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520 results about "Gel state" patented technology

Composition for controlling wellbore fluid and gas invasion and method for using same

The disclosure is directed to a composition for controlling wellbore fluid and gas invasion including methods for using said composition. The composition of the invention is a flowable slurry preferably comprising about 70 to 30% by weight of magnesium oxychloride and about 70 to 30% by weight of water. The composition is a flowable slurry at composition temperatures below about 60° C. and sets to form a substantially solid mass upon reaching a composition temperature of about 60-68° C. The phase transition is rapid, thereby limiting or avoiding formation of gel states which contribute to incomplete wellbore seals. The rapid set of the slurry further avoids invasive contamination of earthen formations surrounding the wellbore. The composition has a near-linear relationship between the time required for the phase transition to occur and the composition temperature at which the phase transition occurs. This advantageous property permits the composition set time to be accurately determined and modified as required through the addition of accelerators and inhibitors. The phase transition occurs predictably at high pressures typical of those encountered in wellbore operations. Additives may be included to modify the properties of the composition. The method includes use of the composition to control the loss of fluids and gases from the wellbore.
Owner:HALLIBURTON ENERGY SERVICES INC

Method for continuously preparing regenerated cellulose fibre

The invention discloses a method for continuously preparing regenerated cellulose fibers through the solvent method, comprising the following steps that: a cellulose raw material is dissolved into an ion liquid to prepare a spinning liquid; gel type regenerated cellulose fibers are obtained through spinning; and the regenerated cellulose fibers are obtained through cleaning, rear draft and drying, wherein, the ion liquid is selected from one or a plurality among the following ion liquids: a). an ion liquid with 1, 3-dialkyl imidazole as a cation and formiate radical, radical vinegar or propionate radical as an anion; and b). an ion liquid with 1-R1-3-R2- dialkyl imidazole as the cation and chlorine, bromine, iodine, formiate radical, radical vinegar, sulfate radical, nitrate radical, tetrafluoroborate radical, thiocyanate radical, hexafluorophosphate radical, p-toluenesulfonate radical or trifluoromethanesulfonic acid radical as the anion. The method has the advantages of wide technological range, mild temperature condition, adequate pressure, quick spinning speed and so on, can prepare the regenerated cellulose fibers with superior performance and complete specifications, and has low production cost, high production efficiency and wide application prospect.
Owner:INST OF CHEM CHINESE ACAD OF SCI +1

Porous complex gel-nanofiber oxygen permeation dressing and preparation method thereof

The invention discloses a porous complex gel-nanofiber oxygen permeation dressing and a preparation method thereof. The method comprises the following steps: obtaining a collagen nanofiber membrane by adopting a collagen solution by virtue of an electrostatic spinning method; performing chemical crosslinking on two natural and non-toxic macromolecule polysaccharides such as chitosan and alginic acid, and preparing complex gel; and preparing the porous sponge-nanofiber double-layer composite material in a freeze-drying mode, wherein the upper gel layer of the dressing is in a sponge state during drying and is in a gel state after moisture absorption. The biological wound dressing is prepared under the condition that any toxic chemical crosslinking agent is not added, the process is simple, and the safety is high. The prepared biological wound dressing disclosed by the invention has the characteristics of excellent oxygen permeation performance, water-absorbing quality, water permeability, moisture penetrability and high biocompatibility, a physiological wet environment of the wound surface can be maintained, wound healing and effective haemostasis are promoted, wound infection can be avoided, the recovery is accelerated, the wound surface can be effectively recovered, and the dressing is applied to multiple wound surfaces such as trauma, burns and ulceration.
Owner:FOURTH MILITARY MEDICAL UNIVERSITY

