908 results about "Battery electrolyte" patented technology

A non-woven battery separator and processes for forming the non-woven battery separator includes a fiber blend including cellulose fibers, microfibrillated fibers, and optionally polyester and / or aramid fibers. Also disclosed are batteries including the non-woven battery separator. During fabrication, the non-woven battery separator can be effectively dried at temperatures between 120°C and 180°C, which results in the fibers absorbing water when in use. Some battery electrolytes such as lithium hexafluorophosphate react with water to form hydrogen fluoride (HF), which can be corrosive and shorten battery lifecycles and affect performance. Absorbing water from the electrolyte increases the battery life cycle by reducing HF generation.

The invention belongs to the technical field of batteries, discloses a battery electrolyte solvent capable of adapting to a wide temperature range and preparation of a battery, and provides application of a mixed organic solvent as an energy storage battery electrolyte solvent, the mixed organic solvent is composed of tetrahydrofuran, 1, 3-dioxolame and 1, 1, 2, 2-tetrafluoroethyl-2, 2, 2-trifluoroethyl ether, and the 1, 1, 2, 2-tetrafluoroethyl-2, 2, 2-trifluoroethyl ether is composed of tetrahydrofuran, 1, 3-dioxolame and 1, 1, 2, 2-tetrafluoroethyl-2, 2, 2-trifluoroethyl ether. The volume percent content of the 1, 2, 2-trifluoroethyl ether is 10%-50%. The solvent composition of the energy storage battery electrolyte is improved, 1, 1, 2, 2-tetrafluoroethyl-2, 2, 2-trifluoroethyl ether is introduced into an ether organic solvent (namely tetrahydrofuran and 1, 3-dioxolame) to serve as a diluent, meanwhile, the volume percentage of the diluent is controlled, and the obtained electrolyte solvent formula can adapt to the wide temperature range of the full temperature interval of-130 DEG C to 60 DEG C, so that the energy storage battery electrolyte is suitable for being used as an energy storage battery electrolyte. And the problem of battery failure of the current energy storage battery under the extremely low-temperature and high-temperature conditions can be effectively solved.

The invention belongs to the technical field of magnesium ion batteries, and particularly relates to a magnesium ion battery electrolyte, a preparation method thereof and a magnesium ion battery. The invention provides a magnesium ion battery electrolyte. The magnesium ion battery electrolyte comprises a magnesium salt electrolyte, an amine organic solvent and an imidazole organic solvent. According to the magnesium ion electrolyte, the imidazole and amine organic solvents are used as the mixed cosolvent of the magnesium ion electrolyte, so that the electrolyte magnesium salt can be effectively dissolved, and the problems of decomposition and passivation of the electrolyte solvent and corrosion of a magnesium metal negative electrode can be effectively solved; the amine and imidazole co-soluble magnesium ion electrolyte provided by the invention can realize reversible deposition and dissolution of a magnesium metal negative electrode under the condition of a wide temperature range of-30 to 80 DEG C, and can be applied to a rechargeable magnesium battery.

Systems and apparatus may carry out analysis of battery physical phenomena, and characterize batteries based on phenomena occurring in particular time and / or frequency domains. These systems may be additionally responsible for charging and / or monitoring a rechargeable battery. Examples of battery physical phenomena include mass transport (e.g., diffusion and / or migration) in battery electrolytes, mass transport in battery electrodes, and reactions on battery electrodes.

Systems and apparatus may carry out analysis of battery physical phenomena, and characterize batteries based on phenomena occurring in particular time and / or frequency domains. These systems may be additionally responsible for charging and / or monitoring a rechargeable battery. Examples of battery physical phenomena include mass transport (e.g., diffusion and / or migration) in battery electrolytes, mass transport in battery electrodes, and reactions on battery electrodes.

