The invention discloses a preparation process of
graphene oxide liquid phase coated
nano silicon. The preparation process comprises the following steps: S1, preparing modified
nano silicon; s2, preparing a
graphene oxide dispersion liquid; step S3: construction of a pre-
coating system; s4, carrying out dynamic
liquid phase coating reaction; step S5, post-treatment and purification;
nano silicon is modified before
coating, amino active groups are introduced to the surface of the nano
silicon through gamma-aminopropyltriethoxysilane and can interact with carboxyl and hydroxyl on the surface of
graphene oxide, the interfacial compatibility of the nano
silicon and the graphene oxide is remarkably improved, and the
binding force between a coating layer and the nano
silicon is enhanced; the falling of the coating layer in the charging and discharging process is effectively inhibited; according to the preparation method, the graphene oxide is prepared by adopting an improved
Hummers method, the dispersing agent is added, a stirring-
ultrasonic dispersion process is combined, and meanwhile, the temperature in the ultrasonic process is controlled, so that the
dispersity of the graphene oxide is effectively improved, agglomeration of the graphene oxide is avoided, and a foundation is laid for subsequent uniform coating.