348 results about "Nanodiamond" patented technology

The invention relates to a nano-diamond coating, a coating and application thereof, and belongs to the technical field of coatings and surface engineering. The nano-diamond coating provided by the invention is prepared from the following raw materials: resin, a curing agent and organic fluorosilane modified nano-diamond, the organic fluorosilane modified nano-diamond is prepared from raw materials including organic fluorosilane and nano-diamond. According to the invention, the organic fluorosilane is adopted to modify the nano-diamond, the unique physicochemical characteristics of the nano-diamond can be utilized to construct a firm and wear-resistant coating, and the application limitation of the existing amphiphobic coating, especially a super-amphiphobic coating, is broken through; meanwhile, the nano-diamond can spontaneously migrate to the surface in a resin system through modification of the organic fluorosilane, the surface of the coating is endowed with amphiphobic performance and even super-amphiphobic performance, the paint and the coating which are excellent in wear resistance, self-cleaning performance, corrosion resistance and antifouling performance are finally obtained, the preparation process is simple and rapid, and the preparation method is suitable for industrial production. The cost is low, and large-scale production can be realized.

The invention discloses a self-dispersing nano-diamond reinforced coating as well as a preparation method and application thereof, and belongs to the technical field of protective coatings. The self-dispersing nano-diamond reinforced coating provided by the invention comprises a component A and a component B. The component A comprises the following components in parts by mass: 15-35 parts of epoxy resin, 1-30 parts of nano-diamond, 5-15 parts of a solvent and 0.5-1 part of a defoaming agent; and the component B comprises the following component in parts by mass: 2-15 parts of a curing agent. The coating is simple in ingredient, has good effects in adhesive force, impact strength, flexibility, neutral salt spray test and alkaline soaking, is a multifunctional transparent coating with corrosion resistance, wear resistance and antifouling performance at the same time, and has wide application scenes and practical value.

The invention relates to a chip integrated heat dissipation system and a preparation method thereof, and belongs to the technical field of heat dissipation of semiconductor devices. The chip integrated heat dissipation system comprises a nano-diamond transition layer attached to a chip. A micro-column array supporting layer is arranged on one side, far away from the chip, of the nano-diamond transition layer; the micro-column array supporting layer is in contact with one surface of the diamond film, and the other surface of the diamond film is attached to the three-dimensional micro-channel heat dissipation layer. The invention also provides a preparation method of the chip integrated heat dissipation system. The chip integrated heat dissipation system provided by the invention has the advantage of efficient heat dissipation, and through the combination of the three-dimensional structure and the high heat conduction characteristic of diamond, the heat dissipation power density is remarkably improved, the junction temperature of the chip is reduced, and the heat dissipation requirement of a high-power device is met. The heat dissipation performance reliability is high, the thermal stress is eliminated through the gradient structure design, the interlayer binding force is improved, and the stable performance is still kept after multiple thermal cycles. And the preparation process is good in compatibility and convenient for large-scale production.

Luminescent diamond is made by subjecting a volume of diamond grains to high-pressure / high-temperature conditions with or without a catalyst to cause the grains to undergo plastic deformation to produce nitrogen vacancy defects in the diamond grains, increasing the luminescent activity / intensity of the resulting diamond material. The consolidated diamond material may be further treated to further increase luminescent activity / intensity, which treatment may comprise reducing the consolidated diamond material to diamond particles, heat treatment in vacuum, and air heat treatment, which reducing process further increases luminescent activity / intensity. The resulting luminescent diamond particles display a level of luminescence intensity greater than that of conventional luminescent nanodiamond, and may be functionalized for use in biological applications.

