz powder, 5-12 parts of reinforcing fiber, 1-5 parts of additive, 0-0.5 parts of calcium polyacrylate (CPA), and 0-0.2 parts of silane coupling agent.The low-carbon and environment-friendly ultra-high performance concrete provided by the application can greatly reduce the dosage of cement, silica ash and other cementitious materials and the dosage of fiber compared with traditional ultra-high performance concrete, but still maintains excellent mechanical properties and durability.

The invention belongs to the technical field of functional finishing of textiles, and particularly relates to microcapsule emulsion with a pH indicating function, preparation of the microcapsule emulsion and application of the microcapsule emulsion in a textile finishing agent. The invention provides a preparation method of a microcapsule emulsion with a pH indication function, which comprises the following steps: reacting isocyanate with polyol to obtain a polyurethane prepolymer, mixing and dissolving the polyurethane prepolymer with a pH indicator solution, an acrylate monomer and an initiator to obtain an oil phase, and taking an aqueous solution of a polymer emulsifier as a water phase; then mixing and emulsifying the oil phase and the water phase, adding a chain extender, heating to carry out chain extension reaction, cross-linking to a certain degree to form a polyurethane-polyurea-polyacrylate hybrid shell layer on an oil-water interface, and coating a core material pH indicator to obtain the microcapsule emulsion with the pH indication function. According to the invention, the pH indicator is coated in the form of microcapsules for the first time, and industrial production and processing can be carried out.

The invention belongs to the technical field of secondary batteries, and discloses a polyurethane acrylate emulsion and a secondary battery. The polyurethane acrylate emulsion comprises water and a polymer dispersed in the water; the polymer comprises a core and a shell, the shell covers the core, the core comprises water, and the shell comprises urethane acrylate; the polyurethane acrylate comprises a polyurethane unit and a polyacrylate unit, and the polyacrylate unit comprises an organic silicon chain segment; on the basis of the mass of the polyurethane acrylate, the mass content of the organic silicon chain segment is 0.1%-10%. The polyurethane acrylate emulsion provided by the invention has the characteristics of high bonding strength, electrolyte corrosion resistance and good dispersity to a conductive agent, and when the polyurethane acrylate emulsion is used as a silicon-based negative electrode binder, the polyurethane acrylate emulsion can effectively cope with large volume change of a silicon-based material, the problem of interface failure of a silicon-based negative electrode is solved, and the cycle performance and the dynamic performance of a battery are improved.

The invention relates to the technical field of functional coatings of medical instruments, in particular to a temperature-sensitive response type sodium polyacrylate catheter leakage-proof coating, a preparation method and application thereof, and the coating is of a three-layer composite structure. And the bottom bonding layer adopts a polydopamine modified silane coupling agent system, contains silver nanoparticles, has the thickness of 5-15 microns, and ensures strong bonding and antibiosis of the substrate. The middle functional layer is a three-dimensional cross-linking degree gradient interpenetrating network polymer, is composed of a plurality of monomers and nano materials, and is 50-100 [mu] m in thickness, the cross-linking degree of the middle functional layer is gradually increased from inside to outside, gradient transition of mechanical properties is achieved, the outer protective layer is composed of a copolymer, is 3-8 [mu] m in thickness, and provides excellent anti-fouling and biocompatibility. The coating is endowed with strong adhesive force, gradient mechanical property and surface stability, the sodium polyacrylate component absorbs water and expands in urine to form sealing, and the expansion degree of the sodium polyacrylate component is regulated and controlled by the pH value and ionic strength of the urine.

