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67 results about "Ethyl propionate" patented technology

Ethyl propionate is a compound with formula C₂H₅(C₂H₅COO). It is the ethyl ester of propionic acid. It has a pineapple-like odor. Some fruits such as kiwis and strawberries contain ethyl propionate in small amounts.

Electrolyte, electrochemical device, and electronic device

The invention provides an electrolyte, an electrochemical device and an electronic device, and belongs to the technical field of energy storage. Based on the mass of the electrolyte, the electrolyte comprises ethylene carbonate with the mass content of A%, methyl propyl carbonate with the mass content of B%, diethyl carbonate with the mass content of C%, ethyl propionate with the mass content of D% and propyl propionate with the mass content of E%; wherein 5 < = A < = 20, 10 < = B < = 20, and 0.1 < = A / (B + C + D + E) < = 0.5. By controlling the components and the mass content of the electrolyte, the components are matched with one another, so that the high-temperature cycle capacity retention ratio of the battery can be improved, the increase of the thickness of the battery in a high-temperature and high-humidity storage environment is controlled, the service life of the battery is prolonged, and the use safety of the battery is improved.
Owner:NINGDE AMPEREX TECHNOLOGY LTD

Production and processing device of ethyl dicyanopropionate and processing method thereof

The invention discloses a production and processing device of ethyl dicyanopropionate and a processing method thereof, relates to the technical field of chemical production, and aims to solve the technical problem that a traditional stirring method cannot realize overall uniform mixing of mixed liquid according to density and viscosity, and the production and processing device comprises a tank body, a stirring mechanism, a turnover assembly and a defoaming unit. According to the stirring mechanism, the rubber rod is bent under the action of centrifugal force, the stirring area is enlarged, the mixing efficiency above the stirring cavity is improved, and different working conditions are adapted; the overturning assembly pushes the middle mixed liquid to uprush by utilizing a rubber barrel which is pressed to be concave inwards, so that segmented stirring is realized, and the mixing effect is enhanced by vibration force generated by contact between a rubber rod and a concave part; the defoaming unit enables foams to flow into a bearing ring to be defoamed by means of centrifugal force of mixed liquid, and a fixing cylinder, a spring and an extrusion block guarantee defoaming stability; the whole device is compact in structure, components are coordinated, operation is easy and convenient, and the standard processing method assists in improving the production quality and efficiency of ethyl dicyanopropionate.
Owner:WENZHOU JIALI CHEM

Electrolyte for ternary positive electrode secondary battery and secondary battery

The invention provides an electrolyte for a ternary positive electrode secondary battery, the electrolyte is used for a secondary battery with a positive electrode active material being LiNixCoyMnzO2, x, y and z respectively represent molar fractions of nickel, cobalt and manganese, x + y + z = 1, and the electrolyte comprises carbonic ester, ethyl propionate, a lithium salt, an organic silicon additive and a lithium acesulfamide additive. According to the electrolyte and the secondary battery, the high-voltage performance can be improved.
Owner:ANHUI JINHE SYNTHETIC MATERIAL RESEARCH INSTITUTE CO LTD

Low-temperature electrolyte for laminated soft-package lithium ion battery, lithium ion battery and preparation method of lithium ion battery

The invention discloses a low-temperature electrolyte for a laminated soft-package lithium ion battery, the lithium ion battery and a preparation method of the lithium ion battery. Comprising the following components: 4%-6% of propylene carbonate, 9%-11% of diethyl carbonate, 30%-32% of methyl ethyl carbonate, 24%-26% of ethylene carbonate, 9%-11% of ethyl propionate, 14%-16% of electrolyte salt and 3.6%-4.0% of an additive, according to the low-temperature electrolyte and the lithium ion battery, the solvent and the additive of the electrolyte are optimally combined, so that the obtained electrolyte has the characteristics of high conductivity and low impedance at low temperature, the low-temperature charge-discharge performance of the lithium ion battery can be remarkably improved, in addition, the obtained low-temperature electrolyte and the lithium ion battery have wide application prospects, and the application prospect is wide. And the method is especially suitable for the field with high low-temperature performance requirements.
Owner:GPCOMM TECH LTD

