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1945 results about "Graphite electrode" patented technology

Multi-purpose, multi-oxy-fuel, power burner/injector/oxygen lance device

A multi-purpose, multi-oxy-fuel High Temperature Power Burner/Injector/Oxygen Lance, Mechanical System Apparatus Device, for steelmaking from recycled scrap and/or virgin ferrous charge, which can be employed in multi-oxy-fuel (natural gas; pulverized carbonaceous matter; heavy oil), especially by Oxygen Combusted mixture of Natural Gas/Pulverized Carbonaceous Matter in High Temperature Power Burner Mode, for efficient and rapid melting of solid ferrous charge (cold or preheated) in a special steelmaking Metallurgical Furnace or Open Hearth Furnace, Tandem Furnace, BOF, EAF, as its augmenting or only source of thermal energy; more than one Device in Oxygen-Natural Gas/Pulverized Carbonaceous Matter Power Burner Mode, can be employed as the only source of thermal energy in a modified, originally Electric Arc Furnace, as total replacement of Graphite Electrodes and Electric Arc System, the replacement being noticeably more primary energy efficient than the thermal energy provided by Graphite Electrode/Arc System; it also can be employed in an Solid Particles Injector Mode, for injecting of adequately granulated carbonaceous materials or lime into the molten steel for its carburizing or for foamy slag control; further it can be employed in a natural gas shrouded, pulsating oxygen stream, for vertically to the charge oriented soft blow supersonic Oxygen Injection Lance Mode, for decarburization of the molten metal contained in the hearth of the metallurgical furnace and foamy slag control; in one of the embodiments-generally arcuate-pivotally mounted, liquid media cooled composite body, is pivoted into and out of a furnace vessel through a small opening in the shell wall for auto-regulated constant optimal positioning of the Composite Body Tip against solid or molten charge, in each and all multi-purpose modes; furthermore, when inserted into the furnace vessel, the arcuate composite body can be rotated about its longitudinal axis for directing the oxy-fuel high temperature flame towards unmolten charge in the furnace; in an other-generally linear-embodiment, the liquid cooled composite body is attached to the mast type carrier allowing vertical movement of the composite body which enters the furnace vessel through a small opening in the furnace roof; the bimetallic, liquid cooled special tip assembly of both-arcuate and linear embodiments-of the composite body includes easy replaceable, independent, multi-opening nozzles, mounted in a protective, retracted position inside of the liquid cooled special tip assembly.
Owner:EMPCO (CANADA) LTD

Method for electrochemically preparing graphene

The invention discloses a method for electrochemically preparing graphene, which preferably comprises the steps of pressing a high-purity graphite raw material to form a graphite electrode, carrying out anodization through the graphite electrode by using sulfuric acid aqueous solution or acetic acid and the like mixed acid solution as an electrolyte to prepare a graphite intercalation product, and obtaining expanded graphite by high temperature or microwave and other methods; and then pressing the expanded graphite to prepare a reaction electrode, and carrying out secondary electrochemical intercalation and expansion to finally obtain laminar graphene. According to the invention, in the preparing process, potassium permanganate and other strong oxidizers are not used, and the damage of the strong oxidizers to the structure and performance of graphene are avoided; alkali metal, fuming sulfuric acid oxydol and other inflammable and explosive dangerous substances are not used, and toxic or harmful substances are not introduced, so that the production is safe and environment friendly; and at the same time, the method is simple in process flow, easy to operate, low in cost, high in yield, mild in reaction conditions and low in energy consumption, and is suitable for industrialized large-scale production.
Owner:苏州格瑞丰纳米科技有限公司

Method for regenerating graphene by recovering waste lithium ion battery

The invention discloses a method for regenerating graphene by recovering a waste lithium ion battery. The method is characterized by comprising the following steps of: S1, recovery of an active substance of a battery electrode: carrying out pre-charge or pre-discharge treatment on the waste lithium ion battery which takes graphite as an anode material, and then separating a cathode coating and an anode coating from a current collector and an outer package to obtain a cathode and anode blending material; S2, separation of an intercalated graphite electrode material: drying and crushing the cathode and anode blending material, and separating the active substances of a positive electrode and a negative electrode by adopting a physical method to obtain intercalated graphite powder; and S3, preparation of graphene from the intercalated graphite powder: preparing the graphene by an oxidation-reduction method or an ultrasonic stripping method based on the intercalated graphite powder as a raw material. After the method is adopted, the industrial recovery of the lithium ion battery is realized, and a graphene material can be regenerated by a graphite anode with high added value, so that the method has better application prospect and feasibility, and can produce greater economic benefit and social benefit.
Owner:SHENZHEN GRADUATE SCHOOL TSINGHUA UNIV

