2986 results about "Stearic acid" patented technology

The invention relates to the technical field of insulating materials, in particular to insulating powder and a preparation method thereof. The invention discloses a flame-retardant coating which comprises the following components in parts by weight: 15-25 parts of epoxy resin, 10-20 parts of aluminum hydroxide, 5-12 parts of nano boron nitride, 1-3 parts of a silane coupling agent KH-560, 3-8 parts of polytetrafluoroethylene micro powder, 2-6 parts of fluorine-modified montmorillonite, 4-9 parts of melamine cyanurate, 2-5 parts of nano titanium dioxide, 1-4 parts of a fluorine-modified graphene oxide-polyaniline composite material and 0.5-2 parts of pentaerythritol stearate. The anti-corrosion coating is prepared from the following components in parts by weight: 1 to 3 parts of nano zinc oxide, 5 to 10 parts of glass fiber, 2 to 5 parts of polyhedral oligomeric silsesquioxane-polyimide copolymer, 1 to 4 parts of ferrocenyl epoxy resin and 0.5 to 2 parts of perfluorooctyltriethoxysilane. The insulation powder is high in corrosion resistance, excellent in insulation, heat dissipation and mechanical performance, environmentally friendly in processing, good in adaptability, capable of prolonging the service life of equipment and reducing the cost, suitable for special environments and wide in popularization prospect.

The invention relates to a high-stability bronze powder pigment and a preparation method and application thereof.The preparation method comprises the following steps that copper-zinc alloy coarse powder, stearic acid and a dissolved compound passivator are taken and subjected to ball milling in the nitrogen atmosphere, and a ball milling product is screened, washed and subjected to suction filtration to obtain an amino-functionalized passivated base material; the preparation method comprises the following steps: dispersing SiO2 in anhydrous isopropanol to obtain a reaction system, adding deionized water and a catalyst, dissolving tetraethoxysilane and phenyltriethoxysilane in anhydrous isopropanol, slowly dropwise adding, carrying out a heat preservation reaction, and carrying out suction filtration and washing to obtain a phenyl modified SiO2 coated intermediate; the preparation method comprises the following steps: dispersing a compound stabilizer in anhydrous isopropanol to obtain a mixed system, heating and stirring, dissolving the compound stabilizer in anhydrous isopropanol, dropwise adding into the mixed system, reacting, centrifuging, washing, and drying in vacuum to obtain the bronze powder pigment. The bronze powder pigment disclosed by the invention has excellent oxidation resistance, chemical corrosion resistance and long-term storage stability, and can keep the natural color gloss of metal to the greatest extent.

The invention discloses a flexible fireproof cable and a preparation method thereof, and belongs to the technical field of cables. The cable comprises a conductor, a mica insulation layer, a copper protection layer, a buffer layer and a cable sheath layer. The buffer layer is made of a polyurethane foaming material; the cable sheath layer is prepared from the following components in parts by weight: 80 to 100 parts of methyl vinyl silicone rubber, 18 to 20 parts of modified carbon black, 5 to 8 parts of titanium dioxide, 1 to 2 parts of platinum catalyst, 3 to 6 parts of hydroxyl silicone oil, 0.5 to 1 part of zinc stearate and 0.8 to 1 part of dicumyl peroxide. The modified carbon black is added into the raw materials of the sheath layer, so that the compatibility, the interface bonding force and the flame retardant property of the carbon black and a silicone rubber matrix are effectively improved, and the mechanical property, the wear resistance and the fireproof property of the cable sheath layer are remarkably enhanced.

The invention discloses a high-weatherability sound insulation wood plastic wallboard and a preparation method thereof, the high-weatherability sound insulation wood plastic wallboard comprises the following raw materials by weight: 30-40 parts of wood flour or plant fiber, 25-35 parts of a sound insulation functional filler, 35-45 parts of high density polyethylene, 2-2.5 parts of maleic anhydride grafted high density polyethylene, 1-1.5 parts of stearic acid, 3-4.5 parts of a weatherability auxiliary agent, and 1-1.5 parts of azodicarbonamide. The problems of cracking, deformation and the like caused by moisture absorption expansion are relieved by optimizing the proportion and compatibility of the wood flour and the plastic, and then the problems of weather resistance and sound insulation of the wallboard outdoors are solved by filling the porous sound absorption material.