Production method of quizalofop-p-ethyl

The invention relates to a production method of quizalofop-p-ethyl, which comprises the following steps: reacting 2-(4-hydroxyphenoxy) propionic acid with absolute ethyl alcohol to obtain ethyl 2-(4-hydroxyphenoxy) propionate, and replacing the original process of reacting p-toluenesulfonyl chloride with L-ethyl lactate to obtain an intermediate, namely ethyl p-toluenesulfonyl lactate, with a process of reacting 2-(4-hydroxyphenoxy) propionic acid with absolute ethyl alcohol to obtain ethyl 2-(4-hydroxyphenoxy) propionate; meanwhile, in the post-treatment method, centrifugal separation replaces plate-and-frame pressure filtration, closed-circuit flash drying replaces original rake drying, racemization of quizalofop-p-ethyl is effectively avoided, the optical purity and yield of quizalofop-p-ethyl are improved, and the environmental protection benefits of the process are improved. Experiments show that the optical purity of the quizalofop-p-ethyl produced by the method provided by the invention is 99% or above, the yield is 98% or above, and the method is suitable for industrial production.
Owner:HEBEI NONGBIWEI BIOTECHNOLOGY CO LTD

Nonaqueous electrolyte solution, electrochemical device, and electronic device

The invention provides a non-aqueous electrolyte, an electrochemical device and an electronic device. The non-aqueous electrolyte comprises ethylene carbonate, propylene carbonate, propyl propionate and ethyl propionate, and based on the total mass of the non-aqueous electrolyte, the mass contents of ethylene carbonate, propylene carbonate, propyl propionate and ethyl propionate are respectively A%, B%, C% and D%, 5 < = A < = 15, 5 < = B < = 15, 30 < = C < = 50, 5 < = D < = 20, A > = B, 2 < = C / D < = 3.5. When the electrochemical device contains the non-aqueous electrolyte, the cycle performance of the electrochemical device at normal temperature can be improved on the basis of considering the high-temperature performance of the electrochemical device.
Owner:NINGDE AMPEREX TECHNOLOGY LTD

Flavour composition for electronic cigarettes, e-liquid for electronic cigarettes and method for preparing the same

The application provides a flavor composition for electronic cigarettes, electronic cigarette liquid and a preparation method thereof. The flavor composition for electronic cigarettes comprises 0.1-0.4 parts of ethyl isovalerate, 2.0-5.0 parts of isoamyl acetate, 0.1-0.6 parts of ethyl butyrate, 0.4-1.6 parts of ethyl acetate, 0.1-0.6 parts of propyl acetate, 0.1-0.6 parts of myric aldehyde, 0.05-0.3 parts of malic acid liquid and 0.02-0.1 parts of acetic acid liquid. By adjusting the ratio of the flavor composition, the application makes the flavor composition have strawberry flavor, can restore the pure fruit pulp aroma of strawberries, has high restoration degree of strawberry flavor, long aftertaste and good stability after high-temperature and high-humidity baking, and can be applied to electronic cigarette liquid, thereby improving the experience of users using electronic cigarettes.
Owner:BYD PRECISION MANUFACTURE CO LTD

Bacillus velezensis utilizing lactic acid and application of bacillus velezensis in white spirit production

The invention relates to the technical field of microorganisms, in particular to bacillus velezensis utilizing lactic acid and application of the bacillus velezensis in white spirit production. The lactic acid utilization strain obtained through screening has good tolerance, can be applied to Baijiu brewing, can significantly reduce the lactic acid content in the seventh-round fermented grains of Maotai-flavor by about 44.9%, improves the propionic acid and ethyl propionate in Baijiu by about 10.3%, improves the ethyl propionate by about 23.7%, and is stable in effect.
Owner:ANGEL YEAST CO LTD +1

