961 results about "Ethylene glycol" patented technology

This invention discloses a method for improving the yield of urea phosphate in the preparation of wet-process phosphoric acid. The method involves mixing a crystallizer with wet-process phosphoric acid and urea, reacting the mixture, and then cooling, crystallizing, filtering, and drying to obtain urea phosphate. Alternatively, wet-process phosphoric acid is mixed with urea and reacted. After the reaction, a crystallizer or a urea phosphate mother liquor containing the crystallizer is added, followed by cooling, crystallizing, filtering, and drying to obtain urea phosphate. The crystallizer is one or a mixture of two or more of ethylene glycol methyl ether, ethylenediaminetetraacetic acid, and citric acid in any proportion. The urea phosphate produced by this method is in crystalline form, meeting the industrial urea phosphate standard (GB / T27805-2011), satisfying market demand, and featuring a low-cost crystallizer with flexible addition methods, making it very convenient for practical production.

The application discloses a liposome of a FOXO1 inhibitor AS1842856 and a preparation method and application thereof. The liposome comprises the following raw materials: phospholipid, cholesterol, phospholipid PEG derivative and AS1842856; wherein the proportion of the phospholipid, the cholesterol and the phospholipid PEG derivative (for example, distearoyl phosphatidyl ethanolamine-polyethylene glycol 2000 (DSPE-PEG2000)) is preferably in the range of 10:0.2-2:0.5-5 (w / w); wherein the AS1842856 is wrapped in the liposome. The AS1842856 liposome of the application has excellent physical and chemical properties and has a wide application prospect in the field of fibrosis disease treatment.

To provide an inkjet ink that can be adjusted to an appropriate viscosity range and has excellent properties such as continuous and intermittent printing capabilities. [Solution] An inkjet ink is provided comprising a solvent containing a first solvent which is a glycol ether and a second solvent which is an alcohol having C1 to C3 carbon atoms, and a polyvinyl acetal resin, wherein the ratio of the second solvent to the total amount of the solvent is 5% by mass or more and 50% by mass or less. The first solvent may be propylene glycol monomethyl ether.

Materials for use in a 3D printer, including: several metal particles with an average cross-sectional length of less than or equal to 100 nm; and a stabilizing material comprising an organoamine, carboxylic acid, thiol and derivatives thereof, xanthogenic acid, polyethylene glycols, polyvinylpyridine, polyvinylpyrrolidone or a combination thereof; the metal particles and the stabilizing material agglomerate to form particles with an average cross-sectional length of about 1 µm to about 250 µm.

This invention belongs to the field of carbon dioxide reduction technology, and relates to an oxygen-resistant photocatalytic reduction catalyst for carbon dioxide, its preparation method, and its application. The catalyst synthesis steps are as follows: Bi(NO3)3·5H2O is dissolved in a mixed solution of ethylene glycol and deionized water to obtain solution A; KBr is dissolved in ethylene glycol to obtain solution B. Solutions A and B are sonicated separately for half an hour, then mixed and transferred to a round-bottom flask, and stirred and heated at 100℃~200℃ for 1h~10h. After cooling to room temperature, the precipitate is collected by centrifugation, washed and soaked, and then heated and dried overnight to obtain BiOBr-V. O -X-ray photocatalyst. The BiOBr-V prepared in this invention O X-ray photocatalysts have high oxygen resistance, high catalytic efficiency and CO selectivity, and can use natural light as a light source to directly utilize CO2 in the air without further separation and purification.

The application provides a high-styrene solution polymerized styrene-butadiene rubber and a preparation method and application thereof, and the preparation method comprises the following steps: mixing styrene, butadiene, an initiator, a structure regulator and a non-polar solvent, and performing a polymerization reaction to obtain solution polymerized styrene-butadiene rubber; wherein the structure regulator comprises at least two of t-butoxy sodium, t-amyl oxy sodium, 2,3-dimethyl-3-pentanol sodium and ethylene glycol disodium, and a crown ether. By using the composite structure regulator, the application can prepare a random high-styrene content solution polymerized styrene-butadiene rubber, and the rubber almost does not contain styrene blocks, and the content of vinyl in the rubber can be adjusted by the addition amount of the structure regulator. Therefore, the solution polymerized styrene-butadiene rubber prepared by the application has good strength and hardness due to the high styrene content, and the random microstructure reduces the glass transition temperature and heat build-up of the raw rubber, and is suitable for the manufacturing of high-performance tires such as new energy vehicle tires.

