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107 results about "Lithium borate" patented technology

Lithium borate, also known as lithium tetraborate is an inorganic compound with the formula Li₂B₄O₇. A colorless solid, lithium borate is used in making glasses and ceramics.

High-toughness ultrathin flexible glass and preparation method thereof

The invention discloses high-toughness ultrathin flexible glass and a preparation method thereof, and relates to the technical field of glass manufacturing. The ultrathin flexible glass is prepared from the following raw materials: silicon dioxide, aluminum oxide, lithium oxide, sodium oxide, magnesium oxide, a modified nano reinforced phase, a high-temperature melting regulator and cerium dioxide. The modified nano reinforced phase is prepared by the following steps: pre-treating silicon carbide and silicon nitride with hydrochloric acid, and mixing with nano zirconium oxide to obtain a mixture; and modifying the mixture with a silane coupling agent to obtain the modified nano reinforced phase. The high-temperature melting regulator is a mixture of lithium borate, sodium sulfate and lithium fluoride. The preparation method of the ultra-thin flexible glass comprises the following steps: preparing the modified nano reinforced phase, melting and homogenizing the glass, forming the glass substrate, and preparing the ultra-thin flexible glass. The ultra-thin flexible glass prepared by the invention has relatively high fracture toughness and structural rigidity, excellent flexibility and bending fatigue durability, and excellent thermal shock resistance.
Owner:LONGGUANGTIANXU SOLAR ENERGY ZHUCHENG

Electrolyte composition

Provided herein is an electrolyte composition for a lithium-ion battery, the composition comprising: (a) 18-35 wt% of lithium salt; (b) 1-25 wt% of solvent additive; and (c) 45-80 wt% of solvent. The total amount of (a), (b) and (c) is less than or equal to 100 wt% of the electrolyte composition. The lithium salt comprises lithium bis(fluorosulfonyl)imide (LiFSI), lithium 4,5-dicyano-2-(trifluoromethyl)imidazole (LiTDI) and lithium difluoro(oxalato)borate (LiDFOB). The solvent additive comprises one or more fluorinated and / or unsaturated carbonate compounds. The solvent comprises a cyclic carbonate. Also provided is an electrochemical cell comprising the electrolyte composition, an electrochemical energy storage device comprising the electrochemical cell, and uses associated with the electrolyte composition.
Owner:DYSON TECH LTD

Health state monitoring method for mining emergency lithium battery pack

The invention relates to the technical field of battery management systems, in particular to a method for monitoring the health state of a mining emergency lithium battery pack, a battery cell electrolyte contains 0.08%-0.15% of nano cerium oxide, 0.15%-0.25% of lithium borate and 0.03%-0.08% of amino trimethylene phosphonic acid, and a diaphragm is coated with 0.8%-1.2% of a graphene-carbon nanotube-molybdenum sulfide composite coating. The method comprises the following steps: S1, deploying a multi-dimensional sensor, collecting voltage, current and other data, and dynamically adjusting the sampling frequency; s2, carrying out noise reduction, abnormal value elimination and interpolation completion on the data; s3, extracting characteristic parameters such as capacity attenuation rate; s4, detecting the content of POF3, and associating the capacity fading rate; s5, modeling by using an improved BP neural network, and outputting an SOH value; and S6, triggering grading early warning according to the SOH value and the POF3 content. According to the method, through material innovation and multi-dimensional monitoring, SOH evaluation precision is improved, faults are early warned in advance, environmental adaptability and safety prevention and control are enhanced, the defects of a traditional method are overcome, and mining emergency power supply safety is guaranteed.
Owner:BEIJING ZHIYUAN UNITED TECH CO LTD