Composition for odour improvement

Proposed are preparations comprising (i) a mixture of substances comprising (a) one, two or more compounds selected from the group consisting of (a1) alcohol monoterpenes of the formula (I) where R1 is H or methyl, R2 is H or C2-alkenyl, and R3 is a linear or branched, saturated or unsaturated hydrocarbon radical having 4 to 10 carbon atoms, and their enantiomers, diastereomers, racemates, solvates and physiologically acceptable salts, and / or (a2) bicyclic epoxy monoterpenes, (b) at least two lactones of the formula (II) where R4 is H or methyl, R5 is a linear or branched, saturated or unsaturated hydrocarbon radical having 2 to 10 carbon atoms and n is the number 1 or 2, and their enantiomers, diastereomers and racemates, and (c) one, two or more Solvent selected from the group consisting of ethanol, water, dipropylene glycol (DPG), diethyl phthalate (DEP), propylene glycol (PG),Isopropyl myristate (IPM), isopropyl palmitate (IPP), triethyl citrate (TEC), triacetin (TRI), 1,2-propanediol, 1,3-propanediol, propanetriol, pentanediol, hexanediol, octanediol, decanediol, dodecanol, 4-hydroxyacetophenone, butylene glycol, pentylene glycol, hexylene glycol, decylene glycol, propylene carbonate, butylene carbonate, glycerol carbonate, 2-benzylheptanol, trimethyl hydroxypentyl isobutyrate, glyceryl caprylate, ethylhexylglycerin, benzyl benzoate (BB), and optionally (d) further flavorings or fragrances selected from the group consisting of 3-phenylbutanal, acetylmethylcarbinol, anethole, anisyl acetate, dihydroeugenol, linalyl formate, 2-methyldecanal, 2-Benzyl-2-methylbut-3-ene nitrile, 3-hexenyl acetate, styralyl acetate, citronellal, cinnamyl acetate, rhubafuran, betalonone, anther, prenyl acetate, 2-phenylpropanal, 4-(4-hydroxyphenyl)butan-2-one, ethylphenoxyacetate, isoraldein, gamma-terpinene, Limonene, Neocyclocitral, Methyl Lavender Ketone, Styralyl Propionate, Phenyl Ethyl Propionate, Limonenal,4-Isopentylcyclohexanol, 4-methyl-2-phenyl-3,6-dihydro-2H-pyran / 4-methylene-2-phenyl-tetrahydropyran, hydrocitronitrile, phenoxanol, isoamylphenyl acetate, damascone, silvial, nectaryl, ambroxide, acetylpyrazine, trimethylpyrazine, isoamyl acetate, cresyl methyl ether para, filbertone, cyclohexyl acetate, heliotropin, acetophenone, anisaldehyde, methylacetophenone para, veratraldehyde, methyl anisate and vertoprenal, and (ii) aldehydes of the formula (III) where R6 is a saturated or unsaturated, linear hydrocarbon radical, and / or (iii) free fatty acids of the formula (IV) where R7 is a linear or branched, saturated hydrocarbon radical.
Owner:SYMRISE GMBH & CO KG

Secondary battery and electronic device

The invention provides a secondary battery and electronic equipment, the secondary battery comprises a negative electrode plate and an electrolyte, the negative electrode plate comprises a negative electrode active material layer, the negative electrode active material layer comprises graphite and a silicon carbon material, the average sphericity of the silicon carbon material is m, and the range of m is 0.81-0.95; the electrolyte comprises ethylene carbonate, propylene carbonate, ethyl propionate and propyl propionate, based on the mass of the electrolyte, the mass percentage content of the ethylene carbonate is a%, the mass percentage content of the propylene carbonate is b%, the mass percentage content of the ethyl propionate is c%, the mass percentage content of the propyl propionate is d%, b ranges from 5 to 26, (a + b) / (c + d) ranges from 0.23 to 1.51, and the sum of the mass percentage content of the ethylene carbonate, the mass percentage content of the propylene carbonate, the mass percentage content of the ethyl propionate and the mass percentage content of the propyl propionate is d%. The electrolyte further comprises lithium difluorophosphate, the mass percentage content of the lithium difluorophosphate is n% based on the mass of the electrolyte, and m / n ranges from 3 to 14.5. According to the invention, the discharge performance and the safety performance of the secondary battery at low temperature can be improved.
Owner:NINGDE AMPEREX TECHNOLOGY LTD

Saccharomyces cerevisiae with high yield of flower and fruit fragrance and application thereof