The invention relates to a lithium iron phosphate battery electrolyte self-circulation regulation and control method and system, and relates to the technical field of battery regulation and control, and the method comprises the steps: constructing an SEI state recognition model and an SEI loss prediction plug-in on the basis of SEI film loss historical data of similar lithium iron phosphate batteries in a cloud server, and deploying the recognition model to a battery management unit; collecting a first cell characteristic data sequence through a sensor according to a preset frequency, inputting the first cell characteristic data sequence into a recognition model of the battery management unit, and outputting an SEI state recognition result; if the state is a loss state, collecting a second battery cell characteristic data sequence, uploading the second battery cell characteristic data sequence to the cloud server, calling a prediction plug-in, and outputting a prediction loss type and a degradation coefficient; and according to an optimized battery charging repair strategy, outputting an adaptive scheme and controlling battery charging to finish active repair of the SEI film. The method solves the problems that the traditional method is difficult to monitor the loss in the dynamic evolution of the SEI film in real time, so that the repairing effect is poor, and the service life, safety and efficiency of the battery are influenced.

The invention provides an intelligent response nano-film and application thereof in waste lead-acid storage battery electrolyte recycling, and relates to the technical field of waste lead-acid storage battery electrolyte recycling, the intelligent response nano-film breaks through performance limitation of an existing film system through a specific intelligent material structure, and when heavy metal ions such as Pb < 2 + >, Fe < 3 + > and Cu < 2 + > enter the film, the intelligent response nano-film can be recycled, and the service life of the intelligent response nano-film is prolonged. The metal ligands are combined with metal ions to cause local shrinkage or closing of pore channels, so that the active defense and intelligent blocking effects of blocking heavy metals are achieved; and when SO4 < 2-> and H < + > pass through the channel, membrane pore channels are kept in an open state, so that rapid acid flux (namely the amount of substance passing through the membrane layer in unit time) of sulfuric acid is realized. The intelligent response nano film has a programmable aperture of a polymer liquid crystal network and an intelligent response valve mechanism of metal, and selective separation of heavy metal and sulfuric acid is realized by stimulating reversible adjustment of an induced film structure.

The invention belongs to the technical field of lithium / sodium batteries, and particularly relates to a method for pre-embedding lithium / sodium into a battery. The preparation method comprises the following steps: firstly, preparing a lithium / sodium pre-embedded material of the lithium / sodium battery, namely putting a sodium salt of the material into an organic solvent, dropwise adding acid, stirring for reaction, extracting and drying, and evaporating the solvent to dryness; placing the product in deionized water, adding lithium salt, stirring for reaction, and evaporating the solvent to dryness; recrystallizing the solid by using ethyl acetate and dichloromethane; and drying the obtained solid powder to obtain a final material. Dissolving the prepared lithium / sodium pre-intercalation material in a battery electrolyte to realize lithium / sodium pre-intercalation of the battery; the sodium salt of the material takes organic sodium sulfinate as a skeleton, and side groups are substituted with different alkyl groups or aryl groups; the prepared lithium / sodium pre-embedded material is high in specific capacity, good in compatibility with a battery system and good in material stability; lithium / sodium pre-embedding is carried out on the battery through an electrolyte adding method, the lithium / sodium pre-embedding process is safe and convenient, the process is simple, the cost is low, and large-scale production can be realized.

The invention relates to the technical field of solid-state batteries, and discloses an optimized preparation method of a solid-state battery electrolyte, a composition comprises a lithium source, a lanthanum source and a zirconium source, and the molar ratio of lithium to lanthanum to zirconium is (7.0-8.0): 3.0: 2.0; the use amount of the photoacid generator accounts for 0.5-5.0 mol% of the total molar weight of the metal ions; and an organic solvent. The method comprises the following steps: S1, placing a substrate in a high-pressure reaction kettle, and injecting the precursor composition in a supercritical carbon dioxide (scCO2) environment; s2, irradiating the surface of the substrate with ultraviolet rays, performing photolysis on the photoacid generator to generate acid, and catalyzing the metal precursor to be decomposed and deposited into an amorphous film; and S3, taking out the substrate after pressure relief, and carrying out low-temperature heat treatment at 400-700 DEG C to obtain the solid electrolyte film. Through combination of photochemical deposition and a supercritical fluid technology, the problem of decomposition of a positive electrode material caused by high temperature in a traditional process is solved.