Preparation method of lithium cyanoborate derivative

The invention discloses a preparation method of a cyanoborate lithium salt derivative, which comprises the following steps: 1, mixing an alcohol compound, a lithium source compound, a boron source compound and trimethylsilyl cyanide in a polar organic solvent, and filtering after complete reaction to obtain a cyanoborate crude product filtrate; the alcohol compound is selected from one of 2, 2, 2-trifluoroethanol, 2, 2-difluoroethanol, 2-fluoroethanol, 3-hydroxypropionitrile, allyl alcohol and propargyl alcohol; the lithium source compound is selected from one of lithium carbonate and lithium hydroxide; the boron source compound is selected from one of boric acid, diboron trioxide and boron tribromide; the reaction temperature is controlled to be 0-120 DEG C; and 2, adding an inert organic solvent into the cyanoborate crude product filtrate for crystallization, and performing vacuum drying to obtain a finished product of the cyanoborate lithium salt. The method has the advantages of high yield and purity, simple process, convenience in operation and low cost, and is extremely suitable for industrial production.
Owner:ZHANGJIAGANG GUOTAI HUARONG NEW CHEM MATERIALS CO LTD

A multi-element coated ternary positive electrode material and a preparation method thereof

The present application relates to the technical field of lithium ion battery cathode material, in particular to a kind of multi-element coated ternary cathode material and preparation method thereof.The present application provides a kind of multi-element coated ternary cathode material, the ternary cathode material includes lithium nickel cobalt manganese oxide ternary cathode material and the lithium niobium tungsten borate coating material attached to its surface, wherein the chemical composition general formula of the lithium niobium tungsten borate coating material is LiNb 1‑6x / 5‑3y / 5 W x B y O3, 0 The mass of the lithium niobium tungsten borate coating material is 0.02%~0.4% of the mass of the lithium nickel cobalt manganese oxide ternary cathode material.The coulomb efficiency of the ternary cathode material provided by the present application can reach 98.2%, the 100 cycle capacity retention rate can reach 88.4%, and the reversible capacity can reach 182mAh / g.Furthermore, the preparation process of the ternary cathode material is simple, the production cost is low, and it is suitable for mass production.
Owner:TIANJIN UNIV

Electrolytes, batteries, battery packs, and battery systems for lithium (sodium) ion batteries

This invention discloses an electrolyte, battery, battery pack, and battery system for a lithium (sodium) ion battery, comprising an ionic electrolyte containing lithium borate ester (sodium salt) or lithium imine ester (sodium salt); an isoelectric point solvent of triethylamine ester, triethanolamine ester, borate ester, or phosphate ester; electrolyte 20%–50%, solvent 50%–80%. The ionic electrolyte developed in this invention is an organic compound with no ignition point and high safety, and can be used under operating conditions with voltages greater than 5 volts. The voltage of a typical lithium-ion battery is 3.4 volts. Furthermore, the electrolyte used in this invention is used in very small quantities, thus reducing overall cost and resulting in higher economic benefits. The zwitterionic polar solvent of this invention separates molecules into ions based on the charge carried by the material molecules. Due to its isoelectric point, it provides fast charging and discharging capabilities, increasing the ion transfer rate by 2-3 times or more than that of typical carbonate solvents.
Owner:牟华琪 +1

Method for rapidly and accurately measuring multiple elements of limestone powder based on fuse piece method

The invention discloses a method for rapidly and accurately determining multiple elements of limestone powder based on a fuse piece method, and belongs to the technical field of material detection. A fuse piece scheme is designed aiming at the characteristics of fine particles, easy moisture absorption and the like of limestone powder instead of improving a general scheme of materials such as limestone, dolomite and the like, key parameters are optimized, the flux ratio is set as follows: the ratio of lithium tetraborate to lithium metaborate is 67: 33, melting is divided into three processes of preheating, pre-oxidation and melting, the melting temperature is effectively controlled to be 1060 DEG C, the time is 60 seconds, and the melting efficiency is greatly improved. The problem that limestone powder is prone to excessive melting or uneven melting is solved, the matrix effect and the particle size effect are greatly reduced, it is verified that three limestone powder standard samples with known components are selected for testing, the relative error between the result and the standard value is smaller than 1%, data meet the strict allowance requirement of the industry, and compared with an existing fuse piece method, the method has the advantage that the cost is low. The detection adaptability to the limestone powder is remarkably improved, and the component detection requirements of mainstream limestone powder in the industry can be met.
Owner:TIANJIN HUANENG YANGLIUQING POWER CO LTD