Nano-composite phase-changing material and preparation method

InactiveCN101429423AGood compatibilityWill not affect the mechanical propertiesHeat-exchange elementsPhase changeProcess complexity
The invention provides a nano composite phase change material and a method for preparing the same, and belongs to the field of material application. The nano composite phase change material comprises the following components in weight portion: 10 to 15 portions of phase change material, 5 to 60 portions of layer-shaped silicate powder, and 20 to 70 portions of deionized water; the phase change point of the phase change material is between 20 and 80 DEG C; the phase change material is heated up to be completely melted; the layer-shaped silicate powder is dispersed in water by a high shear mixed emulsion machine to prepare layer-shaped silicate gel state aqueous dispersion; and the melted phase change material is added to the layer-shaped silicate gel state aqueous dispersion and stirred at high speed by the high shear mixed emulsion machine to obtain the nano composite phase change material with oil-in-water structure. The nano composite phase change material can be directly added to building base materials such as concrete, gypsum, thereby greatly reducing process complexity and preparation cost; moreover, the composite phase change material also has the advantages of simple preparation, large heat storage, and better application prospect.
Owner:GUANGZHOU SUPER CHEM COATING CO LTDGUANGZHOU SUPER CHEM COATING CO LTD

Medical wound dressing with anti-bacterial nanometer particulate

InactiveCN101224310AGood water vapor transmission rateImprove water absorptionAbsorbent padsBandagesParticulatesWound dressing
The invention discloses a medical wound dressing which is loaded with antibiotic nanometer particles and which is in a spongy state when being dried and in a gel state after absorbing the moisture; the medical wound dressing is fixed in a spongy membrane prepared by chitosan and natural high molecular polymers and derivatives of the chitosan with the proportion of 10 to 19 percent of the spongy membrane and natural polymers by drug-loading nanometer particles; the drug-loading nanometer particles contains antibiotics with the particle size of 100nm to 1000nm, the encapsulation rate of 50 to 98 percent and the drug-loading rate of 5 to 60 percent and the weight percentage of 2 to 10 percent of the drug-loading nanometer particles in the wounding dressing. Combing the sustained and controlled release characteristic and the advantage of polysaccharide membrane, the invention has high water absorbability, air permeability, moisture permeability and good biological compatibility can keep the wound physiological moisture environment and promote the wound to recover and has hemostatic effect; at the same time, the invention has good slow release performance for the antibiotics, can prevent the infection of the wound and accelerate the recovery, thus being suitable for a plurality of wounds such as the traumas, burns and ulcers.
Owner:FOURTH MILITARY MEDICAL UNIVERSITY

Chitosan double-network quick response-type injectable hydrogel and preparation method thereof

The invention relates to chitosan double-network quick response-type injectable hydrogel and a preparation method thereof. The injectable hydrogel is prepared from chitosan or derivatives of the chitosan and sodium glycerophosphate serving as raw materials, and dialdehyde compounds or diepoxy compounds serving as crosslinking agents, wherein the mass ratio of the chitosan to the sodium glycerophosphate is 1:(0.5-10); the mass ratio of the crosslinking agents to the chitosan is (0.01-1):1. The method comprises the following steps: evenly mixing a hydrochloric acid aqueous solution of the chitosan with a sodium glycerophosphate solution in the environment at -1 to 5 DEG C, so as to obtain a solution of which the pH is 7-7.2, and evenly mixing the solution with a crosslinking solution at 35-37 DEG C. Transformation from a sol state to a gel state can be quickly finished under a specific condition, the process is irreversible, and the transition time is controllable. The chitosan double-network quick response-type injectable hydrogel has the advantages of simple reaction condition, short response time, good thermal stability of gel, high mechanical strength, good biocompatibility and the like. The chitosan double-network quick response-type injectable hydrogel is applied to the fields such as tissue filling and repairing, biological scaffolds, scar resistance and anti-adhesion, biogel, and quickly molding or three-dimensional printing materials and the like.
Owner:IMEIK TECH DEV CO LTD

