The invention provides a preparation method of a low-
sulfur diesel oil anti-wear agent, and belongs to the technical field of carbon-containing fuel
processing, and the preparation method comprises the following steps: adding
sodium oleate,
tetrabutylammonium bromide and
xylene into a three-necked flask, uniformly stirring and mixing, heating, dropwise adding 3-chloro-1, 2-
propylene glycol, continuously heating until
reflux, centrifuging, and carrying out rotary
evaporation to obtain glyceryl monooleate; the preparation method comprises the following steps: dispersing NCC in
xylene, adding
lauric acid and p-toluenesulfonic acid, and carrying out heating,
reflux reaction, cooling,
centrifugation, washing and
drying under the protection of an
inert atmosphere to obtain modified NCC; the preparation method comprises the following steps: heating and melting glyceryl monooleate, adding
silane modified
silicon dioxide, stirring, carrying out ultrasonic treatment, cooling to obtain a modified nano-composite, adding the modified NCC and a stabilizer, stirring, and carrying out ultrasonic uniform mixing to obtain the low-
sulfur diesel oil anti-wear agent. The diesel oil anti-wear agent provided by the invention can improve the
wear resistance of diesel oil under the condition that the addition amount is relatively low, and improve the low-temperature fluidity and demulsifying performance.