Electrolyte, lithium secondary battery, and electric device

An electrolyte, a lithium secondary battery and a power utilization device, the electrolyte comprising a first solvent, a silane compound containing a carbon-carbon double bond and a cyclic lithium borate compound, the first solvent comprising a cyclic carbonate compound; wherein the mass content W3 of the cyclic carbonate compound, the mass content W1 of the silane compound containing a carbon-carbon double bond and the mass content W2 of the cyclic lithium borate compound satisfy: 0.001≤(W1+W2) / W3≤2.67 based on the total mass of the electrolyte. The combination of the silane compound containing a carbon-carbon double bond and the cyclic lithium borate compound can improve the flexibility and thermal stability of the SEI film, thereby reducing the gas generation degree during the cycle and storage of the lithium secondary battery, and improving the storage performance, fast charging performance and cycle performance of the lithium secondary battery.
Owner:CONTEMPORARY AMPEREX TECHNOLOGY CO LTD

Method for detecting silicon dioxide, calcium oxide and magnesium oxide in fly ash

The invention discloses a method for detecting silicon dioxide, calcium oxide and magnesium oxide in fly ash, which comprises the following steps: firing the fly ash at a certain temperature for a certain time, weighing a certain amount of fired sample, preparing a glass sheet by using lithium tetraborate-lithium metaborate as a flux and ammonium iodide as a release agent in a melting furnace at a certain temperature for a certain time, and then sintering the glass sheet in a sintering furnace at a certain temperature for a certain time. The X-ray fluorescence intensity of silicon, calcium and magnesium is determined through an X-ray fluorescence spectrometer, so that the determination of silicon dioxide, calcium oxide and magnesium oxide is completed. The method is simple to operate, high in analysis speed, accurate in result and easy to master.
Owner:BAOTOU IRON & STEEL (GROUP) CO LTD

Method for detecting content of each element in slag

PendingCN121595620AMaterial analysis using wave/particle radiationLithium metaborateSlag
The invention discloses a method for detecting the content of each element in slag. The method comprises the following steps: 1) pre-melting a sample; 2) manufacturing a glass sheet; (3) carrying out spectrum detection on the glass sheet prepared in the step (2) by utilizing a fluorescence spectrophotometer; wherein in the step 1), a mixed flux of lithium tetraborate and lithium metaborate and sodium nitrate are used for pre-melting treatment of a sample, and a sample melt is obtained; in the step (2), a mixed flux of lithium tetraborate and lithium metaborate is used for conducting melting treatment on the sample melt again, and the glass sheet is obtained.By means of the method, determination of CaO, SiO2, MgO, Al2O3, MnO, TiO2 and P2O5 in the furnace slag can be completed at the same time.
Owner:BAOTOU IRON & STEEL (GROUP) CO LTD

Method for detecting contents of CaO, SiO2 and total Al in slag pressing agent containing elemental aluminum

