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3020results about How to "Enhanced interface binding" patented technology

Thermoplasticity sizing agent for carbon fiber and preparation and usage thereof

The invention provides a thermoplasticity sizing agent for a carbon fiber as well as a preparation method and a usage method thereof and relates to solvent sizing agent for a carbon fiber as well as a preparation method and a usage method thereof. According to the invention, the problems that the existing thermoplastic sizing agent is complicate in preparation process and pollutes the environment are solved. The preparation method is as follows: the thermoplastic resin, an organic solvent A and an adjuvant are mixed and stirred uniformly so as to obtain the thermoplastic sizing agent, when being used, the carbon fiber is dipped in the thermoplasticity sixing agent, then fractioning is carried out on the carbon fiber with agent and the treated carbon fiber is dipped in an organic solvent B, and finally the carbon fiber is dried. According to the invention, the wettability of the carbon fiber and the high performance thermoplasticity resin of polyarylether can be improved, the boundary bonding performance of the carbon fiber or the resin matrix composite of thermoplasticity polyarylether can be improved, and the thermoplasticity sizing agent has the advantages that the cost is low, the performance is stable, the utilization is stable and the environment is not polluted. The thermoplasticity sizing agent for the carbon fiber is used for the surface treatment of a carbon fiber material.
Owner:HARBIN INST OF TECH

Multifunctional concrete structure endurance protective agent, preparation and application method thereof

The invention discloses a multifunctional concrete structure endurance protective agent as well as the preparation and application method thereof. The protective agent provided by the invention contains the following ingredients of: an organic / inorganic composite fluorosilicone-acrylate copolymer, lithium silicate, sodium silicate, lithium molybdate, sodium tetraborate, sal glauberi, 1,2-aminoazophenylene, nanometer titanium dioxide, anhydrous ethanol and water. The protective agent can penetrate inside concrete, wherein a densification ingredient can minimize internal holes and cracks to raise the compactness of concrete, and a rust-resistant ingredient can penetrate into concrete and be adsorbed on the surface of steel bar so as to passivate and protect the steel bar; the low-surface energy silicon fluoride ingredient can be solidified to form a cured film on the surface of concrete so as to endow the protective agent with the hydrophobic performance; a nanometer ingredient can endow the cured film layer with properties of resisting ultraviolet and ageing and improving the organic polymer performance as well as the self-cleaning performance. In addition, hydroxy generated from the hydrolysis of siloxane group can perform a condensation reaction with hydroxy on the surface of concrete to produce chemical bond, so as to raise the anchoring strength between the film and concrete and improve the interface combination. The protective agent provided by the invention can be widely applied in various concrete structure engineering protections to raise the service life of concrete.
Owner:CENT SOUTH UNIV +1

Graphene-reinforced magnesium-aluminium matrix composite material and preparation method thereof

The invention discloses a graphene-reinforced magnesium-aluminium matrix composite material and a preparation method thereof, and belongs to the technical field of composite materials. The preparation method comprises the following steps: dissolving graphene in an appropriate amount of ethanol solution and ultrasonically dispersing, then intermittently adding a metal powder in the solution, and ultrasonically dispersing and mechanically stirring simultaneously to obtain graphene/metal particle mixed solution with high dispersibility; sequentially carrying out the operations of heating in a low-temperature water bath to remove a solvent, drying in vacuum to obtain a powder, and continuously manually grinding the powder under an inert atmosphere, on the mixed solution, so as to obtain a graphene/metal particle composite powder with uniform dispersion; and carrying out hot-pressing on the composite powder into blocks, carrying out hot extrusion, and finally obtaining the graphene/metal matrix composite material. The preparation process disclosed by the invention is simple, environment-friendly, and free from addition of a non-volatile organic dispersant; low-temperature inert protection is adopted during the process of preparing the composite powder, and high own dispersion of graphene and high dispersion thereof in a metal matrix are achieved while the structural integrity of a graphene reinforcement is kept; and the preparation method is suitable for preparing the high-performance graphene-reinforced metal matrix composite material.
Owner:BEIJING UNIV OF TECH

Method for preparing graphene toughened silicon carbide ceramic composite material

The invention belongs to the field of macromolecule inorganic chemistry, and in particular relates to a method for preparing a graphene toughened silicon carbide ceramic composite material. Specifically, the method comprises the following steps: by taking graphite oxide as a carbon source, wrapping the surface of reduced graphene oxide with a layer of SiO2 granules by using a hydrothermal method so as to form a good interface layer between graphene and SiC, uniformly dispersing, and implementing carbon thermal reduction reaction at the interface of graphene and SiO2 in the high-temperature sintering process so as to growth silicon carbide crystal whisker and granules in situ, thereby improving the interface strength and the oxidation resistance, achieving an interface intensification function, improving crack expansion resistance and further improving the fracture toughness of ceramic. The method aims at the defects that graphene is poor in dispersity and high-temperature oxidation resistance in a conventional graphene/silicon carbide composite material, in-situ growth, crack self-healing and toughness mechanisms are applied to a preparation technique of a graphene/silicon carbide material, and thus graphene toughened silicon carbide ceramic with excellent mechanical properties and interface binding properties can be prepared.
Owner:ZHONGYUAN ENGINEERING COLLEGE