The application provides a masterbatch type vulcanization aid and a preparation method thereof, a rubber composition, a rubber product and a tire. The preparation method comprises the following steps: S1, pre-reaction of stearic acid, an antioxidant and a vulcanization system to obtain a pre-reaction mixture; and S2, mixing of the pre-reaction mixture with rubber to obtain the masterbatch type vulcanization aid. Under the catalysis of stearic acid, the reagents in the antioxidant and the vulcanization system react to generate active intermediates. The active intermediates have the effect of promoting vulcanization and play the role of activating accelerators in advance, so that the active intermediates can replace the role of zinc oxide. The product after reaction is mixed with rubber, and the masterbatch formed can be used to prepare rubber products such as tires without containing zinc elements, so that zinc emission can be realized, and the environment is friendly.

The application discloses a kind of derived biomass hard carbon material pulverization process, belong to biomass charcoal material processing technical field, first, pulverization process includes the following steps: after drying, the coconut shell derived hard carbon block is carried out primary crushing, while spraying first modifier, obtain the particle size 1~3mm of coarse crushing modified particle;Coarse crushing modified particle is carried out secondary precision crushing under argon atmosphere, while spraying second modifier, obtain the precision crushing modified particle of D 50 Particle size is 15 μm;Precision crushing modified particle is carried out roll grinding spheroidization, while spraying third modifier, obtain the spherical modified particle of D 50 Particle size is 10 μm;Spherical modified particle is carried out flash drying after cooling, then add magnesium stearate to it, after mixing, obtain derived biomass hard carbon material.Then, the application realizes breakthrough in tap density, particle size distribution, first efficiency and other core indexes by the coordination of three-stage gradient modification and progressive pulverization process.

The invention discloses a biodegradable polylactic acid composite material and a preparation method thereof, and relates to the technical field of polylactic acid materials. The method comprises the steps that firstly, chitosan activated through hydrochloric acid is subjected to graft modification through a KH550 silane coupling agent, meanwhile, nano-zinc oxide is subjected to surface modification through stearic acid, the chitosan and the nano-zinc oxide are mixed, spray drying is conducted, and antibacterial composite powder is prepared; the preparation method comprises the following steps: performing hydrochloric acid activation and KH570 silane coupling agent modification on nano silicon dioxide, performing hydroxypropylation modification on alkali lignin, and performing reflux crosslinking reaction on the modified alkali lignin, KH570 modified nano silicon dioxide, polycaprolactone, methyl methacrylate and azodiisobutyronitrile to prepare a heat-resistant reinforcer; uniformly mixing polylactic acid, poly (butylene succinate), the antibacterial composite powder, the heat-resistant reinforcer, tributyl citrate, polyethylene glycol and talcum powder, and extruding and granulating by using a twin-screw extruder to obtain the heat-resistant antibacterial material. The composite material prepared by the invention has excellent antibacterial property, heat resistance and biodegradability.

The invention discloses high-performance anti-wear engine lubricating oil as well as a preparation method and application thereof. The high-performance anti-wear engine lubricating oil is prepared from the following raw materials: self-developed lubricating oil base oil, poly-alpha-olefin, zinc dialkyl dithiophosphate, calcium sulfonate, polyisobutylene succinimide, an antioxidant, polymethacrylate, an organic molybdenum complex, a de-foaming agent and a pour point depressant. The preparation method comprises the following steps: 1) synthesizing 9, 10-bis (2-tert-butyl-4-methylphenoxy) trimethylolethane stearate as base oil of the lubricating oil; and 2) mixing the base oil with other assistants to obtain the high-performance anti-wear engine lubricating oil. According to the preparation method, novel-like synthetic ester oil is firstly prepared, a phenol group and a large steric hindrance substituent group are introduced into a polymer, the anti-oxidation function is directly built in base oil molecules, meanwhile, super-strong heat resistance is achieved, and finally the high-performance anti-wear engine lubricating oil is obtained and can be applied to high-end application scenes such as aero-engines or gas turbines.