The invention belongs to the technical field of analysis and detection, and relates to a method for detecting the content of CaO, SiO2 and total Al in a slag pressing agent containing elemental aluminum. Comprising the following steps: S1, crushing a sample, uniformly mixing the sample, raising the temperature of a high-temperature furnace to 850 DEG C, and setting X fluorescence parameters; s2, pre-oxidizing the sample: putting a to-be-detected slag pressing agent sample containing elemental aluminum into a platinum gold crucible with a wall hung by using a mixed flux of lithium tetraborate and lithium metaborate; weighing lithium carbonate; uniformly mixing, and pre-oxidizing in a high-temperature furnace at 850 DEG C; s3, sample melting: taking out the pre-oxidized sheet and placing the pre-oxidized sheet in a 1050 DEG C sample melting furnace; melting is conducted for 15 min; performing mold reversing and sheet forming; s4, X fluorescence detection: putting the fuse piece sample into a spectrograph for detection, and giving a sample result; s5, sample detection is finished, whether a detection result between the parallel samples exceeds an allowable error range or not is judged, and an average result is calculated. The method solves the problem that X-fluorescence spectrum fuse piece analysis cannot be realized at present.
Owner:HUNAN VALIN XIANGTAN IRON & STEEL CO LTD

Metal-based ceramic bond diamond grinding wheel and preparation method thereof

The invention relates to the field of machine manufacturing, and particularly discloses a metal-based ceramic bond diamond grinding wheel and a preparation method thereof.The metal-based ceramic bond diamond grinding wheel comprises the following raw materials of a diamond grinding material, a reinforcing phase and a composite bond; wherein carbon fibers are selected as the reinforcing phase, the composite binding agent comprises a metal binding agent and the balance of ceramic binding agent, and the ceramic binding agent comprises the following raw materials of calcium fluoride, aluminum fluoride, lithium borate, boric acid and the balance of silicon dioxide; the preparation method comprises the following steps: S1, premixing the diamond grinding material and the reinforcing phase, then adding the composite binding agent, spraying a polyvinyl alcohol solution after mixing, and mixing and granulating to obtain granules; s2, the granules are loaded into a mold to be subjected to hot press molding to obtain a grinding wheel blank; and S3, sintering the grinding wheel blank at high temperature to obtain the metal-based ceramic bond diamond grinding wheel. The emery grinding wheel has the advantages that the abrasion resistance and the impact resistance of the grinding wheel are improved, and then the service life of the emery grinding wheel is prolonged.
Owner:ZHENGZHOU HONGTUO PRECISION TOOLS CO LTD

Lithium-based solid electrolyte, method for producing lithium-based solid electrolyte, modified positive electrode active material, modified negative electrode active material, all-solid-state secondary battery, electrode sheet for all-solid-state secondary battery, solid electrolyte sheet, and electrode for all-solid-state secondary battery

An object of the present invention is to provide a lithium-based solid electrolyte having excellent ion conductivity, a method for producing a lithium-based solid electrolyte, a modified positive electrode active material, a modified negative electrode active material, an all-solid-state secondary battery, an electrode sheet for an all-solid-state secondary battery, a solid electrolyte sheet, and an electrode for an all-solid-state secondary battery.The lithium-based solid electrolyte of the present invention contains amorphous lithium tetraborate, water, and a lithium salt, in which a content of the water is 45% by mass or less with respect to a total mass of the lithium-based solid electrolyte.
Owner:INSTITUTE OF SCIENCE TOKYO

Positive electrode slurry for lithium secondary battery and method for manufacturing positive electrode for lithium secondary battery using the same

The present invention relates to a positive electrode slurry for a lithium secondary battery, which includes a positive electrode active material including a lithium nickel-based oxide having a composition in which the nickel content of all metals other than lithium is 50 mol % or more and which is in the form of at least one of single particles or pseudo-single particles, which are secondary particles formed by agglomeration of 30 or less primary particles; a lithium borate-based compound; a binder; a conductive material; and a solvent; a positive electrode for a lithium secondary battery, which includes a positive electrode active material layer formed by coating at least one surface of a positive electrode current collector with the positive electrode slurry; a method for manufacturing the positive electrode; and a lithium secondary battery including the positive electrode.
Owner:LG ENERGY SOLUTION LTD