The invention provides polyacrylic acid-carboxylated chitosan interpenetrating network hydrophobic modified hydrogel as well as a preparation method and application thereof, and belongs to the technical field of wastewater treatment. The preparation method comprises the following steps: mixing an acrylic monomer, a hydrophilic acrylate monomer, an etherification type acrylamide monomer, an allyl quaternary ammonium salt type hydrophobic monomer, a crosslinking monomer and water, then mixing with a chitosan compound, and adjusting the pH value to obtain a reaction solution; and mixing the reaction liquid and a photoinitiator, then carrying out polymerization reaction, and sequentially pre-freezing and freeze-drying the obtained polymer hydrogel. Through multiple synergistic effects of photo-initiated rapid polymerization, amphiphilic hydrophobic modification, etherification auxiliary crosslinking and a chitosan compound interpenetrating network, the structural stability, complexing efficiency, industrial applicability and heavy metal adsorption performance are comprehensively improved; the adsorption rate and capacity of the hydrogel disclosed by the invention are obviously superior to those of the existing similar polyacrylic acid-based or chitosan-based hydrogel.

The present application relates to a kind of high weather resistance and coating adhesion sunscreen coating and its preparation method, belong to sunscreen coating technical field;The present application uses the modifier with disulfide bond and polymerizable double bond to modify polyacrylate emulsion, significantly improve the flexibility of polyacrylate molecular chain after modification, reduce solidification shrinkage stress and internal stress, improve the coating adhesion of sunscreen coating of hard filler to matrix resin, it can also form stable chemical bonding between polyacrylate resin and titanium dioxide, provide stable stress transfer path, reduce the cracking and warping of coating, in addition, the modifier of the present application has good heat resistance aromatic ring structure, using the modifier of the present application can improve the heat resistance of sunscreen coating without introducing additional modifier.

The invention relates to the technical field of medical dressings, and discloses a preparation method of a three-dimensional structure hydrogel dressing for diabetic foot ulcers, the hydrogel dressing is prepared from polyvinyl alcohol, polyacrylic acid, hyaluronic acid, chitosan, poly (N-isopropylacrylamide), manganese dioxide and other materials, and through formula optimization and a 3D printing technology, the three-dimensional structure hydrogel dressing for diabetic foot ulcers is prepared. High-precision structure control is realized, and the preparation requirements of hydrogel dressings in complex shapes are met; strong electrostatic interaction and hydrogen-bond interaction occur between the interface of the grid structure hydrogel and the interface of the low-viscosity colloid, so that a stable three-dimensional flexible network structure is formed; the dressing has excellent flexibility, biocompatibility, antibacterial property and a function of promoting wound healing, and can be naturally gelated and participate in treatment of a wound microenvironment.

The invention relates to a renewable industrial flue gas carbon dioxide adsorbent and a preparation method thereof. The method comprises the following steps: S1, mixing alkali metal, an aluminum oxide precursor, silicon oxide and a first solvent, or mixing an alkali metal solution, the aluminum oxide precursor, the silicon oxide and an optional second solvent, and then molding the mixed material to obtain microsphere particles; s2, mixing the microsphere particles and organic amine, and carrying out first loading treatment and drying treatment to obtain an organic amine loaded material; s3, roasting the organic amine-loaded material, mixing the obtained roasted material with a carrier material, and carrying out second loading treatment, so as to obtain the carbon dioxide adsorbent, the carrier material is selected from at least one of polystyrene-polyacrylic acid-polyethylene oxide, polymethyl methacrylate-b-polystyrene, zirconium oxide and a porous ceramic material. The carbon dioxide adsorbent is relatively high in adsorption capacity and relatively good in selectivity, reproducibility and stability; and large-scale industrial production and application are facilitated.

The invention relates to the technical field of battery materials, in particular to a para-aramid lithium battery diaphragm and a preparation method thereof. The para-aramid lithium battery diaphragm comprises para-aramid slurry and a base membrane, the para-aramid slurry is coated on the two sides of the base membrane to form para-aramid coatings, and the para-aramid slurry comprises the following raw materials in parts by weight: 20-40 parts of modified para-aramid polymer liquid, 10-20 parts of nano ceramic composite material powder and 10-18 parts of a solvent; the nano ceramic composite material powder is prepared from the following raw materials in parts by weight: 50 to 100 parts of nano aluminum oxide, 8 to 12 parts of nano zirconium dioxide, 0.3 to 0.8 part of yttrium oxide, 1 to 5 parts of magnesium nitrate hexahydrate, 0.1 to 1 part of polyacrylic acid, 1 to 2 parts of ammonia water, 1 to 3 parts of coupling agent and 20 to 30 parts of silicon dioxide; the nano ceramic composite material powder is added into the para-aramid slurry, so that the para-aramid diaphragm has better thermal stability, and the phenomenon of thermal shrinkage of the diaphragm at high temperature is reduced.

