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453 results about "Transmission electron microscopy" patented technology

Transmission electron microscopy (TEM, an abbreviation which can also stand for the instrument, a transmission electron microscope) is a microscopy technique in which a beam of electrons is transmitted through a specimen to form an image. The specimen is most often an ultrathin section less than 100 nm thick or a suspension on a grid. An image is formed from the interaction of the electrons with the sample as the beam is transmitted through the specimen. The image is then magnified and focused onto an imaging device, such as a fluorescent screen, a layer of photographic film, or a sensor such as a scintillator attached to a charge-coupled device.

Stamping prediction method based on multi-machine learning model and automatic compensation device

The invention relates to the technical field of computer science, in particular to a stamping prediction method based on a multi-machine learning model and an automatic compensation device.The stamping prediction method comprises the steps that firstly, a sheet microstructure and material characteristics are obtained through a transmission electron microscope and an atomic probe tomography technology, and then finite element simulation sampling is conducted; a data set is expanded by using an adaptive algorithm, multiple models are constructed and trained to obtain a final springback prediction model, an automatic compensation device is embedded to realize automatic compensation, and the automatic compensation device covers visual parameter input, embedded springback prediction, springback compensation calculation and an automatic control module. Parameters can be visually input, springback can be accurately predicted, a compensation value can be calculated, and the process can be adjusted. The method aims at solving the problems that in the high-strength plate stamping process, due to springback, the size and shape of a part deviate from the design requirement, and a traditional prediction and compensation technology is insufficient in precision and efficiency.
Owner:GUIZHOU UNIV

Transmission electron microscope low-temperature sample rod using flexible structure for heat transfer

The invention relates to a transmission electron microscope low-temperature sample rod using a flexible structure to transfer heat. The transmission electron microscope low-temperature sample rod comprises a liquid nitrogen Dewar tank; the sample rod comprises a sample rod body with a front-back through hollow cavity, a heat conduction rod and a flexible heat transfer rope, one end of the heat conduction rod extends into the liquid nitrogen Dewar tank, the other end of the heat conduction rod extends into the sample rod body, one end of the flexible heat transfer rope is wound and fixed on the heat conduction rod, and the other end of the flexible heat transfer rope is wound and fixed on the sample rod body. The other end of the sample rod extends to the outer end of the sample rod body; the sample rod head comprises a sample rod fixing outer frame and a sample rod temperature control part, the sample rod fixing outer frame is connected with the outer end of the sample rod body, the sample rod temperature control part is arranged on the sample rod fixing outer frame, the sample rod temperature control part is connected with the flexible heat transfer rope, and a heating element capable of heating a sample to be tested is further arranged on the sample rod temperature control part. Compared with the prior art, efficient heat conduction can be achieved, meanwhile, the thermal stress influence is reduced, and the temperature stability and the sample position stability are improved.
Owner:FUDAN UNIVERSITY

Magnetic tape, magnetic tape cartridge, and magnetic tape apparatus

ActiveUS12249360B2Magnetic tapeFerrite powder
The magnetic tape includes a non-magnetic support, and a magnetic layer containing a ferromagnetic powder. The ferromagnetic powder is a hexagonal ferrite powder, tilt cos θ of the hexagonal ferrite powder with respect to a surface of the magnetic layer, which is acquired by cross-sectional observation performed using a scanning transmission electron microscope, is 0.85 or more and 1.00 or less, and standard deviation σ of the cos θ in a width direction of the surface of the magnetic layer is 0.03 or less.
Owner:FUJIFILM CORP

In-situ TEM device sample preparation method based on suspended thinning and parallel carrying technology