The invention provides a grinding fluid, the grinding fluid comprises a base fluid, a grinding material, nano-diamond and a dispersion stabilizer, the base fluid comprises polyether and silicone oil, the grinding material comprises surface modified silicon carbide particles, and the dispersion stabilizer comprises polyethylene glycol stearate and polyvinylpyrrolidone. The surface roughness of a grinding piece can be reduced, the scratch density and microcracks of the surface are reduced, damage of grinding fluid to the grinding piece is reduced or even avoided, and the service life of a cutter can be prolonged. The invention also provides a preparation method of the grinding fluid and a process method using the grinding fluid.

The invention discloses a degradable express bag material and a preparation method thereof, and relates to the technical field of high polymer materials. The invention discloses a degradable express bag material. The composite material is prepared from the following raw materials in parts by weight: 40 to 50 parts of poly (butylene adipate-co-terephthalate), 20 to 30 parts of polycaprolactone, 5 to 8 parts of modified bamboo fiber, 2 to 4 parts of modified nano montmorillonite, 3 to 6 parts of tributyl citrate, 0.1 to 0.3 part of antioxidant 1076, 1 to 2 parts of iron dithiocarbamate master batch, 2 to 3 parts of maleic anhydride grafted poly (butylene adipate-co-terephthalate) and 0.3 to 0.6 part of zinc stearate. 0.1 to 0.3 part of baicalein; and 1 to 3 parts of chitosan-sorbitol composite coating liquid. According to the degradable express bag material, poly (butylene adipate-co-terephthalate) and polycaprolactone are used as main degradable raw materials, modified bamboo fibers and modified nano-montmorillonite are matched to enhance the mechanical property, an antioxidant 1076, baicalein and the like are added to guarantee the stability and functionality, temperature is accurately controlled in the preparation process, multi-step modification is adopted for optimizing component combination, and the degradable express bag material is prepared. The performance is improved through the composite coating, degradability is achieved, and good usability is achieved.

The invention relates to the technical field of cheese, and provides a vegetable fat composition, vegetable cheese and a preparation method thereof, the vegetable fat composition comprises myristic acid and stearic acid in a mass ratio of (19-22): (2.5-4.5), and the melting point of the vegetable fat composition is 24.0-26.0 DEG C. The coconut oil is subjected to two-stage dry fractionation, coconut oil fractionation components obtained through separation are combined according to a certain proportion to form the coconut oil composition with specific fatty acid composition and a certain melting point range, and when the coconut oil composition is applied to preparation of the vegetable cheese, the taste problem of the existing vegetable cheese can be solved.

The invention discloses a preparation method of a rubber waterstop material with a low compression set rate, which comprises the following steps: firstly, carrying out blending reaction on hydroxyl silicone oil and boric acid to obtain liquid polyborosiloxane; the preparation method comprises the following steps: adding liquid polyborosiloxane and natural rubber into an internal mixer according to a ratio, and carrying out internal mixing to obtain a mixture; adding zinc oxide, an anti-aging agent, stearic acid and an anti-tearing agent into the obtained mixture, and continuously mixing; continuously adding kaolin talcum powder, calcium carbonate, calcium oxide, white carbon black, N550, N330 and KH550, and internally mixing again to obtain a preform; adding a vulcanization accelerator and a vulcanizing agent into the preform, and continuously mixing to obtain a rubber material to be vulcanized; and vulcanizing and forming the rubber material to be vulcanized to prepare the rubber water-stop belt material with the low compression set rate. According to the invention, the compression set rate of the rubber material can be reduced while the tensile strength, elongation, tear resistance and other properties of the rubber are not sacrificed, so that the product performance is enhanced.

