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1810results about How to "Diffusion fast" patented technology

Preparation method of hydro-treatment catalyst

The invention discloses a preparation method of a hydro-treatment catalyst. The preparation method comprises the following steps: preparing an alumina carrier, preparing an impregnation solution containing the VIII group metal and VIB group metal, wherein the impregnation solution comprises a proper amount of an organic auxiliary agent containing chelating ligand, then impregnating the alumina carrier into the impregnation solution under a proper ultrasonic treatment condition, and drying so as to obtain the hydro-treatment catalyst. The preparation method utilizes the ultrasonic cavitation effect to properly reduce the viscosity of the impregnation solution; at the same time the complexing capacity between the chelating ligand in the organic auxiliary agent and nickel / cobalt is improved by the catalytic function of the ultrasonic, the interaction force between the chelating ligand and nickel / cobalt is strengthened, thus the active metal component is promoted to highly disperse on the carrier surface, furthermore, the existing state of the active metal on the catalyst surface is improved at the same time, the sulfurization degree and sulfurization uniformity of the active metal are both improved, so the activity and stability of the catalyst are both improved. The catalyst is especially suitable for being used in the hydro-denitrogenation process and hydro-desulfurization process of heavy distillate oil.
Owner:CHINA PETROLEUM & CHEM CORP +1

Austenitic stainless steel metallographic etchant, preparing method and use thereof

The invention discloses a metallographic-phase aggressive agent of an austenitic stainless steel, a preparation method thereof and application thereof. The metallographic-phase aggressive agent comprises the mixed solution of hydrofluoric acid and nitric acid, calculated by volume ratio, the proportion of each component of the agent is that hydrofluoric acid : nitric acid : water is equal to 2 : 1 : 7. The preparation method thereof is carried out according to the following steps of: taking 70ml of water first, then taking 10ml of analytically pure nitric acid and finally taking 20ml of analytically pure hydrofluoric acid, which are then evenly mixed. The application method thereof comprises the following steps of: putting a simple of the austenitic stainless steel in the metallographic-phase aggressive agent of the austenitic stainless steel and observing the color change of the surface of the sample by time, taking out the sample of the austenitic stainless steel when metallographic-phase surface of the sample is corroded to darker silver gray, washing the sample with water which is then neutralized with alkaline solution and finally washing with water and absolute ethyl alcohol. The technical effects thereof are represented by good corrosion effect, clear austenite grain boundary, slow corrosion speed, easy control, no pollution and other aspects.
Owner:董加坤

Micro-needle array chip, percutaneous administration device, percutaneous administration patch and preparation method thereof

The invention relates to a micro-needle array chip, a transdermal delivery device, a transdermal delivery patch and a preparation method thereof, wherein a micro-needle is obliquely fixed on a substrate at a set angle, the upper surface of the needle is an elliptic plane parallel to the substrate or obliquely provided with an acute angle, the needle is further treated to have more edge angles, a metal wire bar or tube penetrates a non-metallic material substrate such as polymer and the like along a certain angle, and then a nick of the metal wire bar or tube on the substrate is grinded and polished; and photosensitive resist patterns are formed nearby the nick at one end by adopting photoetching and etching technology, then the metal wire bar or tube is subjected to chemical or electrochemical corrosion to form a needle point and the photosensitive resist is removed, the surface of the manufactured solid micro-needle array chip can be covered with drugs, and the manufactured solid micro-needle array chip can deliver liquid medicine or extract body fluid. The method avoids the skin plugging a transfusion hole, is easy to adjust and control the maximum penetrating depth of the micro-needle, and is suitable for percutaneous transportation of biological macromolecular drugs and cosmetics and skincare and new percutaneous preparation of the prior drugs.
Owner:TSINGHUA UNIV
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