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5839results about How to "Less impurities" patented technology

Method for preparing nano-silver wire with high length-diameter ratio

The invention provides a method for preparing a nano-silver wire with high length-diameter ratio. At least one polyhydroxy liquid organic (1), silver nitrate (2), polyvinylpyrrolidone (PVP) with a K value equal to or larger than 30 (3), at least one hydrogen nitrate compound or one hydrogen-containing compound (4) and at least one chloride for a reaction solution, wherein the chloride can be dissolved in the polyhydroxy liquid organic and can produce chloride ions after dissolved. Reaction is perform for more than 10 minutes under the condition that the reaction temperature is lower than the boiling temperature of the polyhydroxy liquid organic or a part of ingredients is subjected to chemical reaction to form a nano-silver wire solution containing length-diameter ratio exceeding 200, and solid-liquid separation is performed to obtain the nano-silver wire or nano-silver wire dispersing liquid. The nano-silver wire prepared by means of the method is high in length-diameter ratio and yield, few in impurities and good in thickness and length uniformity, and the shortcomings including complicated preparing technology process by means of a traditional polyol method, many impurities and non-uniformity by means of a microwave method and the like are overcome.
Owner:JIANGSU NANOWELL ADVANCED MATERIALS SCI&TECH

Method for preparing length-diameter-ratio nano-silver wire by pH-value regulation solvothermal method

The invention relates to a method for preparing a length-diameter-ratio nano-silver wire by a pH-value regulation solvothermal method. The method comprises the following steps of: preparing the following ethylene glycol solution, namely an ethylene glycol solution A of silver nitrate or silver acetate, an ethylene glycol solution B of polyvinyl pyrrolidone (PVP), an ethylene glycol solution C of water-soluble chloride and concentrated acid D; mixing the components according to a certain amount and fully stirring to form a final mixed solution; moving the final mixed solution into a reaction kettle; placing in an oven for reaction for a certain time; taking the reaction kettle out and cooling to room temperature to obtain mother liquid of the nano-silver wire; adding alcohol into the mother liquid for diluting, and removing supernatant liquor to obtain a precipitate; and repeatedly performing centrifugal separation, and thus obtaining nano-silver wire dispersion liquid uniformly dispersed in the alcohol. The method is simple, high in efficiency and low in cost, and can prepare high-quality nano-silver wires within a wider range of reaction condition; and prepared products are high in length-diameter ratio, good in length uniformity and low in impurity content.
Owner:JIANGSU NANOWELL ADVANCED MATERIALS SCI&TECH

Method for preparing and transferring graphene transparent film

The invention discloses a method for preparing and transferring a graphene transparent film. The technical problem required be solved is that impurities, cracks and bumps after the graphene transparent film is transferred are required to be reduced. The preparing and transferring method disclosed by the invention comprises the steps of: carrying out chemical vapor deposition on the graphene film on a metal substrate, coating methyl methacrylate or photoresist to form a support layer; electrolyzing the graphene film and separating the metal substrate; and coating the methyl methacrylate or photoresist on the support layer, putting the support layer into acetone solution, and attaching the graphene film to an appointed substrate. Compared with the prior art, the film composed of the graphene film and the support layer is separated from the metal substrate by an electrochemical foaming method; the graphene film is transferred to an appointed substrate and then the graphene film well contacts the plane of the appointed substrate without the cracks by spin coating for second time; the metal substrate can be repeatedly used, and the cost of preparation of the graphene transparent film is reduced; the transferred graphene film is well contacted with the substrate, and the impurities are relatively few.
Owner:BTR NEW MATERIAL GRP CO LTD

Rectification tower automatic control and optimization method

The invention relates to a method for controlling and optimizing the distillation tower. It controls the distillation tower in dependence on the material balance relation and component balance relation, optimizes the distillation tower by using representative model. Employing the abstraction proportion between the light product on the top of the tower and heavy product in the bottom of the tower (in following, taking the proportion between light and heavy product for abbreviation) as main controlled variable depending on the distillation principle, the material balance and component balance in the distillation tower, controlling the proportion between the light and heavy product, temperature, reflux ratio to realize stable operation by regulating the quantity of reflux and heat load of re-boiler. Simulating the practical course through the technological process simulation software, and training the nerve net model to become the representative model for the course optimization. Optimizing the operation with the representative model by using the analytical data for the raw material and product to realize the product Ka bian optimization, increasing the productivity of product with high value on the condition of guaranteeing the product quality and realizing the device energy saving and consumption reduction.
Owner:TSINGHUA UNIV