The invention discloses a waterproof long-lasting oil-control gel composition and a preparation method thereof, and belongs to the technical field of cosmetics. The composition comprises 4-6 parts of an oil absorption compound A, 9-13 parts of an oil absorption compound B and 70-95 parts of a gel matrix, wherein the oil absorption compound A is prepared from mesoporous silica and poloxamer 407, and the aperture of the oil absorption compound A is 5-10 nm; the oil absorption compound B is prepared from polymethyl methacrylate microspheres, isododecane and polyglycerol-3 diisostearate, and the pore diameter of the oil absorption compound B is 150 to 300 nm. According to the invention, through dual mechanisms of temperature response and volatilization driving, a dynamic gradient structure of bottom layer small aperture-surface layer large aperture is formed at skin temperature, and directional migration of grease is realized; meanwhile, the surface property transformation of the material after oil absorption is creatively utilized, a hydrophobic membrane is formed on the surface of the polymethyl methacrylate microsphere, a self-enhanced waterproof barrier is constructed, the unique effect that the more oil is absorbed, the more water is resisted is achieved, the problem of makeup removal caused by sebum and sweat can be effectively solved, and the makeup lasting time is remarkably prolonged.

The invention belongs to the technical field of building materials, and particularly relates to a preparation method of a biomass reinforced cement-based thermal insulation wall material and the wall material. The preparation method comprises the following steps: (1) crushing wood fibers, putting the crushed wood fibers into a NaOH solution, washing with water and drying; (2) carrying out dry mixing on cement, the modified wood fiber, nano SiO2 particles and calcium stearate; (3) diluting hydrogen peroxide with warm water, adding into the mixture, and stirring; (4) injecting the foaming slurry into a mold, and vibrating; and (5) steam curing. Through a collaborative technology of fiber surface modification, nano-particle regulation and control and hydrophobic layer construction, the comprehensive performance breakthrough of the fireproofing grade of A1 grade, the heat conductivity coefficient of 0.048-0.055 W / (m.K) and the compressive strength of 1.2-1.8 MPa is realized. The energy consumption is reduced by 70% through the low-temperature steam curing process, the proportion of agricultural waste is larger than or equal to 30%, the carbon emission intensity is smaller than or equal to 150 kgCO2 / m < 3 >, and the requirement for green buildings is met.

The application provides a zinc-free vulcanization aid, a rubber composition, a rubber product and a tire. The zinc-free vulcanization aid is prepared by the following method: zinc oxide, stearic acid, an antioxidant, a vulcanization system medicine are pre-reacted in a solvent, and after pre-reaction, filtration for removing zinc and solvent removal are sequentially performed to obtain the zinc-free vulcanization aid. The zinc-free vulcanization aid contains an active intermediate generated by pre-reaction, the intermediate has the effect of promoting vulcanization, and plays the role of activating the accelerator in advance, so that it can partially or completely replace the role of zinc oxide in the ordinary formula. The zinc-free rubber product can be prepared by using the zinc-free vulcanization aid, zinc emission is realized, the environment is friendly, and through the action of the zinc-free vulcanization aid, the rubber composition can obtain the rubber properties such as crosslinking density, hardness, modulus, hysteresis and the like close to those of the zinc-containing rubber without containing zinc.

The invention discloses a self-lubricating aluminum coating and a preparation method thereof.The preparation method comprises the steps that molybdenum disulfide is pretreated through a silane coupling agent, tetraethoxysilane mixed liquor is added, the pH is adjusted to be 9-10, a water bath reaction is conducted, and molybdenum disulfide-silicon dioxide microcapsules are obtained after high-temperature strengthening treatment; respectively adding a zinc nitrate solution and a hexamethylenetetramine solution, adjusting the pH value to 10-11, carrying out a high-temperature and high-pressure hydrothermal reaction to obtain zinc oxide nanorods, and carrying out ball milling treatment on the zinc oxide nanorods, microcapsules, stearic acid and zirconium oxide balls under the protection of argon to obtain doped microcapsules; after raw materials are pretreated, the raw materials and a dispersing agent solution are added into a mixer respectively, spraying powder, a pretreated base body and the spraying powder are obtained after mixing treatment, spraying treatment is conducted on the surface of the base body through a plasma spraying method, and the self-lubricating aluminum coating is obtained after vacuum annealing treatment. Therefore, the obtained self-lubricating aluminum coating is low in friction coefficient, high in performance and excellent in self-lubricating property.