The invention relates to the technical field of biomedical materials, and discloses a thrombectomy stent support material and a preparation process thereof, the thrombectomy stent support material comprises the following components by mass: 60-70% of a polysebacic diglyceride prepolymer; 25-35% of a dynamic covalent bond cross-linking agent; 5%-10% of carboxylated nano-diamond; 3 to 5 percent of temperature-sensitive and photo-thermal dual-response microspheres; the dynamic covalent bond cross-linking agent is composed of 4-formyl phenylboronic acid and hexamethylenediamine according to a molar ratio of 1: (1-3); the microsphere is prepared from poly (N-isopropylacrylamide), a gold nanorod and a recombinant tissue type plasminogen activating agent, and by combining a low-temperature 3D printing technology, the material can form a complex bionic structure, the mechanical strength is dynamically adjusted along with the physiological environment after implantation, and the material is safely degraded after functions are completed. The material is suitable for the scenes of cardiovascular and cerebrovascular stents, bone repair instruments and the like, has treatment accuracy, manufacturing suitability and clinical safety, and solves the problems of non-degradability, sudden drug release, mechanical mismatch and the like of traditional implants.

The invention belongs to the technical field of catalyst preparation, and provides an M2 diatomic site catalyst for a reaction for preparing phenylenediamine through dinitrobenzene hydrogenation and a preparation method and application thereof.The catalyst is formed by anchoring transition metal M diatomic sites to the surface of a diamond-graphene carrier and is prepared by taking nano-diamond powder as a raw material through a one-step reaction. Annealing treatment is carried out at the high temperature of 750-850 DEG C, a diamond-graphene carrier of an sp3 atsp2 core-shell structure is constructed, and the surface defect density of the diamond-graphene carrier is regulated and controlled in the process; and depositing metal species on the surface of the carrier through ALD double-step deposition to obtain the M2 diatomic site catalyst with high density and stable structure. The M2 diatomic site catalyst is applied to a reaction for preparing a corresponding phenylenediamine compound through hydrogenation of a dinitrobenzene compound, and high conversion rate and high selectivity can be achieved with low metal loading capacity under mild conditions. The method can be popularized to construction of diatomic catalysts of various transition metals, and has a wide application prospect.

Luminescent diamond is made by subjecting a volume of diamond grains to high-pressure / high-temperature conditions with or without a catalyst or pressure transfer media to cause the grains to undergo plastic deformation to produce internal vacancy defects, increasing the luminescent activity / intensity of the resulting diamond material. The luminescent material is then subjected to further treatment to create quantum dots on the surface of the diamond particles. Quantum dot formation can include placing the diamond particles in liquid and subjecting the particles to laser pulses. The consolidated diamond material may be treated to further increase luminescent activity / intensity including reducing the consolidated diamond material to diamond particles, heat treatment in vacuum, and / or air heat treatment. The resulting luminescent diamond particles display a level of luminescence intensity greater than that of conventional luminescent nanodiamond, and may be functionalized for use in biological applications.

The present invention discloses a flow type fluorescence detection system, which comprises: a sample flow channel, which is used for conveying a target object specifically bound with a nano-diamond mark, the nano-diamond comprises an NV color center, and the sample flow channel is provided with a detection area; the exciting light module is used for exciting an NV color center of a detection area of the sample flow channel, so that electrons of the NV color center are transited to generate fluorescence; the microwave radiation module is used for providing a microwave field for a detection area of the sample runner; the optical detection module is used for collecting a target material which is specifically bound with the nano-diamond mark at a preset collection frequency, and when the target material flows through the detection area of the sample flow channel, the NV color center in the nano-diamond emits a fluorescence signal of which the intensity is periodically changed by controlling at least one of the intensity, the frequency and the on-off of a microwave field; the fluorescence signal is associated with whether the target contains to-be-detected biomolecules or not. According to the technical scheme provided by the embodiment of the invention, the detection sensitivity of the fluorescence detection system is improved.

