The invention relates to a method for preparing a carbon nanoparticle/two-dimensional layered titanium carbide composite material. The method includes the steps that a two-dimensional layered titanium carbide nano material MXene (Ti3C2/Ti2C) is prepared through hydrofluoric acid corrosion; the material MXene (Ti3C2/Ti2C) and monosaccharide are processed through ultrasonic treatment, vacuum impregnation, hydrothermal treatment and other steps, so carbon nanoparticles are generated between layers and on the surface of the MXene (Ti3C2/Ti2C) material, and the carbon nanoparticle/two-dimensional layered titanium carbide composite material is obtained. Raw materials which are not toxic and easy to obtain are adopted, the preparation process is simple, the technology is controllable, cost is low, repeatability is good, the layered structure of the prepared two-dimensional layered MXene (Ti3C2/Ti2C) is uniform and complete, the carbon nanoparticles are evenly distributed between the layers and on the surface of the MXene (Ti3C2/Ti2C) material, and the prepared composite material has the advantages of being large in specific surface area, good in conductivity, good in hydrophilic property and the like and can be used in the fields such as functional ceramic, wave-absorbing materials, supercapacitors and ion batteries.