The invention discloses a biological challenge device with combined adjustable resistance for evaluating the effect of a sterilization process, which comprises a shell, the shell comprises a plastic pipe and an inner pipe cap detachably connected with the inner wall of the plastic pipe, the inner pipe cap is provided with a breathable window and covered by a breathable film, and a bacterial contamination carrier for bearing indicator biological spores is attached to the inner bottom of the plastic pipe. An openable container containing a liquid culture medium is arranged in the plastic pipe cavity; the outer side of the inner pipe cap is sleeved with an outer pipe cap detachably connected with the outer wall of the plastic pipe, and the outer pipe cap is provided with a flow blocking structure used for adjusting the speed of the sterilizing agent entering the area of the inner pipe cap; the indicator biological spores are pretreated by a stable protective agent containing one or more of polyethylene glycol, trehalose, sorbitol, polyvinylpyrrolidone and glyceryl stearate. The speed of a sterilizing agent entering the device can be limited, the spores are dry in a suspension added with a stable protective agent, the capability of resisting general environmental changes is very good, and the performance of the device can be maintained for a long time.

The invention discloses a high-whiteness EVA chemical foaming sole material and a preparation method thereof, and belongs to the technical field of footwear products. The EVA chemical foaming sole material is formed by chemical foaming of an EVA composite raw material. The EVA composite raw materials mainly comprise 50 to 70 parts of EVA, 20 to 40 parts of an olefin thermoplastic elastomer, 0.4 to 0.7 part of a peroxide cross-linking agent, 2 to 4 parts of an AC foaming agent, 1 to 2 parts of zinc oxide, 0.3 to 0.8 part of 6-hydroxy-1, 2, 3, 4-tetrahydroquinoline, 0.5 to 1 part of nano zinc carbonate and 0.5 to 1 part of pentaerythritol tetrastearate. The whitening effect of the sole material can be realized on the premise of protecting the EVA foaming-crosslinking structure; therefore, the attractiveness of the product is improved, the durability is better, the mechanical properties and other properties of the EVA foamed sole are not influenced, and the high-quality requirements of elasticity, pressure resistance, comfort and the like of sports shoes can be met.

A green and sustainable tire base rubber composition and a preparation method, relating to the technical field of tire production. The composition comprises a tire base. The tire base comprises 100 parts by weight of cis-1,4-polyisoprene, 20-40 parts by weight of bio-based carbon black, 0-20 parts by weight of bio-based silicon, 0-20 parts by weight of a silane coupling agent, 1-3 parts by weight of stearic acid, 2-7 parts by weight of zinc oxide, 0.5-2 parts by weight of a carbon black coupling agent, 1.5-3.5 parts by weight of the antioxidant 6PPD, 0.5-2 parts by weight of the antioxidant TMQ, 1.5-2 parts by weight of oil-extended sulfur powder, and 1.5-3.0 parts by weight of the accelerator CZ. The use of the carbon black coupling agent reduces the heat build-up of a rubber material, however, the Mooney viscosity of the rubber is significantly increased. Once a dedicated process has been used, the viscosity of the rubber material is controlled, and the tanδ value of the heat build-up of the rubber material at 60°C is significantly reduced, so that the rolling resistance of a tire is reduced, and the tire maintains good physical and mechanical properties.