The invention discloses an in-situ TEM (Transmission Electron Microscope) device sample preparation method based on a suspended thinning and parallel carrying technology, which can be used for preparing in-situ TEM samples of semiconductor two-end devices and three-end devices, and mainly solves the problems of unstable ohm contact, nonuniform thinning, low success rate and high time cost in the prior art. According to the invention, an FIB sample preparation technology is adopted, and stable and reliable ohmic contact between a sample electrode and an MEMS chip electrode is ensured through specific-angle sample extraction, suspended thinning, parallel carrying, circuit breaking treatment and an accurate electrode welding process. According to the sample prepared by the invention, the failure state of a device can be observed in real time under a transmission electron microscope, the sample has the advantages of high sample preparation success rate, good repeatability, stable electrical parameters and wide applicable chip variety, and the reliability and repeatability of in-situ TEM test data are remarkably improved.
Owner:XIDIAN UNIV

A controlled-release diabetic wound healing treatment method

The present invention relates to the technical field of diabetes, and in particular to a controlled-release diabetic wound healing promoting treatment method, comprising the following treatment experimental steps: step S1: preparation of Hst1@PNPs; step S2: Coomassie brilliant blue staining; step S3: scanning and transmission electron microscopy detection; in the present invention, a slow-release Hst1 treatment method is constructed by encapsulating Hst1 into platelet membrane vesicles derived from autologous blood. On the one hand, the PNPs encapsulate the linear Hst1 peptide structure to prevent it from being rapidly degraded by high proteases in diabetic wound exudate, thereby improving bioavailability. On the other hand, the PNPs can adsorb excess LPS in the wound exudate, and cooperate with Hst1 to achieve anti-inflammatory and anti-oxidative stress effects. Subsequent cell and animal experiments further confirmed that Hst1@PNPs have the effects of anti-inflammatory, scavenging ROS, promoting re-epithelialization, collagen deposition and angiogenesis, thereby promoting diabetic wound healing.
Owner:DERMATOLOGY HOSPITAL SOUTHERN MEDICAL UNIV (GUANGDONG PROVINCIAL DERMATOLOGY HOSPITAL GUANGDONG PROVINCIAL CENT FOR STI & SKIN DISEASES CONTROL & PREVENTION RES CENT FOR LEPROSY CONTROL & PREVENTION CHINA)

Method for evaluating growth performance of mangrove forest seedlings in estuary high-salinity environment

ActiveCN120509608ADetails involving 3D image dataResourcesMangroveMitochondrial cristae
The invention discloses a method for evaluating the growth performance of mangrove forest seedlings in an estuary high-salinity environment, and the method comprises the steps: constructing an analysis framework in which a dynamic salinity stress system and a multi-dimensional monitoring technology are coupled, and achieving the precise evaluation of the environmental adaptability of the mangrove forest seedlings; the method comprises the following steps: firstly, carrying out sterile germination and matrix domestication on a target estuary provenance, then establishing a three-dimensional stress model containing basic salinity maintenance, sudden salinity impact and tidal cycle fluctuation, and strictly controlling the sudden salinity impact amplitude within 20% of the historical extreme value of the estuary; synchronously acquiring canopy volume and root architecture parameters of the seedlings by adopting a three-dimensional laser scanning technology, and constructing a morphological database in combination with leaf apparent characteristic records; subcellular structure indexes such as cell wall thickening, chloroplast envelope integrity and mitochondrial ridge density are observed and analyzed through a transmission electron microscope, the molecular mechanism of osmotic regulation and energy metabolism is disclosed, and the concentration of suspended solids in the water body, the oxidation-reduction potential of sediments and the functional diversity of microorganisms are synchronously monitored.
Owner:XIAMEN BRANCH OF CCCC THIRD HARBOR ENG

Liquid specimen grid for transmission electron microscope

A grid for sampling a liquid specimen. The grid includes a mesh and a foil. The mesh includes a plurality of grid bars defining a plurality of openings. The plurality of grid bars forms an outer perimeter of each opening. The foil is coupled to the mesh and the foil includes a plurality of holes. A subset of the plurality of holes is aligned with each of the plurality of openings. Each hole of the subset is spaced from the outer perimeter of the corresponding opening defined by the plurality of grid bars.
Owner:FEI CO