Evaluation method and device for gel state or sol-gel state change of object

InactiveUS20050225752A1Carry-out easily and inexpensivelyEasily and inexpensively productionScattering properties measurementsOptically investigating flaws/contaminationEngineeringCcd camera
The object of the invention is to solve the problems regarding the quality control of processed products (including packaged products and intermediate products during production processes) by establishing a non-destructive and non-contact type method for the measurement of gel state of a material body and a change in sol-gel state of the material body, and thereby to provide a quick automatic inspection system by which 100% inspection can be carried out easily and inexpensively on the production line. The problem is solved by observing an image formation or speckle pattern of a light section formed on the surface or observing face of the material body, using a light scattering observation system in which a coherent light (e.g., from near infrared as a laser beam) is applied to a gel material body or a material which causes a change in sol-gel state, and its reflection or permeated scattered light is image-formed by a two-dimensional image recognizing means, and analyzing and numerically treating conditions of the image (e.g., average brightness, shape, contrast of speckles and the like) and thereby evaluating gel conditions of the material body (concentration, hardness, viscosity, coagulation deterioration, texture and the like qualities and the like), conditional (quality) change from sol to gel and conditional (quality) change from gel to sol. The invention was completed by realizing a practically inexpensive, 100% inspection-performable, quick, non-contact and non-destructive automatic measuring system which is illustratively equipped with a laser beam irradiation source, a CCD camera or the like two-dimensional image recognizing means and a transferring means, can grasp an image or speckle pattern of a light section image-forming on the material body surface or light intercepting device, as a two dimensional image, and can judge the qualities of said material body by analyzing the image data.
Owner:TAKAI TOFU & SOYMILK EQUIP +1

Water-base joint grouting glue for normal temperature road

InactiveCN101643636AAct as a seam sealStrong viscosity and permeabilityMonocarboxylic acid ester polymer adhesivesOther chemical processesWater basedAdhesive
The invention relates to water-base joint grouting glue for a normal temperature road, namely an environment-friendly joint grouting and joint sealing material having high viscosity, high cementing power and high adhesive property, which is formed by special processes of copolymerizing water, a water-base adhesive, bitumen and a dispersing agent, then modifying a macromolecular water-soluble resinand a rubber latex, and adding the auxiliary agents of a stabilizing agent, a thickening material and the like, and can be used for treating and sealing various types of cracks of bitumen and cementroad surfaces and joint seams of cement road surfaces and bridge surfaces. The joint grouting glue is in a gel state at normal temperature, can be stirred but cannot flow, thus the joint grouting gluecan enter joints directly without slotting and cannot infiltrate downwards so as to play a role in sealing the joints; and simultaneously the joint grouting glue is soluble in water; therefore, the joint grouting glue can be mixed with water to prepare strong-permeability joint grouting materials with any viscosities, and can be effectively poured into deep parts of the cracks of road surfaces without slotting. The joint grouting glue combines the advantages of slotting and non-slotting repairing methods, and simultaneously avoids the disadvantages of the two methods.
Owner:李志刚 +2

Polymer electrolyte, its preparation method and battery comprising the same

The invention provides a polymer electrolyte, its preparation method and a battery comprising the polymer electrolyte. The polymer electrolyte contains a stance phase and an ionic conductive phase adsorbed on the stance phase. The stance phase is an electrostatic spinning fiber film, and the ionic conductive phase includes a polymer able to undergo complexation with lithium ions and a lithium salt. The polymer able to undergo complexation with lithium ions contains an ether oxygen functional group. A bi-continuous phase composite electrolyte film characterized by high mechanical strength, good flexibility, high ionic conductivity, good thermal stability, high interface stability and good electrochemical stability can be obtained, and the preparation process is simple and is low in cost. The prepared material can be widely used in mobile phones, notebook computers and other mobile devices, as well as electric vehicles and other fields, and has strong practical significance to development of the battery industry. The polymer battery involved in the invention is different from liquid or gel state batteries, is free of plasticizer, does not cause leakage and other potential safety hazards, so that it can be used in high temperature environment, and does not have combustion, explosion and other hidden dangers.
Owner:BYD CO LTD

Thickening agent for printing and preparation method thereof

InactiveCN102965981AClear outlineHigh structural viscosityDyeing processSodium BentoniteGuar gum
The invention discloses a thickening agent for printing, which comprises the following components in parts by weight: 10-15 parts of etherified guar gum, 60-70 parts of sodium alginate, 30-50 parts of sodium carboxymethylcellulose, 20-30 parts of carboxymethyl starch, 12-20 parts of polyacrylic acid thickening agent blending stock, 10-20 parts of bentonites and 200-400 parts of water. The preparation method of the thickening agent comprises the following steps of: adding sodium alginate and sodium carboxymethylcellulose powder to water, and mechanically stirring till a solution is transparent and clear without a block; then adding the etherified guar gum, the carboxymethyl starch, the polyacrylic acid thickening agent blending stock and the bentonite, uniformly stirring, and standing to bulk the mixed solution so as to obtain the printing thickening agent. In the preparation process, with the bulking of the paste material, the sodium carboxymethylcellulose forms three-dimensional net structure among macromolecules of paste material or at the joints of molecular chain segments because of intermolecular attraction; moreover, besides a macromolecular chain hydration layer, a large amount of water is wrapped to form a gel state, so as to generate very high structural viscocity; therefore, a printing fabric has a clear outline.
Owner:ZHANGJIAGANG SHUNCHANG CHEM