Ultra high power graphite resistor rod with 600mm diameter and method for producing the same

ActiveCN101553060ASolve capacitySolve the scale-up problemElectric discharge heatingVolumetric Mass DensityCoal
The present invention provides an ultra high power graphite resistor rod with 600mm diameter and a method for producing the same. The method utilizes domestic coal series acicular coke with low true density in main physicochemical standard, high heat expansion coefficient and sulphur content for producing the large-size ultra high power graphite resistor rod with 600mm diameter. Volumetric density, bending strength, elastic modulus, electric resistivity and heat expansion coefficient of the product reaches the international standard after detecting which can solve difficult problem that the domestic coal series acicular coke can not produce the large-size ultra high power graphite resistor rod with 600mm diameter because of low true density in main physicochemical standard, high heat expansion coefficient and sulphur content, and can realize localization for raw material acicular coke of the large-size ultra high power graphite resistor rod, simultaneity, also can solve problem that the acicular coke depends on importation in a long time and has high cost for restricting expanding yield and scale of the ultra high power graphite resistor rod in carbon industry. The product can reduce cost and improve economic performance.
Owner:KAIFENG CARBON CO LTD OF CHINA PINGMEI SHENMA GRP

Recycling method of retired lithium iron phosphate battery positive-electrode materials

The invention discloses a recycling method of retired lithium iron phosphate battery positive-electrode materials. The method includes the steps: soaking and dissolving binding agents in an N-methylpyrrolidone solvent by the aid of the N-methylpyrrolidone solvent to strip LiFePO4 positive-electrode materials and aluminum foil fluid collectors; mixing the stripped waste LiFePO4 positive-electrode materials and binding agents; coating a carbon fabric or titanium mesh with mixture of the waste LiFePO4 positive-electrode materials and the binding agents to serve as a positive electrode; taking a graphite electrode as a negative electrode; building an electrolytic tank in electrolyte solution; driving lithium removal by the aid of a direct-current electric field to collectively recycle lithiumions and lithium removal product iron phosphate. According to the method, lithium removal is driven and adjusted by the direct-current electric field, lithium can be basically completely removed, subsequent treatment of the electrode materials after lithium removal is performed, so that treated electrode materials can be converted into the iron phosphate, and the iron phosphate can be used for preparing lithium iron phosphate positive-electrode materials and is good in electrochemical performance. The method is simple and convenient in operation process, controllable in condition, high in recycling rate and environmentally friendly, and popularization and application are facilitated.
Owner:HEFEI UNIV OF TECH

Three-level acceleration type spiral wave plasma propulsion device

The invention discloses a three-level acceleration type spiral plasma propulsion device. The three-level acceleration type spiral wave plasma propulsion device is characterized in that an antenna is connected with an RF (Radio Frequency) power source, the antenna and a discharge chamber are fixedly arranged in a sleeve, and an electromagnetic coil is fixedly arranged on the outer circumferential surface of the sleeve in a surrounding way; the rear part of the discharge chamber is provided with a rotating electric field ion acceleration system, and the rotating electric field ion acceleration system comprises four graphite electrodes which are uniformly and symmetrically arranged on the outer circumferential surface of the sleeve; the tail end of the rotating electric field ion acceleration system is provided with an electromagnetic spray pipe ion acceleration system, and the electromagnetic spray pipe ion acceleration system comprises a conical expanding spray pipe of which one end is connected with the tail part of the discharge chamber, and the electromagnetic coil. According to the three-level acceleration type spiral plasma propulsion device disclosed by the invention, the rotating electric field acceleration system is adopted for carrying out secondary acceleration on a plasma, acceleration is further carried out through the electromagnetic spray pipe, and a three-level acceleration effect is formed, thus the thrust is generated by efficiently accelerating ions, the work of a propulsor under high power can be realized, the reliable performance of high ion ejecting speed and high propulsion capacity can be realized, wide application prospect is obtained, and a high-performance power platform can be provided for future space technology development.
Owner:DALIAN UNIV OF TECH

Protective atmosphere vacuum sintering furnace with high temperature of 1800 DEG C

