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91 results about "Sodium Thiosulfate Pentahydrate" patented technology

Phase transition temperature adjusting system and phase transition temperature adjusting cup

ActiveCN104887011AHeat absorption and release performance are highly matchedGuaranteed to drink normallyDrinking vesselsCarbon nanotubeSodium Thiosulfate Pentahydrate
The invention relates to a phase transition temperature adjusting cup, which comprises a cup body outer casing, a cup body inner casing and a top cover, and the composite phase transition material is filled between the inner casing and the outer casing. The composite phase transition material comprises phase transition material, a nucleating agent, heat conduction filling material and a thickening agent. The phase transition material is selected from one or more of sodium acetate trihydrate, sodium thiosulfate pentahydrate, twelve disodium hydrogen phosphate, sodium sulfate decahydrate and decahydrate. <{EN4}>The nucleating agent is selected from one or more of borax, sodium phosphate dibasic anhydrous, diatomaceous earth, silica, sodium silicate, eight water strontium hydroxide, hexahydrate chloride strontium. <{EN5}>The heat conduction filling material is selected from one or more of graphite, carbon nanotube, expanded graphite, carbon fiber, graphene, three-dimensional graphite foam, silicon carbide, copper powder. <{EN6}>The thickening agent is selected from one of polyacrylic acid emulsion or carboxymethylcellulose sodium. <{EN7}>Compared with existing temperature adjusting cups, the phase transition temperature adjusting cup of the present invention has the advantages of rapid cooling, simple structure convenient operation, 3-4 hours of comfort temperature zone, and not being restricted from external environment.
Owner:YUTIAN ENERGY CO LTD

Inorganic hydrated salt phase change energy storage microcapsule and preparation method thereof

Belonging to preparation methods of energy storage microcapsule materials, the invention provides an inorganic hydrated salt phase change energy storage microcapsule and a preparation method thereof. The energy storage microcapsule includes an inorganic hydrated salt serving as the core material and an inorganic material serving as the wall material. The core material is one or more of potassium fluoride dehydrate, sodium acetate trihydrate, sodium thiosulfate pentahydrate, calcium chloride hexahydrate, magnesium sulfate heptahydrate, barium hydroxide octahydrate, sodium sulfate decahydrate, sodium sulfate decahydrate, disodium hydrogen phosphate dodecahydrate, ammonium aluminium sulfate dodecahydrate, aluminum potassium sulfate dodecahydrate, and aluminum sulphate ocatadecahydrate. The wall material is one or more of silicon dioxide, calcium carbonate, alumina and titanium dioxide. The core material accounts for 30%-80% of the mass of the microcapsule composite material, and the wall material accounts for 20%-70% of the mass of the microcapsule energy storage material. The prepared phase change energy storage microcapsule material has a phase transition temperature of 25-100DEG C and a diameter of 0.1-50 micrometers. The phase change energy storage microcapsule has the advantages of high encapsulation rate, good sealing performance, large phase change potential heat value, and simple preparation method, and has great industrial application prospect.
Owner:CHINA UNIV OF MINING & TECH

Inorganic hydrous salt phase change microcapsule energy-storage material and preparing method

The invention relates to a preparing method of an inorganic hydrous salt phase change microcapsule energy-storage material and belongs to preparing methods of energy-storage materials. The energy-storage material comprises a core material and a wall material, wherein the core material is prepared from one or more of calcium chloride hexahydrate, sodium sulfate decahydrate, sodium thiosulfate pentahydrate, disodium hydrogen phosphate dodecahydrate, sodium acetate trihydrate and sodium carbonate decahydrate inorganic hydrous salt, and the wall material is prepared from one or more of polystyrene, polymethyl methacrylate, poly(ethyl acrylate), polyurethane, cellulose acetate butyrate (CAB) and a diphenylmethane diisocyanate polymer, the core material accounts for 30-80% of the microcapsule energy-storage material by mass, and the wall material is prepared from the polymer and accounts for 20-70% of the microcapsule energy-storage material by mass. The phase change point of the obtained phase change microcapsule energy-storage material ranges from 20 DEG C to 90 DEG C, and the particle size ranges from 1 micrometer to 100 micrometers. The phase change microcapsule energy-storage material prepared with the method is high in encapsulation rate, good in sealing performance, large in phase change latent heat value, simple in preparing method and large in industrial application prospect.
Owner:CHINA UNIV OF MINING & TECH