The invention relates to the technical field of heat-conducting materials, in particular to a heat-conducting silica gel sheet and a preparation process thereof, and the heat-conducting silica gel sheet is prepared from the following components in parts by weight: 100 parts of organic silicon rubber; 300-500 parts of a heat conducting filler; 3-8 parts of a curing agent; 1-3 parts of a catalyst; according to the invention, a composite system of silicon carbide particles with a specific crystal structure, surface-modified graphene sheets and nano-diamond particles is used as a heat-conducting filler, and the filler is subjected to accurate proportioning and surface treatment, so that not only is the heat-conducting efficiency greatly improved, but also the internal binding force and heat stability of the material are effectively enhanced; compared with a traditional heat-conducting silica gel sheet, the heat-conducting silica gel sheet can more effectively transfer heat and reduce thermal resistance under the same condition, so that the heat dissipation performance and operation reliability of electronic equipment are improved, and in addition, the heat-conducting silica gel sheet has good mechanical performance and machinability and is easy to adapt to various complex application scenes.

The invention discloses a nano-diamond reinforced powder metallurgy brake pad friction body material and a preparation method thereof, and relates to a brake pad friction body material and a preparation method thereof. The problem that in the prior art, the stability of a braking system of a train at a high running speed cannot be achieved is solved. The friction body material comprises a matrix component, a lubricating component, a friction component and a basic reinforcing component, wherein the sum of the mass percentages of the matrix component, the lubricating component, the friction component and the basic reinforcing component is 100%; wherein the mass percent of the copper powder in the matrix component is 50%-70%, and the mass percent of the iron powder in the matrix component is 10%-30%; the mass percent of the lubricating component is 10%-20%; the mass percent of the friction component is 1%-5%; the mass percent of the nano-diamond in the enhanced component is 0.1%-1%; the friction component is composed of one or more of silicon dioxide, aluminum oxide, titanium carbide, tungsten carbide, silicon carbide powder and zirconium oxide powder; the lubricating component is composed of one or more of graphite, carbon nanotubes and molybdenum disulfide. Belongs to the technical field of powder metallurgy.

The present invention relates to a process for preparing diamond particles, comprising subjecting a nanodiamond precursor material to a pressure of at least 8 GPa and a temperature of at least 900°C, wherein the diamond precursor material comprises a polycyclic aromatic compound which contains from 10 to 200 fused six-membered aromatic rings.

The invention discloses a preparation method of GaN / diamond with low interface thermal resistance, and aims to solve the bottleneck problems of interface failure, high interface thermal resistance and the like caused by growth of diamond on a GaN substrate. The preparation method of the GaN / diamond with low interface thermal resistance comprises the following steps of: 1, ultrasonically cleaning a GaN substrate; 2, carrying out reverse sputtering cleaning on the GaN substrate; 3, sputtering and depositing a Si3N4 transition layer on the GaN substrate; 4, ultrasonic cleaning; 5, spin-coating the nano-diamond suspension liquid on the GaN substrate; 6, introducing hydrogen, oxygen and methane gas, and depositing a diamond layer in stages; 7, depositing a diamond layer at a first stage under low pressure; and 8, depositing a diamond layer at a second stage under high pressure. The GaN / diamond material with low interface thermal resistance is prepared through a multi-temperature gradient low-temperature growth process in combination with collaborative optimization of air pressure and time, and gradient heat flow control is combined with stress buffering of the Si3N4 transition layer, so that the integrity of the Si3N4 film is ensured.

The invention relates to the technical field of grinding fluid, in particular to efficient grinding fluid for an MPO connector, a preparation method and application of the efficient grinding fluid for the MPO connector. 27%-44% of alpha-aluminum oxide; 8%-15% of a styrene-maleic anhydride copolymer; 2%-5% of a modified polyurea solution; 0.05% to 0.3% of perfluoropolyether; 0.5%-2% of citric acid; 0.5%-1.5% of a polyether modified polysiloxane defoaming agent; by adopting a composite abrasive material system of the nano-diamond and the alpha-aluminum oxide, the grinding efficiency and the surface quality are improved in a breakthrough manner.