Method for preparing graphene reinforced metal-based composite material through discharge plasma (SPS) sintering

The present invention relates to a method for preparing a graphene reinforced metal-based composite material through discharge plasma (SPS) sintering. The method is characterized in that the graphene reinforced metal-based block material is prepared through SPS sintering and has the following advantages that: the preparation method is simple, the material is compact and does not have pores, the graphene mass fraction can be arbitrarily regulated, the distribution is uniform, no aggregation is generated, the material mechanical property isotropy is provided, and the wettability of the metal and the graphene interface is good. The method comprises: (1) reducing graphene oxide through a chemical method or a hydrothermal method to obtain graphene sheets with a sheet layer thickness of not more than 4 nm and sheet layer diameter of not more than 50 [mu]m; and (2) preparing metal powder with a particle size of not more than 200 [mu]m through a rotating electrode atomization method, mechanical crushing or a high-speed ball milling method; (3) carrying out mechanical or ball milling mixing on the graphene powder and the metal powder according to the required mass ratio; and (4) carrying out SPS sintering forming on the mixed powder, wherein the obtained material has characteristics of improved mechanical property, decreased density, good heat conduction capability, and good electric conduction capability, and the performance customizing can be achieved by adjusting the preparation parameters.
Owner:BEIHANG UNIV

Multi-stage wire feeding printing head for 3D printing of continuous fiber reinforced composite materials

A multi-stage wire feeding printing head for 3D printing of continuous fiber reinforced composite materials comprises a fiber guiding pipe fixed to the upper surface of a first-stage heating block. An inner hole channel of the fiber guiding pipe forms a fiber channel. A first-stage throat pipe is fixed to one side of the first-stage heating block. An inner hole channel of the first-stage throat pipe forms a first-stage inner hole channel. High polymer materials penetrate the first-stage inner hole channel and enter a melting cavity of the first-stage heating block. The first-stage heating block is fixed above a second-stage heating block. A second-stage throat pipe is fixed to one side of the second-stage heating block. A second-stage throat pipe inner hole channel forms a second-stage inner hole channel. High-performance thermoplastic materials penetrate the second-stage inner hole channel and enter a melting cavity of the second-stage heating block. As analogized according to the same structure, finally, all the heating blocks are fixed to the upper face of the last-stage heating block, and a spray nozzle is fixed to the lower surface of the last-stage heating block. The multi-stage wire feeding printing head is adopted, multi-stage wrapping can be well performed on base materials for continuous fibers, and continuous fiber reinforced composite material parts with good comprehensive performance are obtained.
Owner:XI AN JIAOTONG UNIV

Preparing method for powder metallurgy high-entropy alloy based composite material

InactiveCN105734324AEvenly distributedGood combination of reinforcement and matrix interfaceIncreasing energy efficiencyHigh entropy alloysPowder metallurgy
The invention relates to a preparing method for a powder metallurgy high-entropy alloy based composite material, and belongs to the field of powder metallurgy materials. The preparing method includes the steps that all components are prepared and taken according to component proportions of a designed high-entropy alloy matrix, and high-entropy alloy powder is prepared through a gas atomization method; and then according to the component proportions of the designed high-entropy alloy based composite material, the high-entropy alloy powder and wild phase titanium diboride powder are prepared and taken, and rapid sintering molding is achieved after even mixing is carried out. According to the preparing method, the atomization method is adopted for preparing spherical high-entropy alloy powder with relatively-even ingredients in advance, and therefore a simple solid solution phase structure of a high-entropy alloy is guaranteed; and discharging plasma rapid sintering is adopted for preparing the needed powder metallurgy high-entropy alloy based composite material, and therefore the shortcoming that the material is prepared with metal powder as a raw material through a powder metallurgy method traditionally, and consequently the high-entropy alloy of the simple solid solution structure is difficult to obtain is overcome. The preparing method is simple in process procedure; according to the prepared powder metallurgy high-entropy alloy based composite material, titanium diboride is evenly distributed, reinforcement and base body interface bonding is better, the comprehensive performance is more excellent, the specific strength is high, the specific rigidity is high, and the abrasive resistance and the corrosion resistance are excellent. The preparing method is suitable for industrial production.
Owner:CENT SOUTH UNIV