The application relates to the technical field of shoe sole materials, in particular to a foamed composite material and application of the foamed composite material in shoe materials, which comprises EVA resin, ethylene-propylene-diene rubber, wear-resistant particles, a filler, a foaming agent, a crosslinking agent, a lubricant and an activator; wherein the wear-resistant particles are modified porous corundum, which is obtained by in-situ ring-opening polymerization of flexible PCL chains in and outside the pores of the porous corundum after surface activation; and the flexible PCL chains further have polyethylene glycol-stearic acid polymer brushes. Compared with the prior art, the application has the beneficial effects that: the EVA provides good processability and elasticity, the ethylene-propylene-diene rubber endows the material with excellent low-temperature performance and aging resistance; the corundum core of the modified porous corundum provides a high-hardness wear-resistant framework, significantly reduces the abrasion amount in a unit volume, the polycaprolactone main chain and the polyethylene glycol-stearic acid side chain compensate the rigidity of the corundum, and guarantee the high resilience, especially the low-temperature resilience, of the EVA material.

The present application belongs to the technical field of adsorbing materials, and particularly relates to a titanium dioxide molecular imprinting polymer as well as a preparation method and application thereof. The present application uses Sudan red as a template molecule, acrylamide as a functional monomer, ethylene glycol dimethacrylate as a crosslinking agent, and azobisisobutyronitrile as an initiator to construct a cavity structure matching the Sudan red molecule on the surface of the amino-modified titanium dioxide ultrafine particles, and successfully prepares the titanium dioxide molecular imprinting polymer. The material combines the photocatalytic characteristics of the titanium dioxide and the selective recognition ability of the molecular imprinting, can degrade the Sudan red under light, and has a higher photocatalytic efficiency than that of the pure titanium dioxide. The material synthesized through the surface imprinting technology has a three-dimensional cavity complementary to the template molecule, and has a larger adsorption capacity than that of the non-imprinted material. The material realizes the integration of the selective recognition, adsorption and degradation of the Sudan red, and is suitable for complex industrial environments.

The application discloses a method for alcoholysis of waste PET polyester, which comprises the following steps: dissolving waste PET polyester in ethylene glycol, contacting with a catalyst, and reacting to obtain bis(hydroxyethyl) terephthalate; the waste PET polyester is at least one selected from waste PET packaging bottles, waste PET films and PET fiber waste; the catalyst is composed of a metal oxide carrier and active metal oxides loaded on the surface of the metal oxide carrier; the metal oxide carrier is at least one selected from ZnO, gamma-Al2O3, Fe3O4, SiO2, TiO2, CeO2 and MgO; the active metal oxides are at least one selected from MnO2, Co2O3, CeO2, PbO, CuO, NiO and SnO2; the mass of the active metal oxides is 5-60 wt% of the mass of the catalyst, wherein the mass of the active metal oxides is the mass of metal elements contained therein.

This invention discloses a Cu2O / Cu3VO4 heterojunction catalyst, its preparation method, and its application in the photocatalytic reduction of CO2 to multi-carbon products, belonging to the field of catalyst materials technology. The preparation method includes: dissolving a copper source and a vanadium source in water to obtain a solution; mixing the solutions and adjusting the pH to 5-8 to obtain an initial solution; dispersing the solid from the initial solution after centrifugation in a mixture of ethylene glycol and water; and performing a hydrothermal reaction at 150-200℃ for 8-12 hours; washing and drying the reactants, and then calcining them at 500-600℃ for 2-5 hours under an inert atmosphere to obtain the Cu2O / Cu3VO4 heterojunction catalyst. In this catalyst, Cu2O and Cu3VO4 form a closely contacted heterojunction structure, enabling efficient separation of photogenerated electrons and holes under a built-in electric field and enhancing the absorption of visible light. Under visible light irradiation, this catalyst can reduce CO2 to multi-carbon products such as CO, CH4, C2H4, and C2H6, with an electron selectivity of up to 79% for the C2 products. The preparation process of this invention is simple and low-cost, and the resulting catalyst has broad application prospects in the field of photocatalytic CO2 reduction.