The invention relates to the field of resource recycling, and discloses an iron slag ash and waste soil composite curing agent as well as a preparation method and application thereof. The composite curing agent comprises the following components in parts by weight: 30-50 parts of iron slag ash; 20 to 40 parts of waste soil; 10-20 parts of industrial alkaline residues; 5-10 parts of a functional auxiliary agent; 3-5 parts of a curing synergist; the curing synergist is composed of an inner core and a coating layer, the inner core material comprises a porous carrier and an exciting agent, and the film forming material of the coating layer is one or more of stearic acid, paraffin and polyethylene wax; the weight ratio of the core material to the coating layer material is (8-9): 1. According to the composite curing agent, resource utilization of waste is achieved, the material cost is remarkably reduced, and the composite curing agent is particularly suitable for flow-state backfilling, light filling and sludge in-situ curing and has remarkable environmental protection and economic benefits.

The invention discloses a polyethylene composite geomembrane and a processing technology thereof in the field of geosynthetic materials. The polyethylene composite geomembrane is prepared from the following raw materials: high-density polyethylene, polyethylene grafted maleic anhydride, a nano montmorillonite / low-density polyethylene composite modifier, an antioxidant, a light stabilizer and a lubricant calcium stearate. Wherein the polyethylene grafted maleic anhydride is prepared by drying high-density polyethylene, mixing the dried high-density polyethylene with maleic anhydride, an initiator and an antioxidant, and performing melt extrusion through a double-screw extruder, so that the surface polarity is improved; the nano-montmorillonite / low-density polyethylene composite modifier is prepared by ultrasonically dispersing Na-montmorillonite, adding hexadecyl trimethyl ammonium bromide, stirring, centrifugally drying to obtain organic modified montmorillonite, mixing the organic modified montmorillonite with low-density polyethylene, performing intercalation reaction, and performing twin-screw extrusion and blending, so that the barrier property is enhanced. The processing technology comprises the steps of raw material mixing, twin-screw extrusion granulation and calendaring molding, and finally the polyethylene composite geomembrane with remarkably improved interface cohesiveness, weather resistance and barrier property is prepared.

The invention provides a high-toughness plastic packaging film material and a preparation method thereof, and belongs to the field of metallocene polyolefin plastics. The high-toughness plastic packaging film material is prepared from the following chemical raw materials: 80 to 90 parts of metallocene polyethylene resin, 5 to 8 parts of supramolecular cross-linking agent, 6 to 10 parts of core-shell type modifier, 3 to 5 parts of ethylene-vinyl acetate copolymer, 2 to 4 parts of stearic acid modified nano calcium carbonate, 2 to 3 parts of polyolefin elastomer, 0.2 to 0.5 part of di (3, 4-dimethyldibenzylidene) sorbitol, 2 to 5 parts of thermotropic liquid crystal polymer and 0.4 to 0.7 part of antioxidant. 0.8 to 1.2 parts of a lubricant and 0.5 to 1.0 part of an antistatic agent. Through the compatibility design of a toughening mechanism, the synergistic balance of an enhancing mechanism and the optimization of transparency guarantee, the functions of all the components in a metallocene polyethylene resin matrix are complemented, and the ultrahigh toughness, high strength and high transparency of the film material are achieved.

The present invention discloses a high thermal conductivity rubber material and a preparation method thereof, and relates to the technical field of rubber production, the high thermal conductivity rubber material comprises a rubber matrix, modified carbon black, a vulcanizing agent, a composite accelerator, an anti-aging agent, zinc oxide, stearic acid, white carbon black, montmorillonite and aramid pulp according to a weight ratio of 100: (40-60): (1.5-3): (2-4): (1-3): (3-8): (1-3): (10-20): (5-15): (3-8); the modified carbon black is prepared by reacting a composite modifier solution prepared from a silane coupling agent, sodium alginate, ammonium polyacrylate, tea polyphenol, polyethyleneimine, nano aluminum oxide and deionized water with carbon black; the composite accelerant is prepared by carrying out pre-dispersion treatment on N-cyclohexyl-2-benzothiazole sulfenamide, tetramethylthiuram disulfide, a rare earth complex and nano zinc oxide. The prepared high-thermal-conductivity rubber material is good in mechanical property and thermal conductivity.