Composition for controlling wellbore fluid and gas invasion and method for using same

InactiveUS20040040711A1Reduce hydrostatic pressureReadily cut through by a drill bitFluid removalFlushingLinear relationshipSlurry
The disclosure is directed to a composition for controlling wellbore fluid and gas invasion including methods for using said composition. The composition of the invention is a flowable slurry preferably comprising about 70 to 30% by weight of magnesium oxychloride and about 70 to 30% by weight of water. The composition is a flowable slurry at composition temperatures below about 60° C. and sets to form a substantially solid mass upon reaching a composition temperature of about 60-68° C. The phase transition is rapid, thereby limiting or avoiding formation of gel states which contribute to incomplete wellbore seals. The rapid set of the slurry further avoids invasive contamination of earthen formations surrounding the wellbore. The composition has a near-linear relationship between the time required for the phase transition to occur and the composition temperature at which the phase transition occurs. This advantageous property permits the composition set time to be accurately determined and modified as required through the addition of accelerators and inhibitors. The phase transition occurs predictably at high pressures typical of those encountered in wellbore operations. Additives may be included to modify the properties of the composition. The method includes use of the composition to control the loss of fluids and gases from the wellbore.
Owner:HALLIBURTON ENERGY SERVICES INC

Coating method for improving electrochemical property of high-nickel ternary nickel cobalt manganese anode material

The invention discloses a coating method for improving electrochemical properties of a high-nickel ternary nickel cobalt manganese anode material. The coating method comprises the following steps: dissolving a titanium source into a solvent so as to obtain a solution, dissolving a lithium source, and further adding citric acid so as to obtain a mixed solution; uniformly dispersing a high-nickel ternary nickel cobalt manganese anode material into a solvent, adding the mixed solution, uniformly mixing, and performing a hydrothermal reaction or a solvent thermal reaction so as to obtain a reaction solution; evaporating the reaction solution to a gel state, and drying so as to obtain an anode material mixture; calcining the anode material mixture, thereby obtaining the high-nickel ternary nickel cobalt manganese anode material with a lithium titanate coating layer. The coating method for improving the electrochemical properties of the high-nickel ternary nickel cobalt manganese anode material, which is disclosed by the invention, is simple in process, low in cost and good in repeatability, the obtained coating layer is high in crystallization degree, small in particle size and good inuniformity, and the charge and discharge specific capacity, the circulation property and the multiplying power of the high-nickel ternary nickel cobalt manganese anode material can be improved.
Owner:HEFEI GUOXUAN HIGH TECH POWER ENERGY

Thermal interface materials

A crosslinkable thermal interface material is produced by combining at least one rubber compound, at least one amine resin and at least one thermally conductive filler. This interface material takes on the form of a liquid or “soft gel”. The gel state is brought about through a crosslinking reaction between the at least one rubber compound composition and the at least one amine resin composition. Once the foundation composition that comprises at least one rubber compound, at least one amine resin, and at least one thermally conductive filler has been prepared, the composition must be compared to the needs of the electronic component, vendor, or electronic product to determine if a phase change material is needed to change some of the physical properties of the composition. A method for forming the crosslinkable thermal interface materials disclosed herein comprises a) providing at least one saturated rubber compound, b) providing at least one amine resin, c) crosslinking the at least one saturated rubber compound and the at least one amine resin to form a crosslinked rubber-resin mixture, d) adding at least one thermally conductive filler to the crosslinked rubber-resin mixture, and e) adding a wetting agent to the crosslinked rubber-resin mixture. This method can also further comprise adding at least one phase change material to the crosslinked rubber-resin mixture. The contemplated thermal interface material can be provided as a dispensable liquid paste, a gel, a tape, or a film. Applications of the contemplated thermal interface materials described herein comprise incorporating the materials into a layered material, an electronic component or a finished electronic product.
Owner:HONEYWELL INT INC

