1038 results about "Ascorbic acid" patented technology

The invention provides a recombinant III-type humanized collagen gel based on a macromolecular crowding effect as well as a preparation method and application of the recombinant III-type humanized collagen gel. The method comprises the following steps: firstly, preparing an rhCol III solution system; then preparing a macromolecular crowding bath containing dextran 70, polyethylene glycol 8000 and ascorbic acid; then adding an rhCol III solution into the macromolecular crowding bath to form an rhCol III microgel; and finally, constructing a 3D printing molecular exclusion mold system which takes agarose as a substrate and contains a functional additive and a temperature-sensitive polymer as a temperature-sensitive release and spatial constraint component, so as to realize directional construction of the rhCol III microgel. According to the method disclosed by the invention, second-level physical gelling (lt; 15s) of rhCol is realized, and a physiological microenvironment supporting cell proliferation is constructed. The recombinant III-type humanized collagen gel prepared by the method can be used for preparing collagen microgel balls, collagen bundles, 3D (three-dimensional) bio-printing products and the like, and is wide in application range.

The invention belongs to the technical field of lithium ion battery material recovery, and discloses a regeneration, repair and doping method of a waste lithium iron phosphate material and a regenerated positive electrode material. The method comprises the following steps: firstly, immersing waste LiFePO4 powder into a mixed solution of citric acid and ascorbic acid, oscillating to selectively dissolve out Fe < 3 + > impurities, and synchronously reducing Fe < 3 + > on the surface to Fe < 2 + >; then Li2CO3 is added into the leached powder for lithium bit compensation, and ball milling and uniform mixing are carried out; then Al2O3 and TiCl3 are added for aluminum-titanium co-doping, and ultrasonic dispersion is carried out uniformly; and finally, carrying out segmented sintering. In the first stage, sintering is carried out in an air atmosphere at 300-350 DEG C; in the second stage, sintering is performed at 600-700 DEG C in an inert gas atmosphere; and finally obtaining the regenerated positive electrode material. According to the method, waste lithium iron phosphate batteries can be turned into wealth, the lithium iron phosphate positive electrode material with good electrochemical performance is obtained, the complex and expensive impurity removal process is omitted, the cost is low, and possibility is provided for large-scale industrial regeneration and repair of waste lithium iron phosphate active substances.

The invention provides a GelMA microneedle patch loaded with chromogenic gold nano bipyramids and a preparation method thereof.The method comprises the steps that citric acid, chloroauric acid and a CTAC solution are mixed, then sodium borohydride is added, and a seed solution is obtained through stirring and standing; mixing chloroauric acid, silver nitrate, hydrochloric acid and CTAB (cetyltrimethyl ammonium bromide), and sequentially adding ascorbic acid and the seed solution to obtain a growth solution; carrying out centrifugation, morphology regulation and chemical etching purification to obtain a chromogenic gold nano bipyramid solution; the preparation method comprises the following steps: reacting gelatin with methacrylic anhydride in PBS, dialyzing and freeze-drying to obtain GelMA; dissolving GelMA in the gold nanoparticle bipyramid solution, and adding a photoinitiator LAP to obtain a mixed precursor solution; and the GelMA microneedle patch loaded with the gold nano bipyramid is prepared through mold casting, centrifugation, ultraviolet light crosslinking and drying demolding. The microneedle extraction and gold nano bipyramid color development integrated scheme is initiated, blood sampling is not needed, the dermis interstitial fluid is extracted in a minimally invasive mode through the microneedle, detection pain and trauma are reduced, the cross infection risk of blood treatment is avoided, and the microneedle microneedle microneedle microneedle microneedle microneedle microneedle microneedle microneedle microneedle microneedle microneedle microneedle microneedle microneedle microneedle microneedle microneedle microneedle microneedle microneedle microneedle microneedle microneedle

The invention belongs to the technical field of antibiosis, and discloses a photodynamic antibacterial modified polyester fiber and a preparation method thereof.The preparation method comprises the steps that 1, SIPM serves as a surfactant, water-soluble silver salt serves as a precursor, ascorbic acid serves as a reducing agent, and water-soluble nano-silver powder is prepared; (2) after PTA and EG are subjected to esterification reaction, EG, SIPM and water-soluble nano-silver powder are added for polymerization reaction, and the photoresponse active material is obtained; (3) preparing the nano-silver antibacterial master batch by taking ECDP as a base material of the nano-silver antibacterial master batch and a photoresponse active material as an additive; and (4) carrying out melt blending on the modified polyester, a water-soluble pore-foaming agent and the nano-silver antibacterial master batch to obtain a spinning melt, spinning the spinning melt, and washing with water to obtain the photodynamic antibacterial modified polyester fiber. The photodynamic antibacterial modified polyester fiber disclosed by the invention has excellent antibacterial and antiviral properties.

