The invention discloses a method for rapidly and accurately determining multiple elements of limestone
powder based on a fuse piece method, and belongs to the technical field of material detection. A fuse piece scheme is designed aiming at the characteristics of fine particles, easy
moisture absorption and the like of limestone
powder instead of improving a general scheme of materials such as limestone,
dolomite and the like, key parameters are optimized, the flux ratio is set as follows: the ratio of
lithium tetraborate to
lithium metaborate is 67: 33, melting is divided into three processes of preheating, pre-oxidation and melting, the
melting temperature is effectively controlled to be 1060 DEG C, the time is 60 seconds, and the melting efficiency is greatly improved. The problem that limestone
powder is prone to excessive melting or uneven melting is solved, the matrix effect and the particle size effect are greatly reduced, it is verified that three limestone powder
standard samples with known components are selected for testing, the relative error between the result and the standard value is smaller than 1%, data meet the strict allowance requirement of the industry, and compared with an existing fuse piece method, the method has the
advantage that the cost is low. The detection adaptability to the limestone powder is remarkably improved, and the component detection requirements of mainstream limestone powder in the industry can be met.