Battery

This battery (100) is provided with a positive electrode (23), a negative electrode (26), a separator (27), and an electrolyte solution (29), the positive electrode (23) containing, as a positive electrode active material, lithium oxide having an anti-fluorite crystal structure and in which a transition metal is solid-solved, and the electrolyte solution (29) containing two or more fluorine-containing lithium salts. The two or more fluorine-containing lithium salts may include a first lithium salt and a second lithium salt, and the first lithium salt may include at least one selected from the group consisting of fluorinated lithium borate and fluorinated lithium phosphate.
Owner:PANASONIC INTELLECTUAL PROPERTY MANAGEMENT CO LTD

Sulfide-based composite solid electrolyte membrane as well as full-dry preparation method and application thereof

The invention discloses a sulfide-based composite solid electrolyte membrane as well as a full-dry preparation method and application thereof, and the method comprises the following steps: (1) forming a lithium borate coating layer on the surface of a sulfide electrolyte by adopting an atomic layer deposition process to obtain coated powder; (2) adsorbing vinyl-containing ionic liquid steam by the coated powder to obtain adsorbed powder; (3) ball-milling and mixing the adsorbed powder, a fluorine-containing polymer binder and a photoinitiator to obtain mixed powder; and (4) maintaining the pressure of the mixed powder, and performing double-sided irradiation with ultraviolet light to obtain the sulfide-based composite solid electrolyte membrane. The sulfide electrolyte is subjected to surface coating through atomic layer deposition, and the full-dry preparation of the sulfide-based composite solid electrolyte membrane is realized on the premise of avoiding solvent contact in combination with gas phase adsorption polymerization and a hot pressing-ultraviolet synergistic curing process.
Owner:HUNAN YIHUA NEW ENERGY CO LTD +1

Positive electrode material and preparation method thereof, positive plate, secondary battery and electric device

The invention discloses a positive electrode material and a preparation method thereof, a positive plate, a secondary battery and a power utilization device, and relates to the technical field of batteries, the positive electrode material comprises a positive electrode active material and a first coating layer at least partially coating the surface of the positive electrode active material, and the first coating layer comprises titanium carbide and lithium borate; the positive electrode active material comprises at least one of ternary lithium positive electrode active materials. Lithium borate is a fast ion conductor, the first discharge capacity is increased, the impedance is reduced, titanium carbide has the advantages of oxidation resistance, good conductivity and the like, lithium ion reduction and electrolyte corrosion can be inhibited when the surface of the ternary lithium positive electrode active material is coated with the titanium carbide, the electrolyte is prevented from being oxidized to generate hydrofluoric acid and H3PO4, and corrosion of the positive electrode active material is reduced.
Owner:DONGFENG MOTOR GRP

Electrolyte suitable for lithium primary batteries

PendingUS20260011753A1Cell electrodesOrganic electrolyte cellsDifluorophosphateElectrolytic agent
The present disclosure relates to an electrolyte suitable for a lithium primary battery. In order to solve the problems of poor safety performance, high-rate discharge and poor discharge performance of electrolytes of the existing lithium primary batteries under a high-temperature condition, the electrolyte includes an electrolyte lithium salt, an additive, and an organic solvent, wherein the electrolyte lithium salt includes one or more of lithium trifluoromethanesulfonate, lithium bis(triflu-oromethanesulphonyl)imide, lithium difluorophosphate, and lithium difluoro(oxalato)borate; the additive includes one or more of (2-trimethylsilylethyl)2-cyanoacetate, diphenyldimethoxysilane, and citraconic anhydride; and the organic solvent comprises a carbon-ate solvent and a glycol ether solvent. A selective combination of the electrolyte lithium salt, the additive, and the solvent, normal-temperature discharge can be met when the electrolyte is applied to the lithium primary battery. The lithium primary battery can take into account the constant / high temperature performance, high-rate discharge performance and safety performance.
Owner:ZHANGJIAGANG GUOTAI HUARONG NEW CHEM MATERIALS CO LTD

A lithium tetraborate-zinc scintillation glass microcrystalline, its preparation method and application