Oil well deep composite blocking profile control agent and application thereof

The invention relates to an oil well deep composite blocking profile control agent and the application thereof. The composite blocking profile control agent comprises the following components: gel blocking agent solution, particle blocking agent, authigene air source and surface active agent, wherein in the gel blocking agent solution, the weight ratio of the partially hydrolyzed polyacrylamide, the sodium bichromate and the sodium thiosulfate pentahydrate is 1:0.025:0.35, a water solution with the total weight concentration of 0.5-1% is prepared from the partially hydrolyzed polyacrylamide, sodium bichromate and sodium thiosulfate pentahydrate, and hydrochloric acid capable of adjusting the pH of the gel blocking agent solution to 3.5-4.5 is contained; the particle blocking agent comprises phenolic resin and phenolic resin, wherein the weight ratio of the phenolic resin and the phenolic resin is 1:0.06; the authigene air source is CO(NH2) 2; the surface active agent is alkylaryl sulfonate; the weight ratio of the gel blocking agent solution, the particle blocking agent, the authigene air source and the surface active agent is 60:6:2:1. According to the composite blocking profile control agent disclosed by the invention, deep blocking and profile control at the oil layer of an oil well is realized through the Jamin Effect of foam generated in the deep part of stratum and the physical blocking function of a solid phase blocking agent.
Owner:PETROCHINA CO LTD

Method for preparing spherical cadmium sulfide (CdS) semiconductor film

The invention relates to a method for preparing a spherical cadmium sulfide (CdS) semiconductor film, which comprises the following steps of: putting cadmium acetate into a beaker, dripping oleic acid into the beaker, uniformly mixing the cadmium acetate and the oleic acid, and adding distilled water into the mixture to obtain solution A; adding sodium thiosulfate pentahydrate into the solution A and performing ultrasonic dispersion to obtain solution B; adding a film forming aid into the solution B and performing ultrasonic processing to form a uniform sol C; fixing a substrate to a cathode of an electrodeposition device, immersing the substrate in the sol C for electrodeposition to obtain a cadmium sulfide film D, and diluting the solution subjected to electrodeposition by ten times to obtain solution E; and pouring the solution E into a hydrothermal reaction kettle, putting the film D into the hydrothermal reaction kettle, immersing the film D in the solution E, naturally cooling to room temperature after the reaction is finished, taking the film D out, and cleaning and drying the hydrothermal reaction kettle to obtain a CdS photoelectric film on the surface of the substrate. In the method, the reaction is finished in a liquid phase and subsequent crystallization and thermal treatment are avoided; processing equipment is simple; the quality of the film is controlled by controlling the deposition voltage, deposition time, the pH value of a precursor and microwave hydrothermal postprocessing; and the obtained film has high purity and uniformity.
Owner:SHAANXI UNIV OF SCI & TECH

Preparation method of adsorbent containing SnO2/Sb2O5, product and application of adsorbent

The invention relates to a preparation method of an adsorbent containing SnO2/Sb2O5. According to the method, SbCl3 with a stable chemical property and low toxicity is taken as a Sb source, sodium thiosulfate pentahydrate, namely SnCl4, is utilized as a Sn source, and a SnO2/Sb2O5 binary composite oxide is prepared. The preparation method comprises the following steps of oxidizing Sb<3+> as Sb(V) in a non-water system taking alcohol as a solvent by adopting the combination of H2O2 oxidation and ultraviolet irradiation, further carrying out hydrolytic precipitation on Sb(V) and Sb<4+> by utilizing a small amount of water introduced by utilizing H2O2 solution as a reactant, and forming a binary SnO2/Sb2O5 composite oxide. The method provided by the invention has the advantages that the hydrolyzing speed of Sb<3+> is slow, the generation of the Sb2O3 is effectively controlled, the Sn/Sb2O5 binary composite oxide with the Sb<3+> oxygenation efficiency being 100% is obtained, the adsorbent can remove the radioactive isotope Co ions and a complex thereof and stable isotope Co ions and a complex thereof, and the adsorptive property of the SnO2/Sb2O5 binary composite oxide and pure Sb2O5 obtained by the introduction of Sb is improved by 200 times.
Owner:TSINGHUA UNIV

Preparation method of sulfur/sisal fiber charcoal lithium ion battery composite negative electrode material