Simulation method for studying life period mechanical property of aluminum alloy material for reactor

The invention relates to a mechanical property simulation method for researching the service life of an aluminum alloy material for a reactor. The simulation method for the life period mechanical property of the aluminum alloy material comprises the following steps: S1, preparing initial, middle and last stage aluminum alloy samples according to a < 27 > Al-< 28 > Si transmutation path of the aluminum alloy material; s2, representing the sample by using a transmission electron microscope, obtaining precipitated particle parameters, calculating a volume fraction f, fitting f and operation time t, and constructing a precipitation evolution model f (t); s3, performing high-energy ion irradiation on the sample, and performing nanoindentation experiment and load-depth curve fitting to obtain nano hardness H; s4, based on the f (t), establishing a relation model of the nano hardness H and the irradiation damage D; and S5, calculating the change quantity of the nano hardness H, converting the change quantity into the change quantity of the yield strength, associating the irradiation damage D with the service time T, and establishing a life period yield strength prediction model. According to the method, the mechanical property of the aluminum alloy in the full service cycle of the research reactor can be accurately evaluated.
Owner:SHANGHAI NUCLEAR ENGINEERING RESEARCH & DESIGN INSTITUTE CO LTD +1

Preparation method of transmission electron microscope sample of sintered neodymium iron boron block material

The invention discloses a preparation method of a transmission electron microscope sample of a sintered neodymium-iron-boron block material, which comprises the following steps of block sample cutting, mechanical grinding, sample punching, ring sticking, pre-thinning and final thinning, so that the transmission electron microscope sample to be observed is obtained. In addition, the method is simple, feasible, economical and practical, and the sample preparation success rate can be remarkably increased.
Owner:GUOBIAO BEIJING TESTING & CERTIFICATION CO LTD

Transmission electron microscope sample preparation method for lunar soil space weathered surface and application

The invention discloses a transmission electron microscope sample preparation method for a lunar soil space weathered surface and application, and the method comprises the following steps: pasting target lunar soil particles on a carbon conductive adhesive tape, and enabling the target flat surfaces of the target lunar soil particles to be placed back to the carbon conductive adhesive tape; plating a layer of carbon film on the surface of the target lunar soil particle to obtain a scanning electron microscope sample of the target lunar soil particle; screening out a plurality of target research areas on the carbon film corresponding to the target flat surface; uniformly plating a layer of gold film on the carbon film corresponding to the target lunar soil particle scanning electron microscope sample; deposition operation of a research area protection layer is carried out on the gold film corresponding to the target research area through an electron beam and an ion beam in sequence; and performing slicing operation perpendicular to the target flat surface on the target lunar soil particle scanning electron microscope sample to obtain the target lunar soil particle transmission electron microscope sample. According to the method, lunar soil space weathering characteristics can be truly reserved, and an accurate and reliable sample is provided for lunar soil space weathering research.
Owner:GUANGDONG UNIV OF TECH

Novel nano-drug as well as preparation method and application thereof

The invention discloses a novel nano-drug as well as a preparation method and application thereof, and co-delivery of siRNA and 3BP is realized on an exosome nano-platform, so that a novel nano-drug Exo (at) siRNA / 3BP-CTX (ERBC) engineering exosome is generated. The surface-modified cetuximab (CTX) is targeted to tumors, and shows high targeting and low toxicity in imaging analysis. CCK-8, western blot and immunofluorescence detection are used for detecting the tumor killing effect and the synergistic effect. The ERBC finds that the occurrence of death-promoting autophagy in KRAS mutation tumors is promoted on the transmission electron microscope (TEM) and molecular level.
Owner:CHONGQING MEDICAL UNIVERSITY