The invention belongs to the technical field of preparation of chloroprene rubber, and provides bio-based plasticizer modified chloroprene rubber and a preparation method thereof. The bio-based plasticizer is chlorinated palm oil methyl ester and is prepared by mixing chloroprene rubber, carbon black, chlorinated palm oil methyl ester, an anti-aging agent, zinc oxide, magnesium oxide, stearic acid and an accelerant according to a certain proportion. A proper amount of chlorinated palm oil methyl ester is added, so that the flexibility and cold resistance of the chloroprene rubber are effectively improved, and the chloroprene rubber still can keep relatively good elasticity and use performance in a low-temperature environment. The environment protection and the re-biochemistry of the plasticizer are realized, the dependence on non-renewable resources is reduced, and the potential harm to the environment is reduced. And the original good physical and mechanical properties, such as tensile strength, of the chloroprene rubber are maintained. Conventional rubber processing equipment and process are adopted, operation is easy, control is easy, the method is suitable for industrial production, and good application prospects and economic benefits are achieved.

The invention relates to the field of sealing materials, in particular to a butyl rubber sealing material and a preparation method thereof. Comprising the following components in parts by weight: 50-70 parts of butyl rubber, 30-50 parts of a brominated isobutylene-p-methylstyrene copolymer, 30-50 parts of carbon black, 8-12 parts of an alkyl phenolic resin vulcanizing agent, 3-5 parts of zinc oxide, 1-3 parts of stearic acid, 1-3 parts of an anti-aging agent and 5-10 parts of a plasticizer. The butyl rubber provides ideal air tightness and heat aging resistance, bromine atoms are introduced into the brominated isobutylene-p-methylstyrene copolymer, co-vulcanization with the butyl rubber is achieved, it is ensured that a uniform and stable co-crosslinking network can be formed between the two rubber molecules, and the service life of the rubber is prolonged. The alkyl phenolic resin vulcanizing agent can form a C-C bond with high bond energy with two rubber molecules, so that the thermal aging resistance of the butyl rubber sealing material is effectively improved, the compression set is reduced, and the butyl rubber sealing material with excellent performance is prepared.

The invention relates to a preparation method of a high-elastic wear-resistant rubber sole. Comprising the following steps: S1, uniformly mixing 50-60 parts by weight of epoxy resin, 10-20 parts by weight of a polyurethane-acrylate copolymer, 20-30 parts by weight of an elastic complex, 3-5 parts by weight of stearic acid, 1-4 parts by weight of zinc oxide, 3-5 parts by weight of zinc stearate and 2-4 parts by weight of zinc oxide; the preparation method comprises the following steps: uniformly mixing 1-3 parts by weight of magnesium oxide and 1-3 parts by weight of an AC foaming agent in an internal mixer at the temperature of 60-70 DEG C, internally mixing for 30-60 minutes, continuously mixing for 15-20 minutes at the temperature of 90-95 DEG C, granulating after open milling, and standing for 20-24 hours at room temperature to obtain a molding master batch; s2, putting the molding master batch into a foaming mold for compression molding, controlling the mold closing pressure to be 15-25MPa, then heating to 180-190 DEG C together with the foaming mold, performing vulcanization treatment for 8-15 minutes, cooling, and performing standing treatment at room temperature for 20-24 hours to obtain the high-elasticity wear-resistant rubber sole. According to the high-elastic wear-resistant rubber sole, the preparation method and the damping shoe, a good damping effect is achieved, and certain mechanical strength is achieved.