The invention belongs to the technical field of microorganisms, and relates to saccharomyces cerevisiae with high yield of flower and fruit fragrance and application thereof. The strain is preserved in the China Center for Type Culture Collection, the preservation number is CCTCC M 20242771, the preservation time is December 10, 2024, the strain is separated from the natural fermentation process of blueberries in Danzhai region of Guizhou province, and the strain has excellent brewing characteristics including high ethanol (13.6% vol) and glycerol (7.48 g / L) yield, low hydrogen sulfide yield, positive killing and the like. When the strain is used for blueberry wine fermentation, the flower fragrance of an obtained blueberry wine sample is richer, the anthocyanin content exceeds that of a wine sample fermented by commercial yeast CECA, flavor analysis shows that the strain has obvious advantages in the aspect of producing key aroma compounds such as methyl benzoate, ethyl propionate, phenethyl acetate and beta-damascenone, and the strain has good application prospects. The OAV value of methyl benzoate in a wine sample fermented by the strain is 306.16, the wine can be endowed with more flower fragrance and fruit fragrance such as cherries, and richer fragrance levels are brought to a wine body.
Owner:KWEICHOW MOUTAI (GRP) ECOLOGICAL AGRI IND DEV CO LTD

Secondary battery and electronic device including the same

The application belongs to the technical field of electrochemistry and relates to a secondary battery and an electronic device comprising the secondary battery. The secondary battery comprises a positive electrode, a negative electrode, a separator and an electrolyte; the negative electrode active material of the negative electrode comprises a silicon-carbon material; the electrolyte comprises ethyl propionate and propyl propionate, the mass percentage content of the ethyl propionate is a% and the mass percentage content of the propyl propionate is b% based on the total mass of the electrolyte, wherein 1.7<=a / b<=5.7; the electrolyte further comprises at least one of vinylene carbonate, a boron-containing lithium salt and a compound comprising a structure shown in Formula I; wherein A in Formula I is selected from C2 to C5 alkylene. The secondary battery, by improving the used electrolyte system, reduces the gas generated by the secondary battery containing the electrolyte system at high temperature, and further improves the high-rate discharge performance of the secondary battery.
Owner:NINGDE AMPEREX TECHNOLOGY LTD

Ethylene carbonate-free electrolyte and battery

The invention relates to the technical field of batteries, in particular to an electrolyte without ethylene carbonate and a battery. The electrolyte comprises fluoroethylene carbonate, diethyl carbonate, propylene carbonate and a compound A, and the compound A is at least one of ethyl propionate and propyl propionate; based on the total mass of the electrolyte, the mass content w1 of the fluoroethylene carbonate is 10-30%; the mass content w5 of the diethyl carbonate is 5%-25%; the content w6 of the propylene carbonate is 5%-28%; the mass content of the compound A is w2, and w2 is 25%-60%; under the condition that the compound A is a combination of ethyl propionate and propyl propionate, the mass content of ethyl propionate is greater than that of propyl propionate; and 1.04 < = w1 / w5 < = 3.5. Comprising the electrolyte provided by the invention is improved in high-temperature stability, dynamic performance and cycle performance.
Owner:ZHUHAI COSMX BATTERY CO LTD

A reaction kettle for producing ethyl propionate

The utility model relates to the technical field of reaction kettle discloses a reaction kettle of production ethyl propionate, including kettle body, the kettle body top is provided with the kettle cover, the kettle cover inside fixedly connected with the feed pipe, the kettle cover top is provided with the motor, the motor output fixedly connected with the pivot, the pivot side wall is provided with the adjusting mechanism, the pivot outside is provided with the stirring vane, the kettle cover inside fixedly connected with the exhaust pipe, the exhaust pipe top is provided with quick -release mechanism, the adjusting mechanism includes the fixed peg and the recessed hole of opening in the pivot inside, the fixed peg side wall sliding connection is in the recessed hole inside. In the utility model, by pulling the fixed peg, makes the slip ring to drive the stirring vane and moves up and down along the pivot's axial direction, can according to the height of liquid level or the increase of material viscosity in the reaction process, the immersion depth and the action area of stirring vane are adjusted flexibly, not only has optimized the mass transfer heat transfer efficiency, also avoided the problem of local overheating and reaction uneven.
Owner:SUZHOU YONGNUOHONGZE BIOTECHNOLOGY CO LTD