The invention discloses a silicone rubber composite material for enhancing the wear resistance of a tire and a preparation method of the silicone rubber composite material, and belongs to the technical field of silicone rubber materials for tires. The silicon carbide nanofibers directionally bear stress through a one-dimensional structure, the surface friction coefficient is reduced through the layered lubricating characteristic of fluorinated graphene, and crack propagation is inhibited on the micro-level through the synergistic effect of the silicon carbide nanofibers and the fluorinated graphene. The tribological performance is further optimized through compound addition of the polyimide microspheres and the nano-diamond powder, dynamic friction loss is reduced through the ball effect, and the surface scratch resistance is improved through the ultra-high hardness of the nano-diamond powder. Meanwhile, the filler-matrix binding force is enhanced through interface bonding of the sulfydryl modified titanium dioxide quantum dots and the zinc borate nanosheets, abrasive particle falling caused by interface stripping is effectively avoided, and the structural integrity of the material is kept under the long-term dynamic load.

The invention provides a gradient composite graphene electrolysis electrode plate and an in-situ preparation method thereof. The electrode plate comprises a metal conductive base material (such as titanium alloy), a porous ceramic skeleton layer (Al2O3-40% ZrO2, the porosity of which is 30 + / -5%), a chemical copper plating layer for filling pores, an electroplated nickel-ruthenium alloy catalytic layer (Ni: Ru = 9: 1) and 3-5 graphene functional layers (ID / IG is less than or equal to 0.08) grown in situ, wherein the porous ceramic skeleton layer (Al2O3-40% ZrO2) is laser-cladded on the surface of the porous ceramic skeleton layer (Al2O3-40% ZrO2). The preparation method comprises the following steps: performing laser cladding on a ceramic skeleton, wherein the power density is 300-500W / mm < 2 >, and sintering at 1600 DEG C to form metallurgical bonding; gradient plating: electroless copper plating (containing nano-diamond enhancement) and pulse electroplating of Ni Ru (duty ratio is 1: 5); and performing directional CVD growth: after reducing the catalyst layer by H2 at 1050 DEG C, introducing CH4 / H2 (the volume ratio is 1: 4) in a pulse manner, and realizing full coverage of the inner wall of the mesh by vortex air intake. The technical effects are as follows: (1) the overpotential of chlorine evolution in saturated salt water at 80 DEG C is as low as 268mV (1A / cm < 2 >); (2) strong acid environment service life gt; the time is 100 thousand hours (12 times that of the national standard); (3) the production cost is lt; and 620 / m < 2 > (90% lower than that of a traditional ruthenium-iridium coating). The problems of graphene transfer damage and special-shaped electrode covering are solved.

The invention belongs to the technical field of battery cooling liquid, and particularly relates to new energy automobile power battery cooling liquid and a preparation method thereof. The new energy automobile power battery cooling liquid is prepared from the following raw materials in percentage by mass: 40 to 60 percent of dihydric alcohol, 0.2 to 3 percent of a corrosion inhibitor, 0.1 to 0.5 percent of an antioxidant, 0.1 to 0.5 percent of a pH regulator, 0.01 to 0.05 percent of an anti-foaming agent, 0.005 to 0.015 percent of a nano additive and the balance of ionized water, the nano additive comprises an ionic flaky nano mineral, nano palygorskite and nano diamond in a mass ratio of (3-5): (0.1-0.5): (0.1-0.5). The new energy automobile power battery cooling liquid has good low dielectric constant, high thermal conductivity and good storage stability.

The invention discloses a flow-type fluorescence detection method and system based on a zero field. The method comprises the following steps: when a target material specifically bound with a nano-diamond mark flows through a detection area of a sample flow channel, detecting the target material; by controlling at least one of the intensity, the frequency and the on-off of the microwave field, the NV color center in the nano-diamond emits a fluorescence signal with the intensity changing periodically; the magnetic field intensity of the detection area meets the zero field condition, the excitation light module is used for exciting the NV color center of the detection area of the sample flow channel, the microwave radiation module is used for providing a microwave field for the detection area of the sample flow channel, and a microwave radiation signal provided by the microwave field has a fixed frequency; the light detection module collects a fluorescence signal at a preset collection frequency; and the data processing module judges whether the target object contains the to-be-detected biomolecules according to the fluorescence signal. According to the technical scheme provided by the embodiment of the invention, the detection sensitivity of the fluorescence detection method is improved.