The invention provides a high-temperature-resistant and corrosion-resistant ammonia water nozzle coating and a preparation method thereof, and belongs to the field of coatings. The ammonia water nozzle coating is composed of a self-repairing metal ceramic bonding layer, an organic-inorganic hybrid corrosion-resistant layer and a functional surface layer which are sequentially arranged in a stacked mode. A coating of the self-repairing metal ceramic bonding layer is composed of the following components of 90-99 parts of NiCrAlY alloy and 1-8 parts of self-repairing microcapsules. A coating of the organic-inorganic hybrid corrosion-resistant layer is prepared from the following components: 40 to 60 parts of fluorinated polyurethane prepolymer, 20 to 40 parts of silicon-aluminum sol, 1 to 8 parts of disulfide bond modified epoxy resin and 10 to 20 parts of magnesium-aluminum hydrotalcite; the coating of the functionalized surface layer is prepared from the following components: 20 to 30 parts of stearic acid modified TiO2 particles, 60 to 80 parts of waterborne polyurethane and 2 to 7 parts of ionic liquid modified SiO2 nanoparticles. The corrosion resistance, the high temperature resistance and the self-repairing capacity of the ammonia water nozzle are improved at the same time.

The invention relates to the technical field of rubber materials, in particular to a wear-resistant non-slip rubber outsole material and a preparation method of the wear-resistant non-slip rubber outsole material. The rubber material is prepared from the following components in parts by mass: 10 to 40 parts of natural rubber, 10 to 20 parts of epoxidized natural rubber, 40 to 80 parts of itaconate rubber, 10 to 60 parts of rice husk white carbon black, 5 to 20 parts of lignin, 5 to 20 parts of cellulose filler, 1 to 6 parts of coupling agent, 1 to 6 parts of dispersing agent, 0.5 to 2 parts of paraffin, 1 to 5 parts of resin, 1 to 3 parts of antioxidant, 1 to 5 parts of active agent, 0.5 to 2 parts of stearic acid, 1 to 3 parts of accelerant and 1 to 3 parts of sulfur. According to the invention, a bio-based rubber material is used as a matrix, various reinforcing fillers and processing aids from bio-based sources are used, the mechanical strength, wear resistance and slip resistance of the material are improved through a modified composite technology, and a material support is provided for green and sustainable development of shoe materials.

The invention relates to a waterproof sealing gasket material for a shield tunnel and a preparation method of the waterproof sealing gasket material. The preparation method comprises the following steps: plastifying raw rubber to obtain plastified raw rubber; the preparation method comprises the following steps: stirring and mixing plasticated raw rubber, carbon black N550, calcium carbonate, paraffin oil, zinc oxide, stearic acid, calcium oxide, an anti-aging agent and an organic magnesium compound, mixing in a mixing mill, and cooling to room temperature to obtain a mixture I; stirring and mixing the mixture I, modified NPE particles and an accelerant, mixing, and cooling to room temperature to obtain a mixture II; uniformly mixing the mixture II and sulfur in a mixing mill, vulcanizing at high temperature, and standing at room temperature for 24 hours to obtain the waterproof sealing gasket material. According to the waterproof sealing gasket material, the modified NPE particles of the core-shell structure are added, the compatibility of a water-swelling material and non-polar rubber is improved, the organic magnesium compound is added as a multifunctional auxiliary agent, the interface bonding, vulcanization network and flame retardant performance are synergistically improved, and the waterproof sealing gasket material has good waterproof performance. The prepared sealing gasket material has excellent mechanical properties, heat aging resistance, compression set resistance and flame retardance.

The invention relates to the technical field of equipment temperature control, in particular to a 12-hydroxystearic acid production reaction temperature control method based on artificial intelligence, and the method comprises the following steps: calculating a reaction heat release index based on the hydrogen feeding instantaneous molar flow at the current moment so as to represent theoretical heat generated through chemical reaction in unit time; based on the output power of the stirring motor at the moment and fluid mechanics characteristics, a viscosity correction factor used for representing the heat transfer capacity attenuation degree caused by the material viscosity change is constructed; in combination with the reaction heat release index and the viscosity correction factor at the current moment, performing energy compensation and nonlinear correction on the actually measured temperature in the kettle at the current moment to obtain a target predicted temperature; the control of the 12-hydroxystearic acid production reaction temperature is realized based on the target predicted temperature at the current moment, and the accuracy of the control of the 12-hydroxystearic acid production reaction temperature can be effectively improved.