The invention discloses a preparation method of a sulfur/sisal fiber charcoal lithium ion battery composite negative electrode material. The method comprises the following steps: (1) deionized water is used for respectively preparing acid and sodium thiosulfate pentahydrate into an acid solution and a sodium thiosulfate solution whose concentrates are 1-2mol/L; (2) sisal fiber is cut into small segments of 2-3 centimetres, sisal and the two solutions in the step (1) are mixed, then ultrasonic concussion is carried out for 25-35 minutes, a hydrothermal reaction is carried out for 12-16 hours, reaction temperature is 120-200 DEG C, washing with water is carried out till the solution is neutral, and drying is carried out; (3) calcination is carried out in an inert gas atmosphere whose gas flow is 20-100ml/min for 0.5-2 hours, heating rate of calcination is 1-10 DEG C/min, natural cooling is carried out to room temperature, and the sulfur/sisal fiber charcoal lithium ion battery compositenegative electrode material is obtained. The method has the advantages of low raw material cost, green and environmental protection, and simple preparation technology; and a new approach is provided for preparation of the lithium ion battery negative electrode material.
Owner:GUILIN UNIVERSITY OF TECHNOLOGY

Method for crystallizing sodium thiosulfate pentahydrate

The invention discloses a method for crystallizing sodium thiosulfate pentahydrate, which particularly comprises the following steps of: continuously feeding sodium thiosulfate solution with the concentration of less than 51Be' into an Oslo cooling crystallizer and continuously feeding the obtained solution into a heat exchanger through a circulating pump for the cooling and temperature reduction; and when the temperature is reduced to a saturation temperature, adding seed crystals in one step, and continuously discharging crystal mush and carrying out solid and liquid separation, wherein the crystallization temperature is in the range of 30 to 38 DEG C and the crystallization retention time is in the range of 15 to 20 hours. In the invention, the Oslo cooling crystallizer capable of maintaining stable growth of the crystals and realizing circulation of clear liquid is used so as to provide an excellent condition for the growth of the crystals; on the basis of continuous operation, large and uniform crystals can be grown, the purity of the product reaches over 99 percent, and the granularity of the product is over 3mm; compared with a discontinuous crystallizer, the production capacity of the Oslo cooling crystallizer capable of continuously operating in unit effective volume is improved by over 30 percent; operation parameters in the continuous crystallizing process are stable; the products have stable quality and no differences among batches; and automatic control can be realized.
Owner:CITIC JINZHOU METAL +1

Preparation method of metallic oxide/conducting polymer dually-modified sulfur composite anode material

The invention relates to a preparation method of a metallic oxide/conducting polymer dually-modified sulfur composite anode material. First, sodium thiosulfate pentahydrate and polyvinylpyrrolidone are adopted for synthesizing hollow nano-sulfur particles, and through the structure, the utilization rate of sulfur is increased, and expansion and shrinkage stress generated in the lithiation process can be released inwards; second, the outer layer of hollow nano-sulfur is wrapped with polyaniline, high-temperature sulfidizing is utilized for generating strong chemical bonds between polyaniline and sulfur, and polyaniline is promoted to have a physical barrier and a chemical acting force at the same time to jointly inhibit loss of polysulfide compounds, and the stability of battery circulation is improved; last, good electrochemical performance of nickel metal hydroxide is utilized for conducting external modification, the wettability of the composite material and the transmission efficiency of ions and electrons are improved, and the electrochemical performance of a lithium-sulfur battery is further improved. The lithium-sulfur battery prepared through the method has the advantages of being high in energy density, good in circulating performance, good in rate capability and the like.
Owner:WUHAN UNIV OF TECH

Antifouling and wear-resisting textile material and preparation method thereof

The invention discloses an antifouling and wear-resisting textile material and a preparation method thereof. The antifouling and wear-resisting textile material is prepared from the following raw materials in parts by weight: 10 to 25 parts of acrylonitrile fibers, 12 to 25 parts of carboxymethyl cellulose, 2 to 10 parts of nano-microcrystalline cellulose, 10 to 20 parts of bamboo charcoal fibers, 11 to 28 parts of diglycidyl ether, 3 to 5 parts of lauryl alcohol, 1 to 3 parts of bis-(phenyldimethyl siloxane)methylsilanol, 4 to 6 parts of beta-hydroxybutyrate, 1 to 3 parts of sodium thiosulfate pentahydrate, 8 to 14 parts of terephthaloyl chloride, 3 to 7 parts of fluorosilane, 1 to 4 parts of methyl L-pyroglutamate, 2 to 3 parts of benzoyl peroxide butyl acetate, 3 to 5 parts of 2,2'-(ethylenedioxy)dianiline, 1 to 2 parts of zinc diricinoleate, 1 to 2 parts of barium metaborate, 2 to 5 parts of an adhesive, 2 to 5 parts of a dispersant and 1 to 4 parts of a thermal stabilizer. The antifouling and wear-resisting textile material prepared by the preparation method has good wear-resisting performance and also has an antifouling property. Meanwhile, the invention further discloses the preparation method of the antifouling and wear-resisting textile material.
Owner:SUZHOU COMFORT TEXTILE NEW MATERIALS TECH CO LTD