Toner and method for manufacturing toner

A toner comprising a toner particle comprising a binder resin and a release agent, wherein the binder resin comprises a first resin and a second resin; the first resin is a crystalline resin having a melting point Tp of 50° C. to 90° C.; the second resin is an amorphous resin; in a cross section of the toner particle observed by a transmission electron microscope, the cross section of the toner particle has a matrix-domain structure composed of a matrix comprising the first resin and domains comprising the second resin; an area ratio of the matrix comprising the first resin in a total area of the cross section of the toner particle is 35 to 70 area %; and where a longest direction of each of the domains is taken as a longitudinal direction, a standard deviation of an angle of the longitudinal direction of the domains is 25° or less.
Owner:CANON KK

Method for preparing aqueous zinc ion battery positive electrode material and detecting charge reaction of aqueous zinc ion battery positive electrode material in metal ion battery

The invention discloses preparation of an aqueous zinc ion battery positive electrode material and a detection method of charge reaction of the aqueous zinc ion battery positive electrode material in a metal ion battery, and belongs to the technical field of batteries. The invention provides the preparation method of the vanadium-based positive electrode material, which is simple in process and low in cost. The preparation method of the positive electrode material comprises the following steps: grinding vanadium pentoxide powder; performing ultrasonic treatment with deionized water, adding inorganic salt, sealing, performing water bath heating reaction, and performing centrifugal washing; and then drying or freeze-drying to finally obtain the batched and high-performance positive electrode material. In 8000 times of charging and discharging, the positive electrode material provided by the invention has excellent cycling stability, and the capacity retention rate is as high as 93%. In addition, an in-situ alternating-current impedance technology is used for rapidly detecting the charge transfer process in the battery, and complex and expensive in-situ X-ray diffraction and transmission electron microscope technologies are avoided. The vanadium pentoxide activation process is accurately controlled through the water bath, the process is simple, the cost is low, and the method has good batch production potential and application prospects.
Owner:HARBIN INST OF TECH

Hollow silicon dioxide particles as well as preparation method and application thereof

The invention discloses a hollow silicon dioxide particle. The ratio of the hollow area of the hollow silicon dioxide particle to the total area of the particle in a transmission electron microscope photo is 10-96%; the average maximum diameter of the hollow silica particles is 100 nm to 10 [mu] m; a shell layer of the hollow silicon dioxide particle is formed by stacking nano particles, the average diameter of nano convex particles in the shell layer is 4-100 nm, and the ratio of the average diameter of the nano convex particles to the average maximum diameter of the hollow silicon dioxide particle is 1 / 2500-1 / 5. The ratio of the average diameter of the nanometer protruding particles on the surfaces of the hollow silicon dioxide particles to the average maximum diameter of the hollow silicon dioxide particles ranges from 1 / 2500 to 1 / 5, so that the bonding force between the hollow silicon dioxide particles serving as filler and resin is high, the fluidity is good when the hollow silicon dioxide particles are added into the resin, and the hollow silicon dioxide particles are suitable for serving as packaging filler of semiconductor devices.
Owner:ZHEJIANG THIRD AGE MATERIAL TECH CO LTD

Resin composition and power cable

The resin composition includes more than 50 mass% and 80 mass% or less of propylene units; and 20 mass% or more of ethylene units or 7 mass% or more of butene units with respect to 100 mass% of a total content of monomer units in a resin component, the resin composition having a co-continuous structure including a first continuous phase in which the propylene units are relatively more and a second continuous phase in which the propylene units are relatively less, or a sea-island structure including a sea phase in which the propylene units are relatively more, and an island phase in which the propylene units are relatively less and a maximum length in a cross-sectional image observed with a transmission electron microscope is 600 nm or less.
Owner:SUMITOMO ELECTRIC INDUSTRIES LTD

Ion thinning instrument control method based on self-adaptive gradient energy reduction algorithm