The present invention discloses a lithium tetraborate-zinc tantalate scintillating glass-ceramics and its preparation method and application. The chemical composition expression of the borate scintillating glass-ceramics of the present invention is Li2B4O7-x at% Zn3Ta2O8, where 0 < x ≤ 20, and the proportion of the microcrystalline phase Zn3Ta2O8 doping in the overall borate scintillating glass-ceramics is 0 to 20 at%. The scintillating luminescent material in the present invention is synthesized by the high-temperature melting method, is stable in air, has a safe and simple process, and is easy to control. Under X-ray excitation, the light yield of the scintillating glass-ceramics of the present invention is 455 to 3198 ph. / MeV. Among them, the light yield of Li2B4O7-5 at% Zn3Ta2O8 is the highest, which is 35.5% of the BGO crystal, and it is a glass-ceramic scintillator with a high light yield that emits light by means of Zn3Ta2O8.
Owner:SHANGHAI INST OF TECH

Positive electrode active material and preparation method and application thereof

The invention belongs to the technical field of battery materials, and particularly relates to a positive electrode active material and a preparation method and application thereof. The invention provides a positive electrode active material which comprises an inner core and a coating layer coating the surface of the inner core, and the inner core comprises a niobium-tungsten co-doped ternary positive electrode material; the coating layer comprises lithium borate and lithium niobate. The prepared solid-state battery has excellent 0.1 C discharge specific capacity, 1C discharge specific capacity and cycle retention rate, and relatively low residual alkali.
Owner:SVOLT ENERGY TECHNOLOGY CO LTD

High-voltage stable electrolyte and application thereof in lithium ion battery

The invention relates to a high-voltage stable electrolyte and application thereof in a lithium ion battery. The electrolyte is synergistically formed by a solvent system and a double-salt system, wherein the solvent system is composed of aliphatic linear carbonate, a sulfone solvent and fluoro cyclic carbonate, and the double-salt system is composed of lithium hexafluorophosphate and lithium borate auxiliary salt. The combination can construct a unique lithium ion solvation sheath structure in an electrolyte, so that an interface reaction path can be accurately regulated and controlled, a film-forming additive is selectively guided to construct an interface film with high stability and flexibility on the surface of an electrode, and meanwhile, harmful decomposition of a solvent is inhibited. On the basis, the electrolyte achieves oxidation stability not lower than 5.2 V, is compatible with a high-voltage positive electrode and a high-capacity silicon-based negative electrode at the same time, effectively solves the technical problem that the high-voltage positive electrode and the high-capacity silicon-based negative electrode are difficult to be compatible, and shows excellent comprehensive cycle performance.
Owner:GUANGZHOU HUACHI SODIUM CHUANG ENERGY TECHNOLOGY CO LTD

Sterilizable lithium ion batteries

PendingUS20260188747A1Electrolytic agentImide
A battery that may be exposed to high temperatures such as when steam sterilizing that retains its capacity and power delivery is comprised of a cathode comprised of lithium metal phosphate, an anode comprised of lithium titanate, a separator comprising a material having a melt temperature of at least 150° C. and an electrolyte comprising a low boiling point solvent, a high boiling point solvent and a salt, the salt being comprised of a sulfur containing salt (e.g. lithium bis(trifluoromethanesulfonimide) and a lithium borate salt (e.g., lithium bis(oxalato)borate), by weight, wherein the sulfur containing salt is a majority of the salt present in the electrolyte. Desirably, the low boiling point solvent is comprised of a linear ester and the high boiling point solvent is comprised of a cyclic ester.
Owner:WILDCAT DISCOVERY TECHNOLOGIES INC +1

Method for synchronously detecting main components and trace elements of carbonate based on ICP (inductively coupled plasma)