Preparation method and application of rod-like nickel disulfide-molybdenum disulfide nano-composite

The invention relates to a preparation method and application of a rod-like nickel disulfide-molybdenum disulfide nano composite. The preparation method comprises the following steps: dispersing nickel nitrate hexahydrate and sodium thiosulfate pentahydrate in deionized water, adding hexadecyl trimethyl ammonium bromide, stirring, adding ethylenediamine, uniformly stirring, transferring into a high-pressure reaction kettle for reaction, centrifugally separating, cleaning with ethanol and deionized water, drying, calcining in a tubular furnace to obtain nickel disulfide, weighing ammonium tetrathiomolybdate and nickel disulfide, adding ammonium tetrathiomolybdate and nickel disulfide into an N,N-dimethylformamide solution, adding hydrazine hydrate, carrying out ultrasonic treatment, transferring the mixed solution into a high-pressure reaction kettle for reaction, centrifugally separating, cleaning with ethanol and deionized water, drying to obtain a rod-like nickel disulfide-molybdenumdisulfide nano-composite, dispersing the composite into a mixed solution of water, ethanol and perfluorosulfonic acid, dropwise coating on the surface of a clean glassy carbon electrode and naturallyair-drying to form a three-electrode system together with a platinum wire and a saturated calomel electrode, wherein the clean glassy carbon electrode is used as a working electrode.
Owner:YANGZHOU UNIV

Method for preparing superfine alumina-chromic oxide or alumina and chromic oxide by using aluminium-chromium mud

The invention relates to a method for preparing superfine alumina-chromic oxide or alumina and chromic oxide by using aluminium-chromium mud which is a chromium ore industrial solid waste, belonging to the technical field of preparation processes of inorganic nonmetallic materials and waste solid recycling and regeneration. The method comprises the following steps of: taking the solid waste aluminium-chromium mud as raw material, washing, sieving, adding hydrochloric acid for dissolving, filtering to remove solid impurities, adding ammonia and polyethylene glycol in the filtrate to generate precipitation, filtering, and drying the precipitation to obtain a solid mixture of superfine aluminium hydroxide and chromium hydroxide. Superfine alumina-chromic oxide can be prepared by baking the solid mixture at the temperature of 250-300 DEG C after thermal decomposition. Superfine alumina can be prepared by adding hydrogen peroxide in the solid mixture, filtering, separating the precipitation and solution, drying the precipitation and baking at the temperature of 140-150 DEG C. Superfine chromic oxide can be finally obtained by adding proper amount of hydrochloric acid, sodium thiosulfate pentahydrate and polyethylene glycol in the solution, adjusting the pH of the solution to 1-1.5, adjusting the pH of the solution to 7-8 when the color of the solution is similarly green in the reaction process to enable chromium hydroxide to spontaneously deposit, and baking the obtained chromium hydroxide precipitation at the temperature of 200-300 DEG C.
Owner:SHANGHAI UNIV

Radiating structure of heat accumulating light emitting diode (LED) lamp

The invention discloses a radiating structure of a heat accumulating light emitting diode (LED) lamp. The radiating structure comprises a lampshade, an LED chip, a radiating pedestal, a heat accumulating box, a lamp body, a screw mouth and a lamp electrode tip, wherein the LED chip is tightly attached to the radiating pedestal; the lamp body is fixedly connected with the radiating pedestal by the heat accumulating box; a control circuit is arranged in the lamp body; and the control circuit is connected with the LED chip by using a lead. The heat accumulating box is sealed, a heat accumulating material is put into the heat accumulating box, and the heat accumulating material is sodium thiosulfate pentahydrate, the melting point of which is about 50 DEG C. The radiating structure has the advantages that: a fan for radiating is not used, and a moving component is not installed; the LED lamp is reliable in use and energy-saving, and has no noise; heat generated when the LED chip works is absorbed by using melting latent heat of the heat accumulating material, so that the temperature of the LED chip is controlled, and the LED chip is effectively prevented from being impacted by heat; and the radiating structure is easy to make and install and convenient to produce.
Owner:林勇
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