The invention provides an adsorption material and a preparation method and application thereof, the adsorption material comprises a carrier and an endotoxin affinity binding ligand, the endotoxin affinity binding ligand comprises a recombinant C factor protein, and the carrier and the recombinant C factor protein are connected through a spacer arm; wherein the carrier comprises at least one of resin, chitosan, cellulose, agarose and glucan; the spacer arm comprises at least one of modified polyethylene glycol, polyvinyl pyrrolidone, polymethylacrylic acid-2-hydroxyethyl ester, polyvinyl alcohol, polyacrylic acid, hexamethylenediamine, divinyl sulfone and glutaraldehyde, and at least one end of the modified polyethylene glycol is provided with carboxyl, aldehyde or amino. The adsorption material provided by the invention can efficiently adsorb endotoxin, has the characteristics of low toxicity risk and excellent blood compatibility, and can improve the safety of blood purification.

The specific embodiment of the invention provides an anti-rust coating and a coating, the anti-rust coating comprises a water-based rust conversion agent and a water-based epoxy coating, the water-based rust conversion agent comprises a water-based acrylic emulsion and ammonium polyacrylate salt, the pH value of the water-based rust conversion agent is 6-8, Fe < 3 + > is converted into a stable complex in situ through a carboxyl chelation reaction, and the stable complex is added into the water-based epoxy coating. The water-based rust conversion agent and the epoxy coating have the advantages that the water-based rust conversion agent is added into the water-based epoxy coating, the continuous acid etching risk of a matrix is avoided, the water-based epoxy coating comprises polydopamine grafted and coated silicon dioxide, micropores can be reduced by the coating, permeation of water, oxygen and chloride ions can be inhibited, hydrolytic stripping and secondary corrosion can be prevented, and the water-based rust conversion agent and the epoxy coating have good compatibility; the formed coating is excellent in interlayer adhesive force and compact and firm in film layer, and the long-acting protection requirement in a severe corrosion environment can be met when the anti-rust coating is used for coating corrosion prevention of a steel member.

The application discloses a kind of binder, ceramic diaphragm and its secondary battery.The binder includes first polymer and second polymer, the first polymer and the second polymer are connected by chemical bond;The first polymer is polyacrylate polymer or SBR polymer containing first self-crosslinking structural unit, the Tg of the first polymer is ≤20 ℃, the second polymer is polyacrylic acid polymer or polyacrylamide polymer containing second self-crosslinking structural unit, the Tg of the second polymer is ≥80 ℃.The first polymer of low Tg is resistant to water and oil, but the heat resistance is generally, mainly plays the role of bonding, high Tg second polymer is resistant to oil and not resistant to water, mainly plays the role of heat resistance and improves electrolyte wettability, and by the interaction of first crosslinking structure and second crosslinking structure, so that binder simultaneously has excellent water and solvent resistance and heat resistance, and the affinity of electrolyte is better.

The invention discloses a PTC ceramic material and a preparation method thereof, and relates to the technical field of PTC, and the PTC ceramic material is prepared from the following components: 50-65 parts of barium titanate, 12-16 parts of lead tetraoxide, 0.1-0.3 part of yttrium oxide, 0.1-0.3 part of lanthanum oxide, 6-15 parts of modified silicon boride, 4-10 parts of aluminum oxide, 1-3 parts of ammonium polyacrylate, and 3-6 parts of polyvinyl alcohol. Through synergistic cooperation of a barium titanate main body and functional fillers such as modified silicon boride, leap-type improvement of the comprehensive performance of the PTC ceramic material is realized, on the basis of maintaining excellent PTC characteristics, the heat conductivity coefficient and the breaking strength of the material are effectively improved, the thermal shock resistance and the mechanical reliability are remarkably enhanced, and the PTC ceramic material has good application prospects. The method is especially suitable for the high-end application fields of automotive electronics, industrial control, high-power LED driving and the like.