Copper-carbon composite material and preparing method thereof

The invention discloses a copper-carbon composite material and a preparing method thereof. Natural flake graphite, colloidal graphite, nano graphite, carbon fiber and the like can be selected as a carbon material in the copper-carbon composite material. The preparing method of the copper-carbon composite material includes the steps that firstly, a chemical nickel plating method is used for preparing a nickel plating carbon material; then a chemical copper plating method is used for plating copper on the nickel plating carbon material; and finally, vacuum semi-solid-state low-pressure sintering is conducted on the copper plating carbon material under the copper melting point temperature, and the copper-carbon composite material is prepared. The copper-carbon composite material and the preparing method thereof have the beneficial effects that a layer of even thin nickel plating layer is formed on the surface of carbon through the nickel plating method so as to reduce the wetting angle of the carbon material, the copper plating layer is formed on the surface of the nickel plating carbon material through the copper plating method so that a three-dimensional copper network can be formed by the material in the sintering process, and the bonding strength of a base body is improved through vacuum semi-solid-state low-pressure sintering. The two phases of the base body and the carbon of the copper-carbon composite material prepared through the method are distributed evenly and are well combined, and the good electricity and mechanical properties and the good frictional wear performance are achieved.
Owner:CENT SOUTH UNIV

Preparation method for in-situ synthesis of three-dimensional graphene-reinforced copper-based composite material

The invention relates to a preparation method for in-situ synthesis of a three-dimensional graphene-reinforced copper-based composite material. The preparation method comprises the following steps: taking copper nitrate trihydrate as a copper source, mixing the copper source with a solid carbon source (glucose or citric acid) and a water-soluble salt template (sodium chloride), then adding the mixture into water to dissolve the mixture, performing stirring uniformly to obtain a precursor solution; performing freeze-drying dehydration to obtain a mixed powder precursor; performing heating to 600-800 DEG C, performing heat preservation for 1-3 h, and then perform cooling quickly to obtain self-assembly powder; washing off sodium chloride by suction filtration, and performing vacuum drying; pouring the product into an ethanol solution of copper nitrate; performing water-bath evaporation drying and vacuum drying; under atmosphere protection, performing heating to 600-800 DEG C, performing heat preservation for 1-3 h, and obtaining three-dimensional graphene-copper particle composite powder by furnace cooling; and molding according to a vacuum hot-pressing sintering technology. The blocky material prepared according to the method has the characteristic that the graphene has good dispersity and is closely combined with a copper base; and meanwhile, the blocky material has excellent toughness and mechanical properties.
Owner:TIANJIN UNIV

Preparation method and preparation system for ultralight composite traction belt

The invention discloses a preparation method and a preparation system for an ultralight composite traction belt, and provides a preparation method and a preparation system for the ultralight composite traction belt with uniform bearing and long service life. The preparation method comprises the following steps: a twist-free continuous monofilament is led out of a fiber yarn group, unfolded uniformly, and introduced into an impregnation tank for impregnation, wherein the impregnation tank is added with a glue solution, then arrangement is performed, and composite enhanced pieces are obtained after pultrusion and curing; the composite enhanced pieces are led out respectively, preheated and introduced into a head die of an extruder, an extruding die core corresponding to the section of the traction belt is arranged in the head die, the composite enhanced pieces are uniformly coated with molten thermoplastic resin in the head die and led out of the head die of the extruder, preliminary forming is realized, and the traction belt is obtained after cooling setting and cooling. The prepared traction belt is light in weight, high in strength, easy to bend, anti-fatigue, long in service life, low in maintenance cost and more applicable to a long-distance elevator.
Owner:TIANJIN GOLDSUN WIRE ROPE

Recycled concrete and preparation method thereof

The invention relates to recycled concrete and a preparation method thereof, and belongs to the technical field of concrete. The recycled concrete comprises (by weight): 150-280 parts of cement, 90-130 parts of water, 800-950 parts of modified recycled coarse aggregate, 400-530 parts of fine aggregate, 40-85 parts of fly ash, 80-100 parts of mineral powder, 50-140 parts of zeolite powder, 30-60 parts of epoxy resin, 4-10 parts of a water reducing agent and 2-6 parts of an air entraining agent. The preparation method of the modified recycled coarse aggregate comprises the following steps: S1, crushing and screening waste concrete to obtain recycled coarse aggregate; S2, soaking the recycled coarse aggregate obtained in the step S1 in an acetic acid solution with the mass concentration of 2-7%, and airing; S3, stirring 80-110 parts of polyvinyl alcohol, 60-110 parts of silica fume, 40-80 parts of sodium silicate and 800-1,000 parts of water to obtain a modified liquid; and S4, soaking the recycled coarse aggregate obtained in the step S2 in the modified liquid obtained in the step S3, taking out the soaked recycled coarse aggregate, and baking the recycled coarse aggregate to obtainthe modified recycled coarse aggregate. The recycled concrete provided by the invention has a good compressive strength effect.
Owner:泸州临港思源混凝土有限公司
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