The application provides a coated white surface kraft paper with a back surface not easy to drop hair and powder and a preparation method thereof, and relates to the field of coated white surface kraft paper. The preparation method of the coated white surface kraft paper with a back surface not easy to drop hair and powder comprises the following steps: preparing a coating liquid, primary sizing and secondary coating. The coating liquid is prepared from the following raw materials: heavy pulp calcium, kaolin, starch, butadiene styrene latex, polyvinyl alcohol, sodium carboxymethyl cellulose, water-based epoxy silane, ethylene glycol diglycidyl ether and amino silicone oil. The preparation method can ensure that OCC waste paper boxes are effectively recycled for the back surface of the coated white surface kraft paper, and can overcome the problems of hair and powder dropping and adhesive residue on the back surface of the coated white surface kraft paper, so as to avoid the secondary transfer of hair, powder and adhesive on the back surface of the coated white surface kraft paper to the front surface of the paper, and to ensure the printing effect and printing efficiency of the coated white surface kraft paper.

The present application provides compositions and methods for treatment of ocular inflammatory conditions, dry eye diseases, and abnormal corneal neovascularization, using etiprednol. In one example, a composition is provided comprising a semi-fluorinated alkane compound such as, e.g., perfluorohexyloctane; and an additive selected from paraffin, propylene glycol diacetate (PGD), a hydroxyalkyl ester of an aliphatic fatty acid, a hydroxyacid alkyl ester, an alkyl ester of a fatty acid, phenethyl alcohol, ethanol, isopropanol, glycerol, propylene glycol, polyethylene glycol, n-butanol, or combinations thereof. Eye drops comprising the compositions are also provided. Methods of using the compositions are also provided and include methods for reducing one or more symptoms of ocular inflammatory conditions, dry eye diseases, or abnormal corneal neovascularization.

This invention discloses a polyethylene glycol-modified magnesium boride nanosheet and its application in treating acute liver failure and hepatic encephalopathy caused by acetaminophen. The nanosheet uses magnesium boride nanosheets as a core, with polyethylene glycol modified on the surface to improve biocompatibility. The nanosheet of this invention exhibits good antioxidant properties and can be used to prepare nanomedicines for treating acute liver failure and / or hepatic encephalopathy caused by acetaminophen. It generates reducing hydrogen gas through a hydrolysis reaction, effectively scavenging reactive oxygen species at the site of liver failure, thereby inhibiting inflammatory responses and effectively alleviating symptoms caused by acute liver failure.

This invention discloses a method for preparing polyethylene cyclohexanedicarboxylate (PECCHD) from waste PET. Specifically, it relates to a solvent composition for dissolving PET, characterized in that the solvent composition comprises a first solvent and a second solvent; the first solvent is a haloalcohol solvent or a cyclic ether solvent; the second solvent is one or more of a cyclic ether solvent, a chain ether solvent, a nitrile solvent, a ketone solvent, or a haloalkane solvent; the chain ether solvent is a chain ether solvent with 2-4 oxygen atoms; the volume ratio of the first solvent to the second solvent is 1:(1-5); the first solvent and the second solvent are not the same solvent. This method has significant advantages in terms of raw material adaptability, reaction efficiency, and industrialization potential, achieving a highly efficient conversion from low-end waste PET to high-value-added PECHD.