Rapid purification device

The utility model relates to the field of ethyl dicyanopropionate, in particular to a rapid purification device which comprises a machine body, a front display controller is fixedly installed outside the machine body, a barrel groove is formed in the upper portion of the machine body, and a first purification barrel is fixedly installed in the barrel groove. An outer temperature sensor is fixedly mounted outside the first purification cylinder, an inner purification cylinder is arranged in the first purification cylinder, and an outer caulking groove is formed in the outer part of the inner purification cylinder. Through the arrangement of the first purification cylinder, the outer temperature sensor, the inner purification cylinder, the electric heating pipe, the spacing cylinder, the second purification cylinder and the filter screen, raw materials entering the first purification cylinder can enable an external operator to firmly grasp the temperature of the inner purification cylinder under the control of the outer temperature sensor; the device can be used for purifying the dicyanoethyl propionate at a proper temperature, and can meet the purification requirements of different dicyanoethyl propionate.
Owner:WENZHOU JIALI CHEM

Low-energy-consumption production process for esterification synthesis of ethyl propionate

The invention provides a low-energy-consumption production process for esterification synthesis of ethyl propionate. According to the method, propionic acid is added from the middle part or the lower part of an esterification tower, and an ethyl propionate-water-ethanol ternary azeotropic system is broken through the strong association effect of propionic acid and water; in addition, sulfuric acid and propionic acid are fixed at the bottom of the esterification tower and the middle lower part of the esterification tower under the strong complexing action of the acid-binding agent, so that side reaction caused by entrainment of the sulfuric acid and the propionic acid on the upper part of the esterification tower can be reduced; reflux of ethyl propionate at the top of the tower can be effectively reduced by reducing concentration of sulfuric acid and propionic acid at the middle or upper part of the esterification tower, and energy consumption is reduced.
Owner:ZHUHAI QIANXIN NEW MATERIALS CO LTD +3

Application of compound in prevention and control of plant pathogenic fungus fusarium oxysporum

The invention discloses application of a compound to prevention and control of plant pathogenic fungus fusarium oxysporum, and belongs to the technical field of agricultural disease prevention and control. The compound is 3-[1-(1H-benzimidazole-2-yl)-5-hydroxy-3-methyl-1H-pyrazole-4-yl] ethyl propionate. According to the invention, it is found for the first time that the 3-[1-(1H-benzimidazole-2-yl)-5-hydroxy-3-methyl-1H-pyrazole-4-yl] ethyl propionate has a relatively strong inhibition effect on plant pathogenic fungus fusarium oxysporum; experiments show that the compound has a median inhibitory concentration IC50 of 25.2 [mu] g / mL on fusarium oxysporum, and compared with other bactericides, the compound has the advantages of high efficiency, low toxicity and low residue, has better environmental compatibility, and meets the requirements of green plant protection and sustainable agricultural production and the needs of development.
Owner:YUNNAN UNIV

Novel electrolyte composition for sodium-ion batteries

The present invention relates to an electrolyte composition comprising at least a sodium salt dissolved in at least one solvent and a combination of additives, wherein: the solvent is selected from the group consisting of ethylene glycol carbonate, dimethyl carbonate, ethyl methyl carbonate, diethyl carbonate, propylene carbonate, ethyl acetate, ethyl propionate, methyl propionate, 4-fluorotoluene, 1,1,2,2-tetrafluoroethyl 2,2,3,3-tetrafluoropropyl ether, difluoroethylene glycol carbonate, ethyl difluoroacetate and mixtures thereof; and the combination of additives comprises at least sodium difluoro(oxalato)borate (NaODFB) and tris(trimethylsilyl)phosphite (TMSPi).
Owner:CENT NAT DE LA RECH SCI (C N R S) +2

A local high-concentration lithium metal battery electrolyte, a preparation method and application thereof

The application discloses a local high-concentration lithium metal battery electrolyte and a preparation method and application thereof. The electrolyte comprises a lithium salt, an organic solvent, an additive and a diluent; the organic solvent comprises at least one of methyl formate, methyl acetate, methyl propionate, methyl butyrate, ethyl propionate, ethyl acetate, ethyl butyrate, methyl trifluoroacetate and ethyl trifluoroacetate; the additive comprises at least one of fluoroethylene carbonate, lithium difluorobisoxalate phosphate and lithium difluorophosphate; and the diluent is a fluorine-containing ether compound. The local high-concentration electrolyte has the advantages of high-voltage resistance of high-concentration electrolyte and inhibition of corrosion of sulfonimide-based electrolyte on aluminum foil, meanwhile, the problems of high viscosity, low conductivity and poor impregnation with a separator of high-concentration electrolyte are overcome, the cycle performance and low-temperature performance of the lithium metal battery are significantly improved, and the local high-concentration electrolyte is particularly suitable for application in a low-temperature high-voltage lithium battery. The preparation method is simple, the cost is low, and the method is suitable for industrial production.
Owner:CENT SOUTH UNIV