The invention relates to the field of high-pressure pressure distribution calibration and imaging, in particular to a high-pressure diamond anvil cell internal pressure calibration / imaging system and method based on wide-field optical detection magnetic resonance. The invention discloses a high-pressure diamond anvil cell internal pressure calibration / imaging system based on wide-field optical detection magnetic resonance. The system comprises a fluorescence excitation and collection unit which comprises a wide-field optical detection magnetic resonance pressure distribution imaging light path based on nano-diamond NV color center fluorescence and a pressure calibration light path based on a ruby microsphere fluorescence spectrum. Compared with the prior art, the technical effects of the invention are that a traditional single-point detection mode is broken through through a wide-field microscopic imaging method, submicron spatial resolution and 0.0045 GPa / Hz1 / 2 noise measurement sensitivity are realized, and a brand new stress field characterization means is provided for a high-pressure experiment.

The invention relates to the technical field of superhard materials, and particularly discloses a polycrystalline diamond compact and a preparation method and application thereof.The preparation method of the polycrystalline diamond compact comprises the following steps that WC-Co alloy powder is sintered to obtain a hard alloy matrix; uniformly mixing nano diamond powder, micron diamond powder and cubic boron nitride, adding a reinforcing agent and a binding agent, and uniformly mixing to obtain a polycrystalline diamond layer mixture; the reinforcing agent is a nitrogen-boron doped graphene bonded amino carbon nanotube; a gradient transition layer raw material and a polycrystalline diamond mixture are uniformly spread on the surface of the hard alloy matrix in sequence, and then a composite blank is obtained through mold pressing; and sintering the composite blank to obtain the polycrystalline diamond compact. Graphene and carbon nanotubes are compounded to form a reinforcing agent with a three-dimensional network structure, so that the strength and wear resistance of the material are improved, and the service life of the material under harsh working conditions is prolonged.

The invention discloses a high-stability magnetic liquid and a preparation method thereof, and belongs to the field of magnetic fluid nano functional materials related to ships. The magnetic liquid comprises a metal-doped iron oxide nano-particle core, a double-layer surface modification layer composed of oleic acid and a silane coupling agent, and a composite carrier liquid formed by compounding poly-alpha olefin synthetic oil and perfluoropolyether and adding nano-diamond. The preparation method comprises the following steps: firstly, coprecipitating and calcining to obtain metal-doped iron oxide nanoparticles, then carrying out double-layer coating modification, and finally carrying out mixed ball milling, ultrasonic treatment and magnetic separation purification on the metal-doped iron oxide nanoparticles and the composite carrier liquid. The saturation magnetization intensity of the magnetic liquid reaches 92-95 emu / g, the magnetic liquid can work for a long time under the high-temperature working condition, the heat conductivity coefficient is increased by 2-3 times, and the redispersibility is excellent. The problems that a traditional magnetic fluid is low in magnetic performance, prone to failure at high temperature, poor in dispersion stability and the like are solved, and the magnetic fluid is suitable for aerospace, high-end manufacturing, ship propulsion and other extreme scenes.

The invention discloses a preparation and application method of a super-lubricating coating based on a two-dimensional material. According to the invention, the charge density wave dynamic regulation and control mechanism of the fluorinated graphene and transition metal chalcogenide heterostructure is combined with the stress buffer characteristic of boron nitride, so that a slip interface with a low shear barrier is constructed on the atomic scale, and the energy dissipation in the friction process is remarkably reduced. A three-dimensional interpenetrating network of the helical carbon nanotubes and the hyperbranched polymer not only effectively inhibits stacking of two-dimensional materials, but also forms a multi-dimensional damage repair mechanism through solid-liquid phase change self-adaptive filling of the liquid metal and a boundary lubrication effect of the nano-diamond. Through the synergistic effect of the material system, the coating keeps the ultralow friction characteristic under the wide-range working condition, meanwhile, the coating has the composite protection capacity of abrasion resistance, high temperature resistance and corrosion resistance, and the intrinsic lubrication characteristic of the two-dimensional material is reserved while the compactness of the coating is guaranteed through the gradient cross-linking technology of ultraviolet curing and heat treatment.