The invention discloses a zinc transition metal complex and preparation and application thereof in fluorescence recognition of biomolecules, and relates to the technical field of metal organic framework materials, the chemical formula of the zinc transition metal complex is [Zn2 (L) 2 (bpe) (H2O) 2] n, and 3, 5-bis (3-carboxylic acid phenyl)-1, 2, 4-triazole, 1, 2, 4-triazole, 1, 3, 4-triazole, 1, 3, 4-triazole, 1, 3, 4-triazole, 1, 3, 4-triazole, 1, 3, 4-triazole, 1, 3, 4-triazole, 1, 3, 4-triazole, 1, 3, 4-triazole The complex material is prepared by co-dissolving 2, 2-bis (4-pyridyl) ethylene, Zn (NO3) 3.6 H2O and N, N-dimethylformamide in an aqueous solution, has excellent fluorescence performance, has the capability of specifically identifying ascorbic acid in various biomolecules, and also has relatively good anti-interference performance, excellent circularity and strong stability, and can be widely applied to the field of biochemistry, biochemistry, biochemistry, biochemistry, biochemistry, biochemistry, biochemistry, biochemistry, biochemistry, biochemistry, biochemistry, biochemistry, biochemistry, biochemistry, biochemistry and biochemistry. The method can be used for detecting ascorbic acid in water and beverages.

The application provides a kind of superfine copper powder and its preparation method and application, the preparation method of the above-mentioned superfine copper powder uses two-step liquid phase reduction method to prepare superfine copper powder, and improves process conditions, using dropwise feeding mode. Among them, the first step uses alkaline ascorbic acid solution to reduce copper chloride to cuprous chloride with narrow particle size distribution; the second step uses ferrous sulfate and sodium citrate as mixed reducing agent, and sodium citrate can also be used as a complexing agent, which helps to reduce the cuprous chloride to spherical, well-dispersed, uniform particle size distribution of superfine copper powder. At the same time, the raw materials used by the application are easy to obtain, the reaction process is mild, and organic solvents and toxic and hazardous reagents such as sodium borohydride and hydrazine hydrate are not needed, the preparation process has cost effectiveness, is friendly to the environment, and is suitable for industrial production.

The invention discloses preparation and application of high-stability nano-selenium in a food matrix, the nano-selenium is polysaccharide modified nano-selenium, and the nano-selenium is insensitive to pH and alcohol environment and can keep good stability in a liquid food matrix. According to the scheme, the nano-selenium is prepared by using polysaccharide as a stabilizer and reducing selenite by using ascorbic acid. According to the scheme, the high-performance stabilizer is screened by combining the growth curve of the nano-selenium and the interaction between the nano-selenium and the polysaccharide, the stability mechanism of the screened stabilizer is mainly a steric hindrance effect, the screened stabilizer is not sensitive to the complex environment of a food matrix, agglomeration of the nano-selenium is effectively prevented, and the stability of the nano-selenium in the food matrix is guaranteed. The nano-selenium prepared by the scheme provided by the invention can be used as a novel selenium nutrition enhancer by virtue of high stability, is widely applied to the fields of functional foods and dietary supplements, and provides an optimal scheme for solving the problems of low bioavailability, high potential toxicity and the like of the traditional selenium supplements.

The present invention provides a method for producing a cartilage-like tissue from pluripotent stem cells, the method comprising a step for culturing pluripotent stem cells in a cartilage differentiation culture medium and a step for increasing the ascorbic acid concentration of the cartilage differentiation culture medium. The present invention also provides a method for regulating the hardness of induced cartilage-like tissue differentiated from pluripotent stem cells, the method comprising a step for culturing pluripotent stem cells in a cartilage differentiation culture medium and a step for increasing the ascorbic acid concentration of the cartilage differentiation culture medium.