The invention discloses a protective atmosphere vacuum sintering furnace with high temperature of 1800 DEG C. A control system is connected with an electronically-controlled execution component arranged in an apparatus, a graphite sealing box is arranged in a heating chamber, an air inlet pipeline and an exhaust pipeline of a high-temperature vacuum sintering furnace are connected with the graphite sealing box. The protective atmosphere vacuum sintering furnace is characterized in that the furnace has two techniques of atmosphere sintering and vacuum sintering, and a function conversion measurement is actualized by a control program; a furnace shell is provided with a thermoelectric couple and a copper electrode; the part of a shell column body is provided with a pipe joint communicated with an evacuation unit of a vacuum system; and a square heating chamber is arranged in the furnace shell, heaters are fixed on four walls in the heating chamber, and the heater is internally provided with a sealing box and a support material frame; and the air inlet pipeline and the exhaust pipeline communicated with the sealing box passes through an upper wall and a lower wall of the heating chamber and the sealing box through a graphite pipe to communicate with the inside of the sealing box, one end of the furnace shell is provided with a gas circulating cooling blower, an inner wall of the sealing box is provided with the thermoelectric couple and the copper electrode, and the copper electrode is connected with the heater through a graphite electrode. A volatile substance sealed in the sealing box can not disperse during vacuum sintering, thereby effectively preventing the volatile substance from polluting and damaging the heater, and simultaneously achieving the effect of enabling the protective gas to take the volatile substance away to protect furnace materials, and improving the utilization ratio of the protective gas.
Owner:SHENYANG HENGJIN VACUUM TECH

Remedying method for removing chrome in contaminated soil of chromium slag site in situ

The invention discloses a remedying method for removing chrome in contaminated soil of a chromium slag site in situ. The method comprises the following steps of: (1) smashing the air-dried chromium-contaminated soil of the chromium slag site, and sieving the smashed soil; (2) mixing the soil sieved in the step (1) and a citric acid solution to ensure that the moisture content of the soil reaches a set value, carrying out uniform stirring and then carrying out balancing for one day; (3) putting the soil balanced in the step (2) in a soil sample chamber of an electrokinetic remediation device, wherein the two ends of the soil sample chamber of the electrokinetic remediation device are respectively a cathode chamber and an anode chamber; and (4) adding an electrolyte to the cathode chamber and the anode chamber, respectively inserting graphite electrodes in the cathode chamber and the anode chamber, and connecting a power source to ensure that electric currents pass through the soil chamber to carry out electrokinetic remediation, wherein the electrolyte is a KCI solution. For the high-chromium-content alkaline contaminated soil of the chromium slag site, the remedying method is simple in technology, higher in removal efficiency of chrome in comparison with a common electrokinetic remediation method, low in unit energy consumption and lowered in cost, and can effectively reduce the bioavailability of residual chromium in the soil.
Owner:CHINESE RES ACAD OF ENVIRONMENTAL SCI

Phi 800mm general power graphite electrode and production method thereof

The invention provides a phi 800mm general power graphite electrode and a production method thereof. The method comprises the following steps of: preparing dry materials by using large delay petroleum coke particles, middle delay petroleum coke particles, delay petroleum coke powder materials and graphite powder; after pre-heating the dry materials, putting into a kneading boiler, adding ferric oxide powder and stearic acid which serve as additives in the kneading boiler, adding middle-temperature modified coal pitch serving as adhesives and wetly mixing to prepare paste materials; and putting the paste materials into a material cooling boiler and cooling, extruding, roasting and graphitizing to produce the phi 800mm general power graphite electrode. According to the method, the ideal extrusion molding manner of the graphite electrode is adopted, and novel technique formula, technology and mature production equipment are used to produce the general power graphite electrode capable of replacing the original carbon electrodes and vibration molding electrodes; moreover, the smelting input power is improved and the smelting energy consumption is reduced. Both the quality index and theuse performance of the produced products reach the national standards; the use consumption of the phi 800mm general power graphite electrode is reduced; and the economic benefit is improved.
Owner:FANGDA CARBON NEW MATERIAL CO LTD

Ultrahigh-temperature thermal current simulation system used for spacecraft vacuum thermal test