The invention discloses a battery electrolyte and a preparation method thereof, an aqueous zinc-iodine battery and terminal equipment. The battery electrolyte comprises an additive, an electrolyte and a solvent, the additive contains an amino functional group, and the concentration of the additive is 0.1 g / L-0. 5 g / L. In addition, the additive can also utilize a nitrogen-containing functional group to reduce the shuttle effect of polyiodide and prevent the loss of an iodine positive active material, so that the electrode of the zinc ion battery is protected, and the cycle life of the zinc ion battery is remarkably prolonged (the capacity is about 20mAh / g higher than that of an electrolyte without L-tyrosine).

The invention provides a supercritical lithium metal battery electrolyte with electric field adaptability and application, and belongs to the technical field of lithium metal batteries. Comprising a lithium salt, a main solvent and a diluent, has the characteristic of adaptively stabilizing a lithium metal negative electrode under the action of an electric field, and is a supercritical state electrolyte obtained by dissolving the lithium salt in the main solvent to form a solution with the concentration being greater than or equal to 5 mol / L and diluting the solution with the diluent; the main solvent is at least one of chain ester, chain ether and siloxane, the diluent is hydrofluoroether, and the volume ratio of the main solvent to the diluent is 1: (0.5-20). The lithium metal negative electrode shows stable self-adaptive capacity under the action of an electric field, and formation of lithium dendrites is inhibited by promoting decomposition of anions at the negative electrode to form SEI rich in inorganic components, so that long-time stable circulation of a high-voltage lithium metal battery is realized.

The invention discloses an organic long-chain zinc salt for a zinc secondary battery electrolyte and a preparation method and application thereof. The organic long-chain zinc salt comprises a long-chain group, an acidic group and zinc ions, the long-chain group comprises at least one of substituted or unsubstituted C8-16 alkyl groups, and the acidic group comprises at least one of a sulfonic acid group, a phosphoric acid group and a sulfuric acid group. The organic long-chain zinc salt serving as an electrolyte salt of the zinc secondary battery can be adsorbed on the surface of zinc to form a protective layer, so that the cycle life and the capacity retention ratio of the zinc secondary battery are effectively improved.

The invention provides a solid-state battery electrolyte material, a preparation method thereof and a solid-state lithium ion battery. The preparation method comprises the following steps: S1, carrying out first reaction on a first raw material comprising an organic ligand, zircon salt, a first acid solution and a first organic solvent to obtain a metal organic framework material; and step S2, carrying out a second reaction on a second raw material comprising dimethyl 2, 6-dipicolinate and a metal organic framework material to obtain the solid-state battery electrolyte material. The solid-state battery electrolyte material obtained by adopting the preparation method disclosed by the invention has good mechanical properties, a wider electrochemical window and higher ionic conductivity, so that the initial efficiency, the capacity and the cycle performance of the battery are improved, and the internal resistance of the battery is reduced at the same time.

The invention discloses a lead-acid storage battery electrolyte density measuring device, and belongs to the technical field of battery measurement, the lead-acid storage battery electrolyte density measuring device comprises a detection mechanism, the detection mechanism comprises a connecting column and a tuning fork mechanism, the tuning fork mechanism comprises a tuning fork base and a tuning fork sensor, and the tuning fork mechanism is sleeved with a double-layer isolation mechanism; the double-layer isolation mechanism comprises an inner cover mechanism and a microporous outer cover mechanism, a microporous material of the outer cover mechanism enables the electrolyte to penetrate through the outer cover mechanism and block bubbles, and the inner cover mechanism enables the electrolyte to turn and flow many times to make contact with the tuning fork sensor through an inner cover first channel and an outer cover second channel which are arranged in a staggered mode. The tuning fork mechanism is sleeved with the double-layer isolation mechanism, the outer cover mechanism adopts a microporous material to achieve electrolyte permeation and bubble blocking, the inner cover forces electrolyte to flow circuitously through the staggered channel design, the double structures cooperatively eliminate bubble attachment and inhibit turbulence interference, and it is ensured that frequency signals of the tuning fork sensor are stable; and the measurement precision and sensitivity are obviously improved.