Shielding longitudinal watertight degaussing cable and production method thereof for ships

The invention discloses a shielding longitudinal watertight degaussing cable and a production method thereof for ships. A tinned copper wire is impregnated with a sealant and then twisted into a twisted copper conductor which is impregnated with a conductor sealant layer on the periphery, an electro-insulating rubber layer is extruded on the periphery of the conductor sealant layer to form insulation core wires, chloroprene rubber filling bars are filled into gaps between the insulation core wires, and a plurality of insulation core wires are twisted wholly into a cable core. A cable core inner sealant layer, an inner jacket rubber layer, an armor shielding layer and an outer jacket rubber layer are sequentially arranged on the periphery of the cable core. A single wire of the cable conductor is impregnated with the sealant, the twisted copper conductor is impregnated with the conductor sealant layer on the periphery, the cable core inner sealant layer is extruded on the periphery of the cable core to form multiple sealing, the chloroprene rubber filling bars swell during follow-up vulcanization and can fill in the gaps inside the cable core completely, and tangency between the insulation core wires can be avoided, so that the sealant can permeate to the inside of the cable core to guarantee the watertight effect when the cable core inner sealant layer is extruded.
Owner:嘉兴顾翔制冷设备有限公司

Stable nanometer silver colloidal sol and preparation method thereof

The invention relates to a stable nanometer silver colloidal sol and a preparation method thereof. The stable nanometer silver colloidal sol adopts a silver containing compound, a protective agent and a solvent, water is used as the solvent, and the silver containing compound, the protective agent and the water are mixed so as to prepare the colloidal sol; and the particle diameters of nanometer silver grains are 1nm-10nm, and the nanometer silver grains are uniformly distributed in the colloidal sol, and can be preserved for 6 months to 24 months without changing at room temperature. The preparation method provided by the invention comprises the following steps of: adopting the silver containing compound and the protective agent as raw materials, adopting the water as the solvent, mixing the silver containing compound, the protective agent and the water so as to form a mixed solution which contains 200-10000ppm of silver, 0.02%-1% of protective agent, and the balance of water according to weight percent; and dissolving and mixing the components when the stable nanometer silver colloidal sol is prepared, then uniformly stirring, conducting ultrasonic processing, using a light source containing ultraviolet rays to light 30 minutes to 24 hours to obtain the nanometer silver colloidal sol containing the nanometer silver grains. The stable nanometer silver colloidal sol and the preparation method thereof provided by the invention have the advantages that the cost is low, the process is simple, and the stable nanometer silver colloidal sol is suitable for large-scale preparation.
Owner:WUHAN KANGYIN GAOKE

Nano-material mixed modified superhigh-temperature high-performance well cementing slurry system and preparation method thereof

The invention relates to a nano-material mixed modified superhigh-temperature high-performance well cementing slurry system and a preparation method thereof. The slurry system comprises the followingingredients in parts by weight: 100 parts of oil well cement, 15-25 parts of coarse silica sand, 15-20 parts of fine silica sand, 1-10 parts of nano-silicon dioxide, 1-10 parts of nano-calcium carbonate, 0.2-1 part of a defoaming agent, 4-10 parts of a fluid loss agent, 0-3 parts of a drag reduction agent, 0.5-4 parts of a retarder and 30-100 parts of water. In the slurry system, set cement has excellent compressive strength and toughness under superhigh temperature, and the compressive strength and the elasticity modulus cannot be obviously changed as the maintenance time is prolonged. The slurry system has good rheological property, lower water loss and proper thickening time, and the comprehensive properties of the slurry system can completely meet the related requirements of site wellcementing construction, so that the technical support is provided for well cementing under high temperature. A nano-material obtained by mixing the nano-silicon dioxide and the nano-calcium carbonateis added, and micropores of the set cement can be effectively filled, so that the system becomes denser. Therefore, the volume shrinkage of the set cement is relieved.
Owner:CHINA UNIV OF PETROLEUM (EAST CHINA)
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