Electrolyte, secondary battery, and electronic apparatus

Disclosed in the present application are an electrolyte, a secondary battery and an electronic apparatus. The electrolyte comprises ethylene sulfate and vinylene carbonate, wherein on the basis of the mass of the electrolyte, the mass percentage content of the ethylene sulfate is A% and the mass percentage content of the vinylene carbonate is B%, 0.1≤A / B≤4; the electrolyte at least comprises ethyl propionate and propylene carbonate; the electrolyte further comprises a first substance, wherein the first substance is at least two selected from lithium difluorophosphate, lithium difluoro(oxalato)borate, lithium bis(trifluoromethanesulfonyl)imide or lithium hexafluorophosphate, and at least contains lithium difluorophosphate, and on the basis of the total mass of the electrolyte, the mass percentage content of the first substance is 0.3 wt%-1.2 wt%. In the process of charge and discharge of the secondary battery of the present application, the low-temperature cycle performance and the overcharge prevention capacity under a large current condition of the secondary battery and an electrochemical apparatus can be improved.
Owner:NINGDE AMPEREX TECHNOLOGY LTD

Wickerhamomyces anomalus JG-WA1 and application of Wickerhamomyces anomalus JG-WA1 in aroma-enhancing fruit wine

The invention belongs to the technical field of fermentation engineering, and particularly relates to Wickerhamomyces anomalus JG-WA1 and application thereof in aroma-enhancing fruit wine. A strain of aroma-enhanced Wickerhamomyces anomalus JG-WA1 is screened from distiller's yeast, apple juice is inoculated with the strain for primary fermentation, then saccharomyces cerevisiae is inoculated for secondary fermentation, and the aroma-enhanced fruit wine is prepared. The content of unpleasant odor substances such as acetone, 4-methyl-1-pentanol, 2-butanol, dimethyl disulfide, 3-hexanone and the like with pungent smell of alcohol or mildew odor and the like in the fruit wine is obviously reduced, while the content of 2-pentanol, ethyl propionate, propyl acetate, 3-methyl-2-pentanone, 3-pentene-2-ketone, hexyl hexanoate, ethyl hexanoate, methyl acetate, heptanal, 2-octanone, 2, 3-pentanone, ethyl hexanoate, ethyl hexanoate, methyl acetate, heptanal, ethyl hexanoate, ethyl hexanoate, ethyl hexanoate, ethyl hexanoate, ethyl hexanoate, ethyl hexanoate, ethyl hexanoate, ethyl hexanoate, ethyl hexanoate, ethyl hexanoate and ethyl hexanoate is obviously reduced. The content of fruit flavor components such as 2, 3-dimethylpyrazine is greatly increased, the brewed apple wine is obvious in ester flavor and transparent and bright in color, and the flavor quality is obviously improved.
Owner:JINAN INST OF FRUIT PRODS CHINA GENERAL SUPPLY & MARKETING COOP +1

Secondary battery and electronic device

PendingUS20260196565A1Electrolytic agentPropanoic acid
A secondary battery, including a negative electrode plate and an electrolyte, where the negative electrode plate includes a negative electrode active material layer. The negative electrode active material layer includes graphite and a silicon-carbon material, and an average sphericity of the silicon-carbon material is 0.81 to 0.95. The electrolyte includes ethylene carbonate, propylene carbonate, ethyl propionate and propyl propionate, where based on a mass of the electrolyte, a mass percentage of the ethylene carbonate is a %, a mass percentage of the propylene carbonate is b %, a mass percentage of the ethyl propionate is c %, a mass percentage of the propyl propionate is d %, and (a+b) / (c+d) is in a range of 0.23 to 1.51.
Owner:NINGDE AMPEREX TECHNOLOGY LTD

Preparation method and application of small-particle-size sulfide solid electrolyte