The invention provides an aqueous zinc ion battery electrolyte, a preparation method thereof and a zinc ion battery, and belongs to the technical field of aqueous zinc ion batteries. The aqueous zinc ion battery electrolyte comprises an additive, an inorganic zinc salt and a solvent, the additive comprises at least one of trimethylamine substituted by 1-3 substituent groups, benzene and C3-C10 straight-chain alkane, and the substituent groups comprise phosphonic acid groups or phosphinic acid groups; the solvent comprises a sodium chloride aqueous solution. By adopting the additive with a specific structure and the solvent containing the sodium chloride aqueous solution, the cycle performance of the zinc negative electrode in the water-based zinc ion battery can be remarkably improved, and the service life of the water-based zinc ion battery is prolonged.

According to the parking battery energy distribution optimization method and system, the initial flowing direction of battery electrolyte is calculated by monitoring the three-axis acceleration and angular speed of a vehicle in real time, and electrolyte concentration gradient distribution is simulated and predicted in combination with fluid mechanics. And when the concentration gradient exceeds a threshold value, dynamically dividing an electrode area and optimizing an activation proportion, synchronously calculating current density distribution and an electrochemical reaction rate, and deducing the real-time output power of the battery by using an equivalent circuit model. By comparing real-time power requirements of electric equipment, a pulse width modulation technology is adopted to generate an initial energy distribution scheme, switching frequency distribution of an electrode activation area is finely adjusted based on current density requirements, and finally dynamic regulation and control of the battery management system on electric energy output are achieved. According to the method, the problem of output power fluctuation caused by non-uniform electrolyte distribution due to vehicle shaking in a parking state is effectively solved, and the energy distribution efficiency and the power supply stability of the battery with the special-shaped structure under a complex working condition are greatly improved.

The invention relates to the technical field of lithium-oxygen batteries, in particular to a lithium-oxygen battery electrolyte and a preparation method thereof. The lithium-oxygen battery electrolyte comprises an organic solvent, an electrolyte lithium salt and a multifunctional additive, the multifunctional additive is prepared by introducing an MOF material, a boron nitride nanosheet and an ionic liquid, coating of the boron nitride nanosheet and introduction of the ionic liquid improve the stability of the multifunctional additive, and the stability of the multifunctional additive is improved. The 1-ethyl-1-methylpyrrolidinium bis (trifluoromethylsulfonyl) imine can effectively play a role for a long time, efficiently captures and stabilizes oxygen free radicals generated in the charging and discharging process, reduces the oxidative degradation of the oxygen free radicals to a positive electrode binder, prolongs the cycle life of the battery, improves the overall battery performance, and improves the battery performance. Powerful support is provided for commercial application of the lithium-oxygen battery.

The invention relates to the technical field of aqueous zinc ion batteries, in particular to an aqueous zinc ion battery electrolyte as well as a preparation method and application thereof. The invention provides an aqueous zinc ion battery electrolyte. The aqueous zinc ion battery electrolyte comprises soluble zinc salt and fulvic acid, and the concentration of the fulvic acid in the electrolyte is 0.01-50 g / L; wherein rich oxygen-containing functional groups contained in fulvic acid molecules can serve as strong coordination sites to be combined with Zn < 2 + > to generate coordination, so that the migration rate of zinc ions is effectively reduced, and uniform deposition of the zinc ions on the surface of the negative electrode is promoted; meanwhile, direct contact between water molecules and the zinc negative electrode can be reduced by utilizing a molecular interface layer formed by fulvic acid molecules on the surface of the zinc negative electrode, so that water-induced side reaction can be relieved. And the cycle stability of the battery is improved through the effects. In addition, the fulvic acid is wide in source, low in cost and environment-friendly, the production cost of the water-based zinc ion battery is reduced, and large-scale application of the water-based zinc ion battery is promoted.