The invention relates to the field of glass production, in particular to an ICP (inductively coupled plasma)-based carbonate main component and trace element synchronous detection method, which comprises the following steps: S1, sample pretreatment: grinding a sample, and melting and digesting with a lithium tetraborate-lithium metaborate mixed solvent to obtain mother liquor; s2, gradient dilution, wherein the concentration of microelements in the mother liquor is kept at 0.01-1 ppm; 1 ml of mother liquor is taken and diluted by 100-200 times, and sub-liquor is obtained; preparing at least five groups of concentration gradient test curve ranges by using a full-element standard solution; s3, ICP (Inductively Coupled Plasma) detection: detecting main components, adding a Y internal standard solution into a sub-solution, correcting the solution concentration and atomization efficiency fluctuation, selecting a vertical test, and detecting the concentrations of Ca and Mg; and trace element detection: selecting a horizontal test during the test, and detecting the concentrations of Li, Zr and Nb. According to the method, the problem of detection deviation caused by carbonate and silicate residues is avoided, the Y internal standard is added during detection to correct instrument fluctuation, the matrix interference problem of traditional ICP detection is solved, the detection efficiency and precision are improved, the cost is reduced, and the application range is wide.
Owner:QINGYUAN CSG NEW ENERGY SAVING MATERIALS CO LTD +1

Coating composition for enhancing a protective layer

The invention relates to a coating composition comprising a resin system comprising an organic film-forming resin and optionally a curing agent reactive to the organic film-forming resin, a lithium salt having a solubility in water at 20°C in the range of 0.01 to 120 g / L, selected from lithium carbonate, lithium phosphate, lithium hydrogen carbonate, lithium tetraborate and lithium oxalate, and a zinc salt of 2,5-dimercapto-1,3,4-thiadiazole (DMTD), wherein the zinc salt of DMTD is present as solid particles, the surface of which is at least partially covered by a film-forming polymer layer. The zinc salt of DMTD proves to have a synergistic effect on the enhancement of the barrier function of the protective layer formed in coating defects due to the presence of the lithium salt. Furthermore, the coating composition has an improved pot life.
Owner:AKZO NOBEL COATINGS INT BV

Low-dielectric-loss chip packaging glass substrate and preparation method thereof

The invention discloses a low-dielectric-loss chip packaging glass substrate and a preparation method thereof, and relates to the technical field of glass manufacturing. The chip packaging glass substrate is prepared from the following raw materials: silicon dioxide, boric oxide, zirconium dioxide, germanium dioxide, aluminum oxide, gadolinium oxide, a composite fluxing component and a low-loss dielectric functional component, the composite fluxing component is prepared from the following raw materials: magnesium fluoride, lithium metaborate and strontium fluoride; the low-loss dielectric functional component is prepared from the following raw materials: silicon nitride, boron nitride micro powder and a coupling agent solution. The preparation method of the chip packaging glass substrate comprises the following steps: preparing the composite fluxing component, preparing the low-loss dielectric functional component, forming the glass substrate, and preparing the chip packaging glass substrate. The prepared chip packaging glass substrate is low in dielectric loss and excellent in mechanical property.
Owner:LONGGUANGTIANXU SOLAR ENERGY ZHUCHENG

Negative pole piece and lithium secondary battery comprising same

The invention discloses a negative pole piece and a lithium secondary battery comprising the same, and belongs to the technical field of lithium batteries, the negative pole piece comprises a negative base pole piece and an artificial SEI layer located on the surface of the negative base pole piece; the artificial SEI layer comprises lithium fluoride, a boron-containing inorganic phase and a phosphorus-containing inorganic phase, the boron-containing inorganic phase is selected from lithium borate and the like, and the phosphorus-containing inorganic phase is selected from lithium phosphate and the like; the average thickness of the artificial SEI layer is 6 to 12 nm; the preparation method comprises the steps of slurry coating and densification treatment in an inert atmosphere, through the synergistic effect of high stability of LiF, high ionic conductivity of a phosphorus-containing phase and high mechanical toughness and film-forming property of a boron-containing phase, and in cooperation with a unique densification process, the problems that a traditional artificial film layer is prone to falling off, high in impedance and the like are effectively solved, and the preparation method is suitable for large-scale production. The interface side reaction and the material volume expansion are obviously inhibited, and the cycle life, the storage performance and the rate capability of the lithium secondary battery are greatly improved.
Owner:JIANGSU RELIANCE ENERGY TECHNOLOGY CO LTD