The invention belongs to the technical field of lithium battery negative electrode slurry preparation, and discloses a lithium ion battery silicon-carbon negative electrode slurry homogenizing process and negative electrode slurry, and the lithium ion battery silicon-carbon negative electrode slurry homogenizing process comprises the following steps: uniformly mixing artificial graphite, silicon carbon, conductive carbon black and sodium carboxymethyl cellulose in proportion to obtain a mixture I; preliminarily mixing the mixture I with the single-walled carbon nanotube conductive slurry, sequentially adding a part of water, a polyacrylic acid binder, a molten carbonate compound, the remaining water and the rubber, and uniformly mixing the mixture I and the single-walled carbon nanotube conductive slurry; adding part of water until the solid content is 60-65%; the next substance is added after each substance is added and uniformly mixed, and the mixing temperature is not higher than 40 DEG C. According to the scheme, the technical problems of bubble and pit defects on the surface of the coated pole piece and poor surface density consistency can be effectively solved.

The invention discloses a sulfide all-solid-state battery silicon negative electrode binder and a preparation method and application thereof, and belongs to the technical field of all-solid-state batteries. The silicon negative electrode binder for the sulfide all-solid-state battery comprises a poly (acrylic acid-co-poly (ethylene glycol) methacrylate) grafted metal nanowire compound, can be well adhered to a pure silicon negative electrode, has excellent mechanical performance and also endows interface impedance regulation and control capability; on one hand, the tolerance to the volume change of the pure silicon negative electrode can be greatly improved, and cracks and pulverization in silicon can be effectively prevented, so that the pure silicon negative electrode has excellent cycle performance; and on the other hand, the interface impedance between the pure silicon negative electrode and the sulfide electrolyte can be effectively reduced, so that the pure silicon negative electrode has excellent rate capability. In addition, the sulfide all-solid-state battery silicon negative electrode binder is obtained only through two-step reaction, the preparation process is greatly simplified, meanwhile, the characteristic of high yield is achieved, and large-scale production is easier.

The invention discloses an adhesive tape for battery insulation and a compounding process thereof, and relates to the technical field of battery insulation. The adhesive tape for battery insulation is prepared by taking a polyimide film as a base film and coating an adhesive, the adhesive is prepared from the following raw materials in parts by weight: 70 to 90 parts of polyacrylate emulsion, 6 to 12 parts of isocyanate curing agent, 4 to 8 parts of terpene resin, 10 to 18 parts of modified aluminum hydroxide, 5 to 9 parts of modified aluminum oxide, 7 to 14 parts of nano montmorillonite, 0.8 to 2.5 parts of antioxidant 168, 0.5 to 2 parts of ultraviolet light absorber UV-327, 2.5 to 5 parts of silane coupling agent KH-570, 31 to 48 parts of propylene glycol methyl ether acetate and 3 to 6 parts of glycerol. The adhesive tape for battery insulation is matched with modified aluminum hydroxide and aluminum oxide to synergistically improve the performance. The product has excellent insulativity, heat resistance and stability, the processing process is controllable, and strict use requirements in the field of batteries are met.

The invention provides a sodium ion specific fluorescence labeled transparent soil sample as well as a preparation method and application thereof, and belongs to the technical field of rock soil and geological engineering. The method comprises the following steps: firstly, sequentially carrying out hydrophilization treatment, solvent evaporation and dissolution on a sodion combined benzofuran isophthalate probe to obtain a probe mother solution; mixing the probe mother solution, a buffer solution, an inorganic sodium salt solution and a solvent to prepare a fluorescence labeling pore solution; and finally, mixing the sodium polyacrylate particles and the fluorescence labeled pore liquid, and performing vacuum saturation treatment to obtain the transparent soil sample. The transparent soil sample provided by the invention still keeps excellent optical transparency while having sodium ion specific response capability, so that a stable and reliable experimental medium is provided for in-situ, real-time and full-field observation of sodium ion migration.