The invention discloses a wide-voltage wide-temperature-range sodium-ion battery electrolyte and a preparation method and application thereof, and belongs to the technical field of sodium-ion battery electrolytes.The wide-voltage wide-temperature-range sodium-ion battery electrolyte comprises sodium salt, an organic solvent and an additive, the organic solvent is selected from one or more of ethylene carbonate, propylene carbonate, ethyl methyl carbonate, dimethyl carbonate, diethyl carbonate, ethylene glycol dimethyl ether, diethylene glycol dimethyl ether and triethylene glycol dimethyl ether, and the additive is selected from one or more of fluoroethylene carbonate, allyl-1, 3-propane sultone, 1, 3-propylene sultone, 1, 3-propylene sultone and 1, 3-propylene sultone. The additive is one or more of 1, 3-propyl sultone, methylene methane disulfonate, ethylene sulfate, trifluoromethanesulfonic anhydride, pentaerythritol bicyclic sulfate, tri (trimethylsilane) phosphate, tri (trimethylsilane) phosphite, tri (trimethylsilane) borate, acesulfame sodium and aluminum trifluoromethanesulfonate, and the additive is one or more of 2, 3-propylene sultone, methylene methane disulfonate, ethylene sulfate, trifluoromethanesulfonic anhydride, pentaerythritol dicyclosulfate, tri (trimethylsilane) phosphate, tri (trimethylsilane) phosphite, tri (trimethylsilane) borate, tri (trimethylsilane) phosphate and tri (trimethylsilane) borate. The electrolyte provided by the invention not only keeps high coulombic efficiency at low temperature, but also has good cycle stability at high temperature.

The invention relates to the field of lithium battery polyether-based electrolyte. The invention provides a polyether-based lithium battery electrolyte and a preparation method thereof. According to the preparation method, polyethylene oxide and bis (fluorosulfonyl) lithium imide are taken as main bodies, a dynamic polyether prepolymer and polyether shell layer aluminum oxide nano powder are combined, and the imine bond conversion rate, the median particle size D50, the content of an organic shell layer and the unit molar ratio of lithium salt to ethylene oxide are controlled; the method comprises the following steps: preparing slurry by using an anhydrous acetonitrile system, casting, drying in stages and post-curing to obtain a film-shaped or coating-shaped electrolyte, so that the water content is not higher than 500mg / kg, the total residual organic solvent content is not higher than 1000mg / kg, the viscosity and the thickness are controllable, and the residual epoxy value is promoted to be reduced; the problem that the viscosity and the purity are difficult to consider in film casting is solved; the method is suitable for large-scale preparation of the lithium battery electrolyte membrane.

The invention relates to the technical field of zinc-iodine battery electrolyte, in particular to aqueous zinc-iodine electrolyte as well as a preparation method and application thereof. The aqueous zinc-iodine battery electrolyte contains an additive and a zinc salt, the molar concentration of the additive is 0.15 M to 0.8 M, and the additive is selected from one or more of triethylamine hydrochloride, 1-butyl-1-methylpyrrolidine chloride, 1, 3-dimethylimidazole chloride, pyridine hydrochloride, aniline hydrochloride, guanidine hydrochloride and 1-ethyl-3-methylimidazole chloride. The method can directionally regulate and control zinc negative electrode deposition and iodine positive electrode reaction kinetics, realizes four-electron reversible conversion, promotes uniform deposition of zinc ions and inhibits side reactions during charging, inhibits multi-iodide shuttle and I < + > hydrolysis during discharging, and has wide application prospects in the zinc-iodine battery electrolyte industry.