The invention belongs to the field of coatings, and particularly discloses a super-hydrophobic organic coating as well as a preparation method and application thereof. The organic coating comprises the following components: organic resin and organic silicon modified composite particles; the mass ratio of the organic resin to the organic silicon modified composite particles is 1: (0.05-0.2); the composite particles contain nano diamond particles and a carbon material; the particle size of the carbon material is 1-30 [mu] m. A coating layer formed by the super-hydrophobic paint has the characteristics of super-hydrophobic performance and high hardness, the water contact angle of the coating layer is not less than 160 degrees, the water rolling angle of the coating layer is not more than 4 degrees, and the pencil hardness of the coating layer is 5H-7H. In addition, a coating formed by the coating has super-hydrophobic durability, specifically, after a friction experiment, the coating still keeps the super-hydrophobic capacity, the water contact angle is still larger than 150 degrees, and the coating has long service life during application.

The invention relates to the technical field of ceramic tiles, in particular to a sapphire single crystal diamond glaze super-wear-resistant ceramic tile and a preparation method thereof. The sapphire single crystal diamond glaze super wear-resistant ceramic tile is prepared from the following raw materials in parts by weight: high-purity alpha-Al2O3 powder, nano-diamond turbid liquid, rare earth modified zirconium silicate, a gas-phase transport agent, a lattice matching cosolvent and zinc oxide whiskers. According to the invention, the high-purity alpha-Al2O3 epitaxially grows on the surface of the nano-diamond to form an atomic-scale coherent interface, the bonding strength is high, the high hardness of sapphire and the wear resistance of diamond are integrated, the self-sharpening characteristic is endowed to the glaze layer by a micro-scale interlocking structure, a new hard interface is exposed in the wear process, the surface wear resistance is continuously maintained, and the service life of the glaze layer is prolonged. The problem of performance degradation after traditional materials are abraded is solved.

The invention relates to the technical field of electrode preparation, in particular to a diamond electrode and a preparation method thereof. The diamond electrode comprises a porous consolidation block formed by consolidating conductive diamond particles; the particle size of the conductive diamond particles is 0.3-10 mm; the conductive diamond particles comprise diamond particles or diamond particles with diamond coatings deposited on the surfaces; the diamond grains or the diamond coating are electrically conductive by doping elements. On the basis, a nano-diamond porous membrane is deposited on the surface of the porous consolidation block, and the thickness of the nano-diamond porous membrane is 1-20 microns. In addition, the invention further provides a preparation method of the diamond electrode. The diamond electrode provided by the invention has a high specific surface area, and can control pores in the electrode and enable the pores to be exposed in a working environment.

The invention discloses an enhanced multi-network hydrogel electrolyte as well as a preparation method and application thereof, and belongs to the field of aqueous zinc ion batteries. Firstly, oxygen terminal nano-diamond is uniformly dispersed in deionized water to form a mixed solution, then sodium alginate is added to be fully dissolved, and the mixed solution is uniformly dispersed; the oxygen terminal nano-diamond-sodium alginate homogeneous solution is obtained. The solution is mixed with a polyvinyl alcohol solution which is completely molten through water bath heating and a proper amount of glycerol, and all the components are ensured to be uniformly distributed through sufficient stirring. And then, through repeated freezing and thawing and zinc ion cross-linking and curing effects, the oxygen terminal nano-diamond enhanced hydrogel electrolyte with a multi-network structure is finally formed. The oxygen terminal nano-diamond is highly uniformly dispersed in the hydrogel electrolyte, dendritic crystal growth and side reaction are effectively inhibited through a triple synergistic mechanism of enhancing the mechanical strength, reducing the free water content and increasing the zinc ion transference number by surface functional groups, and the super-long cycle stability is achieved.