The invention discloses polyacrylate anti-deposition and cerium chloride synergistic composite corrosion inhibitor cooling liquid, relates to the field of cooling liquid, and is particularly suitable for a multi-metal cooling system. According to the method, polyacrylate, cerium chloride, benzotriazole, benzimidazole, ethylene glycol, deionized water and triethanolamine serve as core raw materials, during preparation, equipment and the raw materials are pretreated, then a base solution is prepared, the pH value is adjusted to be alkalescent, then polyacrylate and cerium chloride are dissolved and coordinated, an auxiliary corrosion inhibitor is added, and synergistic protection is formed. And defoaming, filtering and filling. The cooling liquid adapts to multi-metal material protection through the synergistic effect of deposition resistance of polyacrylate and corrosion inhibition and synergism of cerium chloride, the cooling liquid is diluted according to working conditions during application, waste cooling liquid is discharged after being subjected to combined treatment of biological contact oxidation and Fenton oxidation, a finished product needs to be stored in a proper environment in a sealed mode, and the protection performance, the environmental protection property and the storage stability are effectively considered.

The invention provides an organic acid excited solid waste-based cementing material, and belongs to the technical field of solid waste utilization. The solid waste-based cementing material excited by the organic acid comprises 90-105 parts by mass of a silicon-aluminum solid waste base material, 7-12 parts by mass of sulfate and 15.3-19.8 parts by mass of a composite organic acid exciting agent, wherein the composite organic acid exciting agent comprises main acid and polyacrylic acid, and the mass of the polyacrylic acid is 10%-40% of the mass of the main acid; the main acid is one or a mixture of citric acid and tartaric acid. According to the organic acid excited solid waste-based cementing material, strong base is prevented from being adopted as an exciting agent, and the defects of a strong base excitation system are avoided.

The invention belongs to the field of polymer coatings, and provides an aliphatic polyurethane finish paint with high adhesion resistance and a preparation method thereof. According to the invention, a polyurethane phase and a polyacrylate network are adopted to construct a semi-interpenetrating network structure, cyclic carbonate and hydrolyzable silane end groups are introduced into double-end functionalized polysiloxane, and a silicon-oxygen network surface layer is self-assembled after coating and curing; the high crosslinking density with the gel fraction being greater than or equal to 85%, the wear-resistant and anti-slip performance with the dry friction coefficient being greater than or equal to 0.50 and the abrasion mass loss being less than or equal to 0.030 g / 500 r, the ultra-low surface energy anti-dirt performance with the water contact angle being greater than or equal to 105 degrees and the surface free energy being less than or equal to 22 mN / m and the environment-friendly characteristic that the volatile organic compound content is less than or equal to 50 g / L are achieved; the three technical contradictions of high gel fraction and ultralow surface energy silica surface layer coupling, high hardness wear resistance and high friction coefficient maintenance, and high solid content and low volatility organic compound processing window and nano gradient silica surface layer construction are solved, and the nano gradient silica coating has wide application value in the field of industrial terraces and metal base material coatings.

The invention discloses a high-wear-resistance nano filler modified rubber material and a preparation method thereof, and belongs to the technical field of rubber material modification. The preparation method comprises the following steps: by taking water-soluble polyacrylic acid micelles as a template, controlling the hydrolysis rate of tetraethyl orthosilicate by regulating and controlling the dosage of ammonia water, so as to prepare hollow SiO2 nanoparticles with a porous shell layer and a stable structure; and then synergistic modification is carried out through a PEG-PLA block copolymer and a silane coupling agent KH550, so that the dispersity and compatibility of particles are improved. And blending and banburying the modified porous hollow SiO2 particles and butadiene styrene rubber slurry, and carrying out vulcanization molding to obtain the modified rubber material. The wear resistance and tensile strength of the rubber are improved, good elasticity and elongation at break are kept, high strength, high wear resistance and high toughness are considered, and the process is mild and controllable.