The invention provides a lithium metal battery electrolyte, a lithium metal battery and a preparation method. The electrolyte comprises an electrolyte lithium salt, an organic solvent and a functional additive, the functional additive comprises phosphorus oxychloride, and the concentration of the phosphorus oxychloride in the electrolyte is 0.1-2%. And assembling a lithium metal negative electrode, a positive electrode, a diaphragm and the electrolyte in an inert atmosphere, and standing for a certain time after assembling to obtain the lithium metal battery. Phosphorus oxychloride is added into the electrolyte to serve as a functional additive, and a Li3PO4-LiCl composite inorganic interface layer is formed on the surface of a lithium metal negative electrode, so that the mechanical strength and the ionic conductivity of the lithium metal negative electrode are improved.

The invention discloses a universal water-based zinc-based battery electrolyte additive and a battery preparation method, and particularly relates to the technical field of water-based zinc-based secondary batteries, the universal water-based zinc-based battery electrolyte additive is a nitroimidazole organic matter, contains an imidazole ring and a nitryl group, and is characterized in that the nitroimidazole organic matter is a nitroimidazole organic matter; the high-electronegativity zinc ion electrode has one or more functional groups of methyl, hydroxyl, carboxyl, carbonyl, imino, sulfo and halogen, nitryl can be reduced to form imino or imidazole is subjected to ring opening to form an azo compound in the electrochemical process, and high-electronegativity sites can be adsorbed on the surface of the electrode or interact with zinc ions. Nitrogen sites with high electronegativity can be adsorbed to the surface of the zinc negative electrode, contact between water and the zinc negative electrode is isolated, a hydrogen evolution reaction and a corrosion side reaction are limited, the electrochemical environment of an electrode interface is stabilized, and the electrolyte additive can promote 3D diffusion of zinc ions, reduce the critical nucleation size of zinc deposition and inhibit growth of zinc dendrites.

The invention belongs to the technical field of battery electrolyte, and particularly relates to flame-retardant cyclic phosphamide eutectic electrolyte as well as a preparation method and application thereof. According to the invention, through reasonable molecular design, the flame-retardant cyclic phosphamide eutectic electrolyte is obtained. Through the design of the annular structure, a film is formed on the positive and negative electrode interface of the electrode in the battery operation process, so that the stability of the battery is improved. Phosphamide groups are introduced into the cyclic structure, hydroxyl radicals generated in the battery operation process are captured through phosphorus-oxygen bonds, and the chain reaction of combustion is blocked. Meanwhile, different designs of amino groups on phosphamide can achieve a self-cleaning effect, hydrofluoric acid and water generated in a battery circulation process are removed, and the battery is protected from electrode structure collapse caused by the hydrofluoric acid and the water in an operation process. The safety performance of the lithium battery in the cycle process is obviously improved, and the development of the lithium battery with high safety and stable operation is effectively promoted. The preparation process is simple, safe to operate, high in purity and suitable for industrialization.

The invention discloses a sodium ion battery electrolyte and a sodium ion battery, the preparation raw materials of the electrolyte comprise an electrolyte, an organic solvent and a composite additive, the preparation raw materials of the electrolyte comprise a sodium salt and modified graphite, the preparation raw materials of the modified graphite comprise graphite, dopamine hydrochloride, polyethyleneimine, Sb2O3 and BiCl3, the composite additive is prepared from trimethylsilyl trifluoromethanesulfonate, N-methyl pyrrolidone, vinylene carbonate and nano silicon dioxide. Through synergistic compounding, a high-stability three-dimensional ionic conduction network is constructed, so that the electrolyte has a wide electrochemical window and high ionic conductivity.