Construction and component detection method of mirabilite XRF (X-Ray Fluorescence) detection standard working curve

The invention relates to a mirabilite XRF detection standard working curve construction and component detection method. The method comprises the following steps: preparation of a standard sample, preparation of a standard detection product, drawing of a standard working curve, and detection, analysis and calculation. A sample is pre-melted for 20 minutes at the temperature of 450-500 DEG C before XRF detection, then is melted for 15-25 minutes at the temperature of 900-1050 DEG C, and is naturally cooled. Different from the prior art, according to the technical scheme, the sample is subjected to melting treatment, the mineral effect is eliminated, the particle size effect is overcome, and the measurement error is reduced; the preparation method comprises the following steps: adding lithium nitrate, anhydrous lithium tetraborate and lithium metaborate fluxing agents before melting, pre-melting at 450-500 DEG C for 20 minutes, and enabling the lithium nitrate, the lithium tetraborate and the lithium metaborate to act synergistically to fix the sulfur element in the anhydrous sodium sulfate and prevent the sulfur element from volatilizing, so that the accuracy of a detection result is improved.
Owner:FUJIAN RUIBO GLASS CO LTD

Composite positive electrode material, preparation method and proton battery

The invention aims to provide a composite positive electrode material, a preparation method and a proton battery. The lithium ion battery cathode material comprises the following components in percentage by mass: 70%-99.7% of a cathode active material and 0%-30% of a coating material, the positive electrode activity is a protonation product MnOOHx of MnO2, and the coating material is a proton conductor; wherein the coating layer comprises a first coating layer and a second coating layer, and the first coating layer comprises AgCl, amorphous carbon and calcium sulfate hydrate; the second coating layer comprises sulfate hydrate, hydrosulfate, dihydric phosphate, pyrophosphate, phosphate hydrate, a sulfate-aluminum oxide compound, a nitrate-aluminum oxide compound, imidazole proton salt, pyridine proton salt, sulfimide proton salt and chloro-lithium borate. The invention is applied to the technical field of electrochemistry.
Owner:TITANIUM NEW ENERGY TECHNOLOGY (GUANGDONG HENGQIN) CO LTD

Cathode active material coated with lithium borate doped lithium carbonate and sulfide all-solid-state battery comprising same

Disclosed are cathode active material (CAM) coated with a lithium carbonate doped with lithium borate with a formula of Li2+xC1−xBxO3 wherein 0<x<0.5 and a preparation method therefor. Also disclosed is a cathode layer comprising the coated CAM in the form of particles. In one embodiment, an all-solid-state battery comprising the cathode layer exhibits improved stability and cycling performance.
Owner:FACTORIAL INC

Lithium ion battery electrolyte and application thereof

The invention provides a lithium ion battery electrolyte and application thereof, the lithium ion battery electrolyte at least comprises fluorocarboxylate, a first additive and a second additive, the first additive comprises lithium difluoro (1, 2-dihydroxy ethane-1, 1, 2, 2-tetracyano) borate, and the second additive comprises tris (trimethylsilyl) phosphate. According to the lithium ion battery electrolyte and the application thereof provided by the invention, the high-voltage phase change of a positive electrode active material and the continuous oxygenolysis of the electrolyte under high voltage can be effectively inhibited, and the design of high-voltage-resistant and corrosion-resistant fast-charging electrolyte is realized.
Owner:ENVISION DYNAMICS TECH (JIANGSU) CO LTD +1