The invention discloses an anti-ultraviolet heat-insulating radiation-proof water-based glass paint and a preparation process thereof. The anti-ultraviolet heat-insulating radiation-proof water-based glass paint is prepared from the following raw materials in parts by weight: 30-50 parts of acrylic resin, 5-10 parts of a coalescing agent, 3-8 parts of butyraldehyde, 10-20 parts of nano titanium dioxide, 8-15 parts of nano tin antimony oxide, 2-5 parts of a polyacrylate dispersant, 2-5 parts of a polyurethane thickener and 15-30 parts of deionized water. Comprising the following steps: S1, weighing deionized water, a polyacrylate dispersing agent and a polyurethane thickening agent according to a ratio, and adding into a stirring kettle; and stirring at the rotating speed of 400rpm for 8 minutes. Through the synergistic effect of the nano titanium dioxide and the nano tin antimony oxide, the anti-ultraviolet, heat-insulating and anti-radiation functions are achieved at the same time, and the problem that an existing glass paint is single in function is solved; the polyacrylate dispersing agent is adopted, so that the dispersity of the nano functional filler is effectively improved, the agglomeration phenomenon is avoided, and the uniformity of the paint film performance is ensured.

The application provides a sodium ion battery positive electrode slurry, a positive electrode pole piece and a preparation method thereof and a sodium ion battery, and relates to the technical field of sodium ion batteries, and comprises a positive electrode active material, a conductive agent, a binder, a composite dispersing agent and a solvent; the composite dispersing agent is a product formed by mechanically mixing an ionic dispersing agent and a polyoxyethylene ether non-ionic dispersing agent or a composite formed by a chemical reaction between the ionic dispersing agent and the polyoxyethylene ether non-ionic dispersing agent, wherein the ionic dispersing agent is polyacrylic acid and its derivatives; and the positive electrode active material is a polyanion material. The ionic dispersing agent of polyacrylic acid and its derivatives and the polyoxyethylene ether non-ionic dispersing agent are used in combination in the positive electrode slurry, so that the positive electrode slurry has good dispersibility and stability; the provided positive electrode slurry has good dispersibility, the positive electrode pole piece has low resistance, and the sodium ion battery has excellent cycle performance.

This invention discloses a method and sensor for adiponectin detection using a polyaniline and polyacrylic acid-modified wire mesh carbon electrode, relating to the field of adiponectin detection technology. The method involves electrochemically activating the wire mesh carbon electrode, electropolymerizing it to form a polyaniline-polyacrylic acid composite modification layer, immobilizing adiponectin monoclonal antibody after activation with N-hydroxysuccinimide and 1-ethyl-3-(3-dimethylaminopropyl)carbodiimide, blocking the antibody with bovine serum albumin, and reacting it with a serum sample. The adiponectin concentration is determined based on the peak potential shift and peak current change. This invention simultaneously achieves both conductive transport and antibody immobilization, reduces non-specific adsorption and serum interference, and improves detection sensitivity, repeatability, and quantitative accuracy.

This application discloses a nuclear-grade polyacrylic acid, its preparation method, and its applications. The nuclear-grade polyacrylic acid has a molecular weight of 100,000 to 200,000 and a sulfur content of 500 ppb to 1000 ppb. This nuclear-grade polyacrylic acid exhibits controllable molecular weight, good polydispersity, excellent scale inhibition performance, and a superior decomposition half-life. The molecular weight is controllable between 100,000 and 200,000, and the polydispersity is 1.0 to 3.5. The preparation method has a short cycle time and simple operation process; the preparation equipment is simple, and the preparation efficiency is high. The volume of the synthesis reactor used in the preparation can be adjusted according to the production volume, greatly improving the production efficiency. The preparation cost of this invention is low, and it is green, clean, and pollution-free. The raw materials used in the preparation process are inexpensive and readily available. The reactor involved only consumes a small amount of electricity, and the addition of a sulfur-free initiator and alcohol and ether-related solvents results in minimal environmental pollution.