The invention discloses a fluorine ion stabilizer, a lithium carbon fluoride battery electrolyte and a lithium carbon fluoride battery, and belongs to the field of lithium batteries. The fluorine ion stabilizer is prepared from a 1-ethyl-3-methylimidazole cation compound and an alcohol compound; the alcohol compound is selected from at least one of ethylene glycol and polyethylene glycol; the molecular weight of the polyethylene glycol is 62 to 3000. The binding energy of the fluorine ion stabilizer and fluorine ions is low, a solvation product can be stabilized, the final discharge product of the Li / CFx battery is changed, and finally the purpose of reducing the heat produced in the discharge process of the battery is achieved.

This application provides a lithium battery and a power vehicle. The lithium battery combines lithium transition metal oxide with LiFe... 1‑a Mn a PO4 material is used as the positive electrode active material, and LiFe is added. 1‑a Mn a The mass ratio of PO4 material is related to the content of vinylene carbonate in the battery electrolyte, the discharge capacity and DC internal resistance of the battery at 0.33C discharge at 25℃, and the content of Fe dissolved into the negative electrode material after high-temperature cycling. These factors are then made to meet certain conditions to ensure that the battery can achieve both good low-temperature rate performance at 0℃ and high-temperature cycling performance.

The invention relates to a wide-temperature-range high-voltage electrolyte, a preparation method and application of a lithium metal battery, and relates to the technical field of lithium metal batteries. The electrolyte comprises a lithium salt, a solvent and an additive, the solvent is a nitrile-ester blending solvent formed by mixing nitrile and ester, the viscosity of the electrolyte can be reduced, the conductivity of the electrolyte can be improved, meanwhile, a solvation structure can be regulated and controlled through the low freezing point of the nitrile solvent, and a stable passive film can be constructed through the ester solvent, so that the stability of an electrolyte / electrode interface is improved; and meanwhile, the stability of the interface is further promoted by introducing the additive. The electrolyte provided by the invention can be applied to lithium metal battery electrolyte, improves the safety and the cycle life of the battery, and is expected to be applied to energy supplies of electronic equipment such as intelligent war and rescue equipment, combat weapons, aerospace, new energy automobiles, AI auxiliary diagnosis equipment and the like in a wide temperature range (-20 to 60 DEG C).

The invention discloses a preparation method of bis (trifluoromethylsulfonyl) imide salt, and belongs to the technical field of metal ion battery electrolyte materials, and the preparation method comprises the following steps: mixing trifluoromethylsulfonyl fluoride and organic amine alkali to obtain a mixed solution A; dropwise adding the mixed solution A into a reaction kettle filled with ammonia gas, and completely reacting to generate bis (trifluoromethanesulfonyl) imide quaternary ammonium salt; carrying out reduced pressure distillation on the reaction product to obtain pure bis (trifluoromethanesulfonyl) imide quaternary ammonium salt; the preparation method comprises the following steps: mixing bis (trifluoromethylsulfonyl) imide triethylamine salt and metal salt according to a molar ratio of 1: (1-3), and completely reacting in an organic solvent to generate bis (trifluoromethylsulfonyl) imide salt; and filtering the reaction liquid, and carrying out reduced pressure distillation to obtain the final product bis (trifluoromethylsulfonyl) imide salt. The preparation method provided by the invention has the characteristics of simple process, high yield and high product purity, and solves the problems of complex process, low yield, low product purity and the like in the existing preparation method.

The invention relates to a flow battery electrolyte and an application thereof. The flow battery electrolyte comprises vanadium ions, a supporting electrolyte and an additive, the additive is selected from one, two or more of ammonium sulfate, ammonium phosphate, potassium phosphate, sodium metaphosphate, diammonium hydrogen phosphate and hydrogen peroxide. According to the vanadium battery electrolyte provided by one embodiment of the invention, the specific additive is added, so that vanadium ions can be in a liquid state or a microemulsion state, separation or precipitation of the vanadium ions is prevented, and the efficiency of the battery is remarkably improved.