This invention provides a method for preparing small-particle-size sulfide solid electrolytes and their applications. Under an inert atmosphere, a sulfide solid electrolyte precursor is mixed with a first solvent and reacted. The first solvent is selected from at least one of ethylenediamine, N,N-dimethylacetamide, and 1,2-ethylenedithiol. The mixture is then further mixed with a second solvent, and stirred to precipitate the sulfide solid electrolyte. The second solvent is selected from at least one of n-hexane, n-heptane, ethyl acetate, ethyl propionate, and N,N-dimethylacetamide. Solvent separation, drying, and heat treatment are then performed. This method synthesizes the sulfide solid electrolyte in the first solvent, which is then directly transferred to the second solvent, allowing the sulfide solid electrolyte to precipitate. Direct solvent separation eliminates the crystallization process, significantly reducing time and costs. The method is simple and efficient, resulting in high purity and high ionic conductivity. The resulting battery exhibits high discharge capacity, excellent cycle performance, rate capability, and limiting current density.
Owner:WEICHAI POWER CO LTD

A continuous closed-loop production process for preparing propionic acid esters from methanol or dimethyl ether as raw material

The application discloses a continuous closed-loop cyclic production process for preparing propionic acid ester by taking methanol or dimethyl ether as raw material, and belongs to the technical field of organic synthesis chemical industry. The process comprises the following steps: S1, methyl acetate is hydrogenated to generate mixed alcohol of methanol and ethanol; S2, mixed alcohol is etherified with methanol to generate mixed ether comprising dimethyl ether, diethyl ether and methyl ethyl ether; S3, mixed ether is carbonylated with dimethyl ether and carbon monoxide to generate mixed ester comprising methyl acetate, ethyl acetate, methyl propionate and ethyl propionate; S4, ethyl acetate, methyl propionate and ethyl propionate products are obtained through rectification separation in a plurality of towers in series connection, and methyl acetate is recovered; and S5, the recovered methyl acetate is recycled back to the step S1. By constructing a methyl acetate directional closed-loop cyclic system, the application realizes efficient co-production of propionic acid ester and ethyl acetate, uses solid catalysts in the whole process, avoids strong acid corrosion, has high raw material utilization rate, has mild reaction conditions, can be continuously produced in industry, and effectively solves the problems of high cost, single product and non-recyclable utilization in the prior art.

Wide-temperature-range sodium-ion battery electrolyte suitable for hard carbon negative electrode and preparation method and application of wide-temperature-range sodium-ion battery electrolyte

The invention relates to the field of sodium-ion batteries, in particular to a wide-temperature-range sodium-ion battery electrolyte suitable for a hard carbon negative electrode and a preparation method and application of the wide-temperature-range sodium-ion battery electrolyte. The wide-temperature-range sodium-ion battery electrolyte suitable for the hard carbon negative electrode comprises sodium salt, an organic solvent and an additive, wherein the sodium salt is selected from sodium perchlorate; the organic solvent is composed of a solvent A and a solvent B, the solvent A is selected from propylene carbonate, and the solvent B is selected from ethyl propionate; the additive is selected from fluoroethylene carbonate. The sodium ion solvation structure is regulated and controlled by regulating and controlling the salt concentration, the cosolvent proportion and the additive proportion, then an interface passivation layer is precisely regulated and controlled, electrochemical decomposition is inhibited, interface impedance is reduced, the wide-temperature-range cosolvent electrolyte is developed, stable and reversible charging and discharging of a sodium ion battery at the temperature of 50 DEG C below zero to 70 DEG C are achieved, and the application scene of the battery is widened.
Owner:NANKAI UNIV

Electrochemical device and electronic device

An electrochemical device includes an electrode assembly and an electrolyte. The electrode assembly includes a negative electrode plate including a negative electrode active material layer. The negative electrode active material layer includes a negative electrode active material; and a negative electrode binder including an ester substance and a non-ester substance. Based on a mass of the negative electrode binder, a mass percentage of the ester substance is x; the electrolyte includes fluoroethylene carbonate and a high-kinetic solvent, the high-kinetic solvent includes at least one of ethyl propionate, propyl propionate, or diethyl carbonate. A ratio of a mass percentage of fluoroethylene carbonate to a mass percentage of the high-kinetic solvent in the electrolyte is y; and 17%≤x+y≤53%, y is from 0.4% to 14%. Based on a mass of the electrolyte, a mass percentage of fluoroethylene carbonate is from 0.1% to 10%.
Owner:NINGDE AMPEREX TECHNOLOGY LTD