The invention discloses an ion thinning instrument control method based on a self-adaptive gradient energy reduction algorithm, and belongs to the technical field of transmission electron microscope (TEM) sample preparation. The problem that a traditional ion thinning technology has many limitations is solved, dynamic optimization of parameters such as ion beam energy, beam current density and sample temperature is achieved through the self-adaptive gradient energy reduction algorithm, and the sample preparation efficiency is remarkably improved; by combining multi-modal data acquisition and dynamic gradient optimization, the thinning process can be accurately controlled, and the sample quality is improved; sample damage is effectively avoided by combining a damage constraint mechanism and self-adaptive step length control, and the stability of the preparation process is improved; the method is suitable for various materials through a pre-stored optimization path library, and has wide applicability; therefore, the energy of the ion beam is optimized, the incident angle and the beam density are dynamically adjusted, and the thinning instrument is controlled.
Owner:CHONGQING UNIV

Matrices and systems for preservation of biomolecules in vacuum

PendingUS20250060292A1Preparing sample for investigationStaining techniqueMass analyzer
Methods for preparing imaging samples by applying a liquid or semiliquid substance to a substrate surface in order to mitigate the deleterious effects of vacuum and other conditions used for sample preparation, thereby preserving the structure of at least a portion of deposited samples. These methods are useful for MS-based electron microscopy (EM) sample preparation at room temperature, but are also applicable to other imaging methods. These methods also enable transmission electron microscopy (TEM) structural confirmation of ions passing through a mass spectrometer. Additionally, only entry-level negative staining techniques for TEM are required, making this technique much more widely available than cryogenic electron microscopy (cryo-EM).
Owner:WISCONSIN ALUMNI RES FOUND

Preparation method of exosome antibody microsphere conjugate

The invention provides a preparation method of an exosome antibody microsphere conjugate, which belongs to the technical field of exosomes, and comprises the following steps: preparing a carboxyl polystyrene microsphere suspension with the particle size of 50 nanometers, and ensuring that the size of the microsphere is stabilized in a range of 50 + / -5 nanometers by optimizing centrifugation and cross-linking conditions. And then coupling the exosome marker antibody with the microspheres, and closing unreacted active groups. A mathematical model is adopted to optimize purification process parameters for purification. A dynamic light scattering and transmission electron microscope is utilized to characterize coupling physics properties, and a conjugate meeting requirements is screened. And finally, obtaining fluffy porous exosome antibody microsphere conjugate freeze-dried powder under the protection of a sucrose solution by adopting a vacuum freeze-drying method. The method solves the technical problems that in an existing exosome microsphere conjugate preparation process, centrifugation and purification parameters are often set according to artificial experience, optimization is difficult to obtain, and the quality of the exosome microsphere conjugate is affected.
Owner:QINGDAO RAISECARE BIOTECHNOLOGY CO LTD

Medium manganese steel oxygen vacancy defect identification method and device

The invention provides a medium manganese steel oxygen vacancy defect identification method and device. The method comprises the following steps: obtaining a first oxygen vacancy defect area based on a measurement result of a positron annihilation lifetime spectrum and a Doppler broadening spectrum on a target sample block; aiming at each ultra-thin sample, observing the ultra-thin sample through a high-resolution transmission electron microscope, and collecting a bright field image and a dark field image of the ultra-thin sample; obtaining a second oxygen vacancy defect area based on the bright field image, the dark field image and the first oxygen vacancy defect area; performing electron energy loss spectrum analysis on the second oxygen vacancy defect area, and determining a third oxygen vacancy defect area and corresponding oxygen vacancy defect concentration in the ultrathin sample; and determining each target oxygen vacancy defect region and oxygen vacancy defect concentration of the target medium manganese steel sample according to the third oxygen vacancy defect region and oxygen vacancy defect concentration in each ultrathin sample. According to the invention, information such as position, number, size and distribution pattern of oxygen vacancy defects can be accurately obtained.
Owner:河钢数字技术股份有限公司 +1