This invention belongs to the field of new material preparation and application, specifically relating to a silicon carbide support and its application in hydrogenation catalysts. Using water glass as the silicon source, the pH of the water glass is adjusted to 7.0 with 10% dilute nitric acid. After filtration, washing, and further filtration, a slurry is obtained. Then, methylcellulose is used as the carbon source and mixed with the slurry. After drying, it is calcined at high temperature in a flowing inert atmosphere to form stable carbon-containing silicon carbide powder. Then, methylcellulose is used as a binder for kneading and extrusion molding, followed by high-temperature calcination in air to obtain the desired silicon carbide support. This SiC support has a high specific surface area and, when used in the preparation of hydrogenation catalysts, can effectively reduce the sulfuric acid color of octanol (octenal hydrogenation product) and effectively improve the ultraviolet light transmittance of ethylene glycol (ethylene glycol hydrogenation refining product).

This invention discloses a method for preparing a Schiff base corrosion inhibitor for AZ91D magnesium alloy coolant. The method involves adding an ethanol or acetone solution of the ketone-containing heterocyclic compound dropwise to an aqueous solution of the alkaline amino acid at a molar ratio of 1:1 to 1.5. The reaction is carried out at 40–80°C for 4–36 hours, followed by concentration, extraction with glacial ethyl acetate, washing with glacial ethyl acetate, and drying to obtain the corrosion inhibitor. Further, the corrosion inhibitor is formulated into a coolant specifically for AZ91D magnesium alloy. This coolant is composed of a mixture of raw materials with the following weight percentages: 0.1–2% corrosion inhibitor, 39–60% deionized water, and 39–60% ethylene glycol. This invention features a simple preparation process, and the obtained corrosion inhibitor can be stored for a long time, exhibits good thermal stability, strong oxidation resistance, low conductivity, high corrosion inhibition efficiency, and good corrosion inhibition effect on AZ91D magnesium alloy.

An oil-in-water microemulsion comprising water; an oil selected from an ester oil, a triglyceride, or combinations thereof; a liquid non-ionic surfactant having an HLB from 7 to 13, preferably, from 9 to 13, and more preferably, from 9 to 11; and a polyethylene glycol / polypropylene glycol / polyethylene glycol triblock polymer having an HLB value from 15 to 29, preferably, 15 to 28, and more preferably, 16 to 27, wherein the microemulsion is transparent and mono-phasic, and wherein the pH of the microemulsion is from 4.5 to 7.5, preferably, from 5 to 7, and more preferably, from 5.5 to 7.

The present disclosure relates to ionic copolymers and terpolymers derived from monomers such as 1-alkyl-3-vinylimidazolium halides, 1-vinylimidazole, acrylamide, n-vinylpyrrolidone, and poly(ethylene glycol) methyl ether methacrylate, and their use as corrosion inhibitors in process streams in industrial systems, more specifically in oil refinery streams. The corrosion inhibitors function at concentrations below 100 ppm, temperatures up to 60° C., and in the presence of congenital waters or synthetic brines.

This invention relates to the field of organic synthesis technology, specifically to a highly efficient and stable Grignard preparation and its green preparation method. By weight, it comprises 8-18 parts of a magnesium source, 40-92 parts of a halogenated hydrocarbon, 150-200 parts of a green solvent, 15-20 parts of ethylene glycol dimethyl ether, and 2.3-3.2 parts of a synergistic stabilizer. The green solvent is 2-methyltetrahydrofuran, or a composite solvent with a weight ratio of 2-methyltetrahydrofuran:methyl tert-butyl ether of 150-160:40-50. The synergistic stabilizer is composed of 1.5-2.0 parts of N,N,N',N'-tetramethylethylenediamine and 0.8-1.2 parts of butylated hydroxytoluene, or composed of 1.5-2.0 parts of N,N,N',N'-tetramethylethylenediamine and 1.0 part of phenothiazine. This invention uses a green solvent system to replace traditional toxic and harmful solvents, and combines it with a solvent recovery process to achieve solvent recycling, which greatly reduces waste emissions and makes the production process safer and more environmentally friendly, in line with the development direction of green chemical industry.