Yogurt flavor and method for preparing the same

The application relates to the technical field of edible essence. The application discloses a yogurt essence and a preparation method thereof. The raw material composition of the yogurt essence comprises ethyl maltol, vanillin, butanedione, acetic acid, ethyl acetate, propionic acid, 2,3-pentanedione, 3-hydroxy-2-butanone, butyric acid, ethyl butyrate, isoamyl acetate, methyl thio butyrate, hexanoic acid, ethyl hexanoate, 10% furanone, isoamyl butyrate, ethyl levulinate, linalool, p-cymene, 4-terpinenol, nerol, citral, geraniol, neryl acetate, geranyl acetate, D-limonene, lemon oil, distilled white lemon oil, sweet orange oil, glycerol triacetate, rosemary extract and bitter gourd extract. The yogurt essence prepared by the application has a flavor closer to real yogurt, good thermal stability and good flavor persistence.
Owner:DONGGUAN QIYI SPICES CO LTD

Lithium-ion rechargeable battery

This invention provides a lithium-ion secondary battery containing allyl succinic anhydride as an electrolyte additive, which exhibits excellent initial charge efficiency and output characteristics. [Solution] The lithium-ion secondary battery comprises a positive electrode containing a positive electrode active material capable of intercepting and releasing lithium ions, a negative electrode containing a negative electrode active material capable of intercepting and releasing lithium ions, a separator disposed between the positive electrode and the negative electrode, and a non-aqueous electrolyte containing a lithium salt, a non-aqueous solvent, and an electrolyte additive. The negative electrode active material contains natural graphite and artificial graphite, the non-aqueous solvent contains ethylene carbonate, diethyl carbonate, ethyl propionate, and propyl propionate, and the electrolyte additive contains allyl succinic anhydride and dinitrile, with the electrolyte additive containing dinitrile in a proportion of 1.5% by mass or more and 3.2% by mass or less.
Owner:THE FURUKAWA BATTERY CO LTD

Sodium metal battery electrolyte used under high voltage and preparation method and application thereof

The invention discloses a sodium metal battery electrolyte used under high voltage and a preparation method and application thereof, and belongs to the technical field of sodium metal batteries. The sodium metal battery electrolyte comprises sodium salt, cyclic carbonate, chain carbonate and fluorocarboxylate, wherein the concentration of the sodium salt is 0.5-1.5 mol / L, and the mass ratio of the cyclic carbonate to the chain carbonate to the fluoro carboxylic ester is (0.3-0.35): (0.4-0.55): (0.1-0.3); the sodium salt is one of sodium hexafluorophosphate and sodium bis (fluorosulfonyl) imide, the cyclic carbonate is fluoroethylene carbonate, the chain carbonate is ethyl methyl carbonate (EMC), and the fluorocarboxylic ester is one of ethyl 2, 2-trifluoroacetate, methyl 3, 3, 3-trifluoropropionate, ethyl 3, 3, 3-trifluoropropionate, methyl 4, 4, 4-trifluorobutyrate, ethyl 4, 4, 4-trifluorobutyrate and methyl perfluorobutyrate. Through the combined design of fluoroethylene carbonate (FEC), chain carbonate and fluorocarboxylate, an advanced electrolyte system is constructed together, and the electrolyte has excellent performance of high rate performance and long-term cycle stability at the same time under high voltage.
Owner:BEIJING UNIV OF CHEM TECH

Essence with strawberry flavor as well as preparation method and application thereof

The invention belongs to the technical field of essence, and particularly relates to essence with strawberry flavor as well as a preparation method and application thereof. Comprising one or more of a strawberry hot reflux extract, a strawberry supercritical CO2 extract, 200 nm, 50 nm, 10 nm, 5 nm and 2 nm membrane interception liquid or 2 nm membrane permeation liquid of strawberries, and strawberry molecular distillation light components. The plant essential oil further comprises one or more of furanone, leaf alcohol, ethyl acetate, ethyl propionate, peach aldehyde, vanillin, vanilla planifolia extract, ethanol, cinnamyl alcohol, citric acid and Peru balsam. The obtained strawberry-flavored essence has the function of restoring the natural fragrance of strawberries from different dimensions.
Owner:HONGTA LIAONING TOBACCO CO LTD