Preparation method of transmission electron microscope sample

The invention provides a preparation method of a transmission electron microscope sample, which comprises the following steps: welding a prepared cross section TEM sample on a carrying net, horizontally placing the carrying net, and forming a first protection layer on the cross section; forming a limiting mark; forming a second protective layer on the first protective layer; after the part, close to the connecting end of the same carrying net, of the cross-section TEM sample is welded together with a nano manipulator, the sample and the carrying net are cut and separated at the connecting position; the nano manipulator is moved to the hovering position, and then the nano manipulator is taken back; overturning the sample table to enable the carrying net to be vertically placed; after adjustment preparation, the other end, opposite to the end connected with the nano manipulator, of the sample is welded to the carrying net; after the sample and the nano manipulator are cut and separated, the nano manipulator is taken back; and inclining the sample table to 52 degrees, and cutting and thinning the sample according to the limiting marks to obtain the required planar TEM sample. The purpose of comprehensively knowing the plane and section structure information of the sample can be achieved.
Owner:HUAHONG INTEGRATED CIRCUIT (CHENGDU) CO LTD

Multi-field coupling transmission electron microscope in-situ sample rod and bidirectional accurate temperature and electromagnetic field control system method thereof

The invention discloses a multi-field coupling transmission electron microscope in-situ sample rod and a bidirectional accurate temperature and electromagnetic field control system method thereof, and belongs to the field of transmission electron microscopes. The rod head of the sample rod comprises an objective table, a micro U-shaped electromagnet and a PCB (Printed Circuit Board) which are arranged in the objective table, a temperature conducting plate and a liquid nitrogen circulating pipe which are arranged at the rear end of the objective table, and a four-electrode MEMS (Micro Electro Mechanical System) thermoelectric chip arranged on the objective table. Dual control of heating and an electric field is realized through the MEMS thermoelectric chip, and bidirectional temperature adjustment of a sample is realized in combination with a liquid nitrogen cooling system. And meanwhile, the sample rod is also integrated with a micro U-shaped electromagnet to apply a controllable parallel magnetic field. The whole system can carry out multi-field coupling experiments under extreme conditions, such as dynamic researches of electricity, magnetism, phase change and the like.
Owner:LANZHOU UNIV

Method for rapidly realizing crystallographic orientation imaging in transmission electron microscope

The invention discloses a method for rapidly realizing crystallographic orientation imaging in a transmission electron microscope. The method comprises the following steps: collecting conical scanning dark field images of front 8-10 diffraction rings under inclination angles of 3-5 samples through the transmission electron microscope; carrying out drift correction on the dark field images under different sample inclination angles and then carrying out binaryzation on all the dark field images; building an incident electron beam conical scanning model, simulating electron diffraction patterns of any orientation under different sample inclination angles, and building an electron diffraction pattern database; reconstructing a diffraction pattern of each pixel in the dark field image under the same sample inclination angle, and calibrating orientations of all the pixels; and completing orientation calibration of all pixels in combination with data of multiple sample inclination angles. The rapid characterization of the grain orientation is realized based on the transmission electron microscope conical scanning dark field imaging technology and the crystallographic orientation calibration algorithm, and the method is suitable for the crystallographic orientation characterization of the crystal material under the transmission electron microscope.
Owner:CHONGQING UNIV

Toner and method for producing toner

A toner comprising a toner particle comprising a binder resin, wherein the binder resin comprises a first resin and a second resin, the first resin is a crystalline resin, the second resin is an amorphous resin, in an observation of a cross section of the toner particle with a transmission electron microscope, a matrix-domain structure composed of a matrix comprising the first resin and domains comprising the second resin is present, an area ratio occupied by the matrix in a total area of the matrix and the domains is from 35 area % to 70 area %, a [hydrocarbon group index (Ge)] / [hydrocarbon group index (DIA)] after washing the toner with hexane is 1.10 or more.
Owner:CANON KK

Schottky diode with transverse structure, in-situ sample preparation method and processing technology