Method for planting and cultivating rhizoma gastrodiae

The invention belongs to agricultural cultivation, and particularly relates to a method for planting and cultivating rhizoma gastrodiae. The method comprises the steps that corn flour is boiled to paste and mixed with activated carbon powder so that a mixture of the corn paste and activated carbon can be produced; the mixture is laid on a flat plate; after the mixture is in a gel state, bacteria sticks and rhizoma gastrodiae seeds are tightly coiled and then planted. According to the method, the rhizoma gastrodiae seeds can tightly surround the bacteria sticks, so that the germination rate and the inoculation rate of the seeds are improved and finally, the yield of rhizoma gastrodiae of the method is more than two times as much as that of a traditional rhizoma gastrodiae sowing method. On one hand, the corn paste can serve as compost of the rhizoma gastrodiae, the activated carbon powder is added to the corn paste, and therefore the air permeability is guaranteed; on the other hand, when the rhizoma gastrodiae is planted, the phenomenon that the rhizoma gastrodiae is constrained or damaged is avoided along with the process that the corn paste is gradually dissolved, so that operation and later-period temperature and humidity management are facilitated and the operable sowing method is provided for rhizoma gastrodiae concentration seeding and efficient industrialized sowing. In addition, according to the method, special paper is not needed, the method is easy to achieve, and cost is saved.
Owner:CHONGQING FUXINYANG EDIBLE FUNGUS

Injection-type cartilage bionic matrix for regenerative repair of cartilage and method for using same

InactiveCN101934092AReduce dwell timeSolve the problem of excessive degradationProsthesisCell-Extracellular MatrixMedicine
The invention discloses an injection-type cartilage bionic matrix for the regenerative repair of cartilage and a method for using the same. The materials, of which the main components are the same as those of the extracellular matrix of the normal articular cartilage, are used as a raw material, and the raw materials undergo dissolution and pH adjustment to form the injection-type cartilage bionic matrix which is in a sol state at the low temperature and at a gel state at the body temperature; and by using the injection-type cartilage bionic matrix as a carrier, the injection-type cartilage bionic matrix is mixed with seed cells at the low temperature and then injected in cartilage deficiency parts, the injected materials undergo phase change by raising the temperature of the deficiency area to turn into the gel, so that the seed cells are fixed in the deficiency parts to conduct the regenerative repair function. The method is simple and easily implemented, the product is conveniently used, the operation injury is small, and the repair effect of the deficiency parts is good; the raw material has high biocompatibility and safety, all components undergo intermolecular bonding under the preparation conditions of the invention, so that the problem that the single bionic material is degraded too fast is solved; and the seed cells are directly mixed with the raw materials, and the culture in vitro is unnecessary so that the detention time in vitro of the seed cells are shortened, and the clinical application is safer.
Owner:THE FIRST AFFILIATED HOSPITAL OF THIRD MILITARY MEDICAL UNIVERSITY OF PLA

Method for preparing chitosan/cellulose composite material

The invention discloses a method for preparing a chitosan/cellulose composite material, and relates to a natural macromolecular composite material. The method for preparing the chitosan/cellulose composite material comprises the following steps of: dissolving cellulose in ionic liquid and heating to obtain solution A; dissolving chitosan into the ionic liquid and heating to obtain solution B; mixing the solution A and the solution B, levelling the mixed solution on a glass sheet, and immersing into a coagulating agent to obtain a membrane in a gel state; or spinning the mixed solution, immersing in the coagulating agent to obtain filaments in the gel state; and washing the membrane or the filaments, and drying to obtain a product. In the method, the cellulose and the chitosan are dissolved by the green solvent ionic liquid, the dissolution process depends on the powerful destruction capacity of hydrogen bonds, and an amino group of the chitosan is not protonized; and the composite material obtained by mixing the chitosan and the cellulose uniformly has excellent mechanical property, and the application of the composite material in fields of clinical medicine and the like can be expanded and promoted. The chitosan/cellulose composite material has the advantages of easy control of appearance, simple equipment requirement, simple and convenient operation, recyclability of the ionic liquid and environmental protection in the integral reaction process.
Owner:XIAMEN UNIV
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