Luminescent diamond is made by creating vacancies in diamond grains and heat treating the diamond grains by controlling a thickness of the diamond grains on a substrate. The heat treatment may occur in a temperature range that does not burn the diamond grains, and the controlled thickness produces an even color change and / or promotes oxygen terminations on the diamond particle surfaces.

The invention relates to the technical field of preparation of environmental functional materials, and discloses a directional synthesis method of magnetic porous iron-doped graphitized biochar, which is realized by the following steps: cooperatively inducing low-temperature graphitization by utilizing a biomass endogenous S < 2 > self-template and nano-diamond; performing double-complexing ultrasonic impregnation on the iron precursor to realize nanoscale dispersion; performing staged pyrolysis, pre-carbonizing in an inert atmosphere to construct a carbon skeleton, and synchronously completing iron reduction and graphitization in a reducing atmosphere; performing mixed pickling to synchronously remove the template and construct a passivation layer; and finally, carrying out magnetic separation to obtain the high-porosity and uniformly iron-doped magnetic graphitized charcoal. A graphitized porous structure is realized through cooperation of a low-temperature self-template and nano-diamond, iron agglomeration is inhibited through a double-complexing ultrasonic technology, a protective layer and active sites are synchronously constructed through mixed pickling and passivation, and three technical barriers of high-temperature collapse, iron particle inactivation and short cycle life of a traditional process are broken through.

The invention discloses a preparation method of a modified graphite / copper composite heat sink material, and belongs to the technical field of metal-based composite materials. The method comprises the following steps: carrying out acid activation on crystalline flake graphite, modifying the crystalline flake graphite with a silane coupling agent, and selectively stripping to obtain graphite nanosheets; preparing copper-based alloy powder containing at least two carbides of Zr, Cr and Ti; performing graded ultrasonic-ball milling composite dispersion on the surface modified graphite powder, the copper-based alloy powder, the nano-diamond powder, the carboxyl functionalized multi-walled carbon nanotubes and the graphene oxide; gradient filling cold pressing forming and pre-sintering are carried out; performing hot pressing / spark plasma sintering, applying a magnetic field or a vibration field to realize graphite orientation, generating a carbide interface transition layer in situ, and reducing graphene oxide; and after machining, pulse electrodeposition is carried out on the copper-graphene composite coating, and surface micropores / micro textures and phase change material filling can be selectively formed. The method is suitable for efficient heat management of high-power electronic devices.

Provided is an initial break-in lubricant composition capable of easily and economically reducing the coefficient of friction of a sliding portion. The initial break-in lubricant composition includes an organic dispersion medium and nanocarbon particles in a quantity from 0.1 to 2000 ppm by mass. The nanocarbon particles are preferably particles of one or more nanocarbon material(s) selected from the group consisting of: nanodiamonds, fullerenes, graphene oxide, nanographite, carbon nanotubes, carbon nanofilaments, onion-like carbon, diamond-like carbon, amorphous carbon, carbon black, carbon nanohorns, and carbon nanocoils.

The invention belongs to the technical field of diamond micro-powder preparation, and particularly relates to a supporting plate, four supporting rods and a drying box are fixedly connected to the top of the supporting plate, a mixing barrel is fixedly connected to the top ends of the three supporting rods, a conveying barrel is fixedly connected to the top end of one supporting rod, and a stirring motor and a feeding pipe are fixedly connected to the top of the mixing barrel. By arranging a stirring motor and a rotating motor, people can control the stirring motor to operate through an external controller to enable a rotating shaft to rotate, nano-diamond particles and micron-diamond particles can be mixed through a stirring plate, people can control the rotating motor to operate through the external controller to enable a first gear to rotate, and through a second gear, the nano-diamond particles and the micron-diamond particles can be mixed. The rotary shaft and the rotary frame are rotated to drive the placement barrel to rotate, and the mixed materials in the placement barrel can be comprehensively dried through the exhaust fan and the heater, so that the mixing and drying device has higher mixing and drying effects and is more convenient to use.