The invention discloses a Schottky diode with a transverse structure, an in-situ sample preparation method and a processing technology. The cathode and the anode of the Schottky diode are in the same plane, the cathode ohmic contact layer is arranged on the periphery of the structure, the anode Schottky metal layer is arranged in the center of the structure, and the AlGaN barrier layer and the GaN substrate layer are sequentially arranged between the cathode ohmic contact layer and the anode Schottky metal layer. According to the in-situ sample preparation method, the FIB sample preparation technology and the selected area circuit breaking method are adopted to complete connection of the sample and the chip, the failure behavior of the device can be observed in real time under a transmission electron microscope, and the processing technology achieves effective isolation of the anode and the two-dimensional electron device through silicon oxide in the sample preparation process. Meanwhile, silicon oxide isolation can prevent short circuit of a power supply, so that a current passing path is shorter, the efficiency is higher, and the surface of a sample and a metal functional area below the sample can be effectively prevented from being damaged when ion beams are operated. The problems of low device power conversion efficiency, electrode short circuit and the like are solved.
Owner:XIDIAN UNIV

Separation-free detection method for extracellular vesicle marker based on nanoparticle enhancement

The invention provides an extracellular vesicle marker separation-free detection method based on nanoparticle enhancement, and belongs to the technical field of detection methods, the method comprises the following steps: preparing gold nanoparticles with the surface modified with a first antibody, the first antibody being used for specific recognition of an extracellular vesicle surface marker; determining the particle size distribution of the gold nanoparticles by adopting a dynamic light scattering method, and determining the surface potentials and surface isoelectric points of the gold nanoparticles by adopting a potentiostat; adopting a transmission electron microscope to characterize the morphology of the screened gold nanoparticles; co-modifying polyethylene glycol molecules on the surfaces of the gold nanoparticles to form an anti-interference layer; mixing the gold nanoparticles with uniform morphology with a sample to be detected; adding a second antibody into the mixed system; distinguishing signals of the binding-state second antibody and the free-state second antibody through fluorescence lifetime analysis; preparing an extracellular vesicle standard substance, and obtaining a standard curve and a system response curve; the optimal detection condition is determined by solving the detection system optimization equation set, and separation-free detection is carried out.
Owner:QINGDAO RAISECARE BIOTECHNOLOGY CO LTD

Aluminum alloy sheet and method for producing same

To provide an aluminum alloy sheet excellent in rollability.SOLUTION: 0.05% by mass or more and 0.35% by mass or less of Si, 0.05% by mass or more and 0.50% by mass or less of Fe, 0.01% by mass or more and 0.35% by mass or less of Cu, 0.10% by mass or more and 0.80% by mass or less of Mn, 2.0% by mass or more and 6.0% by mass or less of Mg, 0.01% by mass or more and 0.15% by mass or less of Cr, and a balance of Al and inevitable impurities, in a cross section in a sheet thickness direction, a ratio of an area occupied by central grains is 1.15% or less, and in a sheet thickness Mg2Si region, a number-density ratio obtained by dividing a number-density of precipitates observed with a transmission-type electron microscope by a number-density in a reference aluminum alloy sheet, a Si-amount ratio obtained by dividing a Si content by a reference Si content, and a Mg-amount ratio obtained by dividing a Mg content by a reference Mg content satisfy the following formulas: Number density ratio ≥ 10.929 * Si amount ratio - 15.814 + 2.043 * (Mg amount ratio - 1) SELECTED DRAWING: Figure 5
Owner:KOBE STEEL LTD