InactiveCN104015942ASolve the technical problems of ultra-high temperature and extremely high heat flow simulationSolve temperature problemsCosmonautic condition simulationsThermal insulationHeater Rod
The invention discloses an ultrahigh-temperature thermal current simulation system used for a spacecraft vacuum thermal test in a vacuum container. The ultrahigh-temperature thermal current simulation system mainly comprises a semi-cylindrical graphite heating array, high-reflectivity high-temperature thermal insulation assembly units, a graphite heating array installing support, an ultrahigh temperature measuring unit and a power-regulator power control unit. A plurality of graphite heating rods are arranged and combined into the semi-cylindrical graphite heating array according to the requirements for the density and uniformity of thermal currents. Each graphite heating rod is composed of a graphite heating body and a graphite electrode, alternating-current electricity supply is adopted, and wiring electrode leads penetrate through a high-current cabin-penetrating electricity supply flange arranged on a container wall of the vacuum low-temperature environment simulation container and are electrically connected with the temperature measuring unit and the power-regulator power control unit respectively. Through the unique design of the graphite heating array, the high-reflectivity high-temperature thermal insulation assembly units and the ultrahigh temperature measuring unit, measurement of and control over temperatures over 1800 DEG C in the space environment simulation container are achieved, and the ultrahigh-temperature thermal current simulation system is also suitable for high-temperature and high-thermal-current environment simulation requirements in vacuum thermal tests of all types of spacecraft.
Owner:BEIJING INST OF SPACECRAFT ENVIRONMENT ENG

Ultrathin graphene piece, apparatus for preparing ultrathin graphene piece, method for preparing ultrathin graphene piece, capacitor, and method of manufacturing capacitor

The problem addressed by the present invention is to provide an apparatus for preparing ultrathin graphene pieces capable of preparing ultrathin graphene pieces in which less than 10 pieces of graphene are overlapped in large quantities, a method for preparing ultrathin graphene pieces capable of preparing the ultrathin graphene pieces with high yield, an ultrathin graphene piece in which less than 10 pieces of graphene are overlapped, a capacitor having high performance by using the ultrathin graphene piece as an electrode, and an efficient method of manufacturing the capacitor. The above-described problem can be solved by using an apparatus 20 for preparing ultrathin graphene pieces, the apparatus comprising: a graphite electrode 21; a counter electrode 22 which is made of graphite, a corrosion resistant alloy, or a precious metal; an electrolytic solution 25 in which one end sides of the two electrodes 21 and 22 are immersed; a container 24 which stores the electrolytic solution 25; and a power source 28 which is connected to the two electrodes 21 and 22 via wirings 26 and 27. The apparatus is also provided with a porous filter 23 so as to cover at least the immersed part of the graphite electrode 21 that is immersed in the electrolytic solution 25.
Owner:NAT INST FOR MATERIALS SCI

Process for producing moderate temperature modified bitumen by continuously pressurizing and hot-polymerizing at two stages connected in series

The invention relates to a method for manufacturing high-quality intermediate temperature modified pitch through two-section serial continuous pressurizing hot polymerization. The method comprises the following steps that: mid-temperature pitch is made into modified pitch by a two-section serial reaction kettle through low-pressure heating polycondensation; heating precracking reaction is carried out during a first section, while heating polycondensation reaction is carried out quickly during a second section so as to increase the content of toluene insoluble and reduce the content of quinoline insoluble, thereby increasing a beta value; the reacted material is fed in a flash tower, and the softening point of the modified pitch is adjusted inside the flash tower; and the tail gas of a flash system is fed in a flue gas absorption system to be absorbed by circular wash oil, and then is discharged through a chimney. The method can manufacture intermediate temperature modified pitch which meets special requirements and has a lower softening point (80 to 90 DEG C), a controllable softening point amplitude of between 1 DEG C below zero and 1 DEG C and higher beta resin content (more than 18 percent), thereby providing a high-quality raw material for making an ultra-high power graphite electrode.
Owner:山西宏特煤化工有限公司

Process for the production of needle coke

A process is disclosed for producing needle coke from heavy atmospheric distillation residues having sulfur no more than 0.7 wt %, which process involves the steps of heating the feedstock to a temperature in the range of 460 to 540° C. for thermal cracking in a soaking column under pressure in the range of 1 to 10 kg/cm2 to separate the easily cokable material, separating the cracked products in a quench column and a distillation column and then subjecting the hydrocarbon fraction from the bottom of the quench column and a heavy gas oil fraction having 10% true boiling point more than 370° C. and 90% true boiling point not less than 480° C. from the distillation column and/or any other suitable heavier hydrocarbon streams in a definite ratio depending on certain characteristic parameters to thermal cracking in a second soaking column at a temperature of 440 to 520° C., pressure in the range of 2 to 20 kg/cm2 in presence of added quantity of steam for formation of a mesophase carbonaceous structure which on steam stripping and cooling forms a solid crystalline coke suitable for manufacturing of graphite electrode of large diameter having co-efficient of thermal expansion lower than 1.1×10−6/° C. measured on graphite artifact in the temperature range of 25 to 525° C.
Owner:INDIAN OIL CORPORATION
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