The application discloses a water-based zinc ion battery electrolyte, a preparation method and application thereof. The water-based zinc ion battery electrolyte contains a zinc salt, ethylene glycol ether and water. The zinc salt is selected from at least one of ZnSO4, ZnCl2 and Zn(OTf)2. In the water-based zinc ion battery electrolyte, the mass content of the ethylene glycol ether is 1-20 wt%. The concentration of the zinc salt is 3M.

The invention relates to a multilayer electrocatalyst (2) for the electrochemical conversion of CO2 to ethylene glycol, comprising a first catalyst layer (4) for the electrochemical reduction of CO2 to CO, a second catalyst layer (6) for the conversion of CO to ethene and a third catalyst layer (8) for the electrocatalytic conversion of ethene to ethylene glycol.

The application discloses a leakage-proof long-service-life energy storage battery cooling concentrate as well as a preparation method and application thereof. The leakage-proof long-service-life energy storage battery cooling concentrate comprises the following components: ethylene glycol, a surface tension improver, a buffer, a benzotriazole compound and an organic acid. The cooling concentrate has excellent heat conduction performance, metal corrosion resistance, acid resistance, leakage prevention performance and super-long service life, and the cooling concentrate also has good environmental protection performance. By using the cooling concentrate, the performance and service life of the energy storage battery can be effectively improved, the operation and maintenance cost is reduced, and a powerful guarantee is provided for the safe and stable operation of a power system.

The application relates to a preparation method of a nano WC-Co-based composite powder with inhibitor uniform distribution, and belongs to the technical field of powder preparation. In the application, tungsten oxide and cobalt oxide with large brittleness are used as raw materials, the raw materials are easily broken in a ball milling process, the superfine and nano particle size of a precursor mixed powder containing an inhibitor and the uniform distribution of the raw materials are ensured, the precursor of the inhibitor is dissolved in anhydrous ethanol, a solution is formed, and the solution is mixed with other raw materials, so that the uniform distribution of the component of the inhibitor element in the precursor mixed powder containing the inhibitor is ensured. Polyethylene glycol is added in the ball milling process, the agglomeration of powder particles is reduced, the friction between the powder particles is reduced, and the flowability of the particles is increased. Through the matching of precursor components, the density of the mixed powder of the inhibitor-containing compact and a stage-by-stage heating process, the full reaction of the compact is ensured, the rapid discharge of generated gas is ensured, and through the further ball milling treatment of the prepared powder, the powder is ensured to have the characteristics of pure phase, small WC particle size and uniform component distribution.

The application discloses a kind of multistage synergic covalent grafting type hydrolysis-resistant self-cleaning PET submarine cable monofilament and preparation method, the monofilament includes three parts of core layer, skin layer and surface layer, the core layer is the high viscosity polyethylene terephthalate resin containing carbodiimide anti-hydrolysis agent;Skin layer is the modified PET resin of functional polysiloxane covalent grafting, wherein the functional polysiloxane has epoxy end group or isocyanate end group, and main chain has Si-H group;Surface layer is the fluorine-free low surface energy layer formed by polyvinyl long side chain alkane polysiloxane and residual Si-H group in skin layer through hydrosilylation reaction.The application significantly improves the durability of monofilament in humid heat environment, so that it is suitable for long-term humid heat service environment such as marine cable and industrial fabric, and can maintain stable mechanical strength and self-cleaning performance for a long time.

A polyester resin composition is disclosed, comprising polybutylene terephthalate resin (A) and polyethylene terephthalate resin (B), wherein the amount of terminal hydroxyl groups of the aforementioned polybutylene terephthalate resin (A) is 30-70 mmol / kg relative to the total amount of the aforementioned polybutylene terephthalate resin (A) and the aforementioned polyethylene terephthalate resin (B).

A liquid additive composition comprising a particulate material, an organic carrier fluid, a deflocculant, and optionally a viscosifier and / or a surfactant; wherein the particulate material is substantially insoluble in the organic carrier fluid, and wherein the organic carrier fluid comprises a glycol and / or a glycol ether. A method comprising (a) contacting a particulate material, an organic carrier fluid, a deflocculant, and optionally a viscosifier and / or a surfactant to form a mixture; and (b) agitating the mixture to form the liquid additive composition.