Application of cucumber CsAPRR2 gene in regulating and controlling peel color

The invention discloses an application of a cucumber CsAPRR2 gene in regulating and controlling the color of pericarp. The invention relates to the field of plant genetic engineering, and provides application of inhibiting expression and / or activity of CsAPRR2 protein in creation of yellow peel cucumber. CsAPRR2 is knocked out through a CRISPR-Cas9 mediated gene editing technology, all knockout mutation lines show the pericarp yellowing character, a transmission electron microscope (TEM) shows that the chloroplast structure of the CsAPRR2 knockout line is damaged, and it is proved that the CsAPRR2 gene can regulate and control the color of the pericarp of the cucumber. The invention provides a molecular tool and a gene resource for researching a cucumber peel yellowing regulation mechanism and cultivating a new variety.
Owner:CHINA AGRI UNIV +1

Application of NtIPMD gene in regulating chlorophyll content in tobacco

The present invention discloses the application of the NtIPMD gene in regulating the chlorophyll content of tobacco, and belongs to the field of plant genetic engineering technology. Based on the existing progress in tobacco genetic engineering and the observation and identification of related plant phenotypes, the present invention conducts in-depth research on the NtIPMD gene and finds that it is related to the development of tobacco chloroplasts. The nucleotide sequence of the NtIPMD gene is shown in SEQ ID NO.1. After silencing the gene, the chlorophyll content of the leaves decreases, the growth of the plants slows down, and transmission electron microscopy observation reveals abnormal chloroplast development. The present invention finds that the gene encoding tobacco isopropylmalate dehydrogenase, NtIPMD, plays a key role in regulating the chlorophyll content of tobacco leaves, laying the foundation for clarifying the molecular regulatory mechanism of chlorophyll biosynthesis in tobacco leaves and providing a new precise regulatory gene for regulating the chlorophyll content of tobacco leaves.
Owner:ZHENGZHOU TOBACCO RES INST OF CNTC

Selenium nano-particles as well as preparation method and application thereof

The invention provides selenium nanoparticles as well as a preparation method and application thereof, and belongs to the technical field of selenium nanoparticles. Acetone ultrasonic cleaning and chemical polishing pretreatment are performed on a pure titanium substrate to obtain a clean surface, an anodic oxidation method is adopted to prepare a # imgabs0 # nanotube array carrier, and the nano-particles are prepared into selenium nano-particles. The method comprises the following steps: accurately depositing selenium nanoparticles on a carrier by using an electrochemical deposition method, realizing load control by combining an electrochemical kinetics principle, realizing uniform dispersion of the particles by matching an ultrasonic dispersion technology with a particle swarm optimization algorithm, and carrying out centrifugal separation and vacuum drying to obtain a spherical selenium nanoparticle product. And a multi-dimensional quality control detection system of a transmission electron microscope, an X-ray photoelectron spectroscopy and dynamic light scattering is established, so that the technical problems that the particle size distribution is non-uniform and the deposition load is difficult to accurately control in the preparation process of the selenium nanoparticles are solved.
Owner:QINGDAO UNIV

Toughening and forming method of high-performance PEI plate for high-heat-resistance structural member

The invention discloses a toughening forming method of a high-performance PEI plate for a high-heat-resistance structural part, and particularly relates to the technical field of high-performance composite material forming. Pre-embedding a PEI toughening layer between thermosetting prepreg layers, and controlling the temperature, the pressure, the pressure maintaining time and the heating rate in the hot pressing process; carrying out infrared spectrum or solid nuclear magnetic resonance testing on the interface area sample subjected to hot press molding, and calculating the chain segment residual rate Rp; determining the interface penetration depth Di through a transmission electron microscope in combination with energy spectrum analysis; inputting the Rp and the Di into an interface coupling model, and outputting an interface combination quality factor Q by the model in a form of combining weighted linearity and logarithmic functions; the interface bonding grade is judged according to the Q value, and when the Q value is lower than a threshold value, hot-pressing process parameters are backtracked for optimization; according to the method, quantitative evaluation of the interface performance and process closed-loop optimization are realized, and the interface bonding strength and service reliability of the composite material can be effectively improved.
Owner:JIANGXI TONGYI POLYMER MATERIAL TECH CO LTD