The application relates to the cosmetic technical field, and particularly discloses an anti-aging composition for reducing stress fatigue, a preparation method and application thereof. The anti-aging composition comprises a camellia chrysantha extract, a prosopis juliflora seed extract, a mu-conotoxin and an ascorbic acid polypeptide; the mass ratio of the camellia chrysantha extract, the prosopis juliflora seed extract, the mu-conotoxin and the ascorbic acid polypeptide is (0.1-5):(0.01-2):(0.001-1):(0.01-5). The anti-aging composition provided by the application can reduce stress damage of skin cells, improve cell vitality, thereby improving the problems of skin dullness, roughness, looseness and fine lines caused by overwork, work and emotional stress, and is mild and non-irritating, and is suitable for sensitive skin people.

The invention relates to the field of biological product preparation, in particular to a preparation method of high-activity oyster-derived small molecule peptide. The method comprises the following steps: selecting fresh meat of pacific oysters or ostrea rivularis as a raw material, degreasing, adding water, crushing, filtering, sequentially carrying out compound protease and neutral protease hydrolysis, implanting a sensor and a probe in hydrolysis, monitoring in real time, and dynamically adjusting reaction conditions; adding a targeting microcapsule wrapping an ascorbic acid glutathione composite protective agent, and releasing the protective agent when a target peptide signal is detected; separating and concentrating through a gradient membrane, and purifying the target peptide by using a molecular imprinting chromatographic column; carrying out alkaline hydrolysis on enzymatic hydrolysis residues to prepare chitosan for cyclic utilization, carrying out enzymatic hydrolysis on residual residues to generate collagen peptide, treating and recycling wastewater, and recovering protease. According to the method, the technical effects that the high-activity and high-purity target peptide is prepared, the resource utilization rate is increased, the production cost is reduced, the target peptide has good oxidation resistance and biological activity, the intestinal enzyme degradation rate is reduced after glycosylation modification, and the blood half-life period is prolonged are achieved.

The invention discloses application of cordyceps javanica Bd01 and a dispersible oil suspending agent thereof to prevention and control of spodoptera frugiperda, and relates to the technical field of biology. The research finds that the cordyceps javanica Bd01 has a strong infection lethal effect on larvae of spodoptera frugiperda at all ages, the pupation rate and eclosion rate of the larvae can be remarkably reduced, and the breeding cycle of pests can be effectively blocked. The invention further develops a dispersible oil suspending agent, and the suspending rate is effectively improved through formula optimization. The dosage form takes soybean oil as a dispersion medium, does not contain harmful solvents such as methylbenzene, is free of dust pollution and is friendly to operators and the environment, and ascorbic acid is added to improve the ultraviolet resistance of spores and prolong the effective period of the pesticide effect. In addition, the preparation also has a certain control effect on caffeinidae, is wide in application scene, provides a new scheme for green control of spodoptera frugiperda, solves the problems of chemical pesticide resistance and residue, and accords with the development requirements of green agriculture.

The invention relates to the technical field of functional nutritious food, in particular to multi-layer skin nutrition powder with a whole-spectrum skin growth and repair promoting effect and a preparation method and application thereof, the core of the multi-layer skin nutrition powder is composed of a collagen peptide system (60-62%), a proteoglycan system (20-22%) and the like, collagen peptide is compounded with three sources of cattle, fish and chicken, and the multi-layer skin nutrition powder has the advantages that the multi-layer skin nutrition powder is prepared; according to the present invention, with the combination of the following components, the skin structure and activity are jointly promoted by using the synergistic effect of the functional polypeptide compound (2.5-3.5%) and the plant active component (3.5-4.5%) rich in asiaticoside and procyanidine, and the nutrition enhancers (4-5%) such as L-ascorbic acid and amino acid chelated zinc and the food-grade auxiliary materials (8-10%) such as microcrystalline cellulose are integrated in the formula, such that the various systems achieve the synergistic effect so as to achieve the effect of nourishing the skin; through the synergistic compatibility of the three-source collagen peptide, the comprehensive supplement of various types of collagen in skin tissues is realized.

The invention discloses a multi-stage cooperative processing technology for a tinned pin oxide layer of a plastic package device, and belongs to the technical field of electronic component packaging. The process comprises the following steps of: (1) low-temperature plasma pretreatment: under a vacuum condition, adopting mixed gas of argon and nitrogen, and generating plasma through a radio frequency power supply to carry out irradiation treatment on the surface of a pin; (2) composite reduction treatment: soaking the device in a citric acid-ascorbic acid composite solution with the pH value of 2.8-3.5; and (3) molecular self-assembly protection: carrying out surface coating by adopting an ethanol solution of gamma-aminopropyltriethoxysilane, and curing to form an anti-oxidation protection layer. According to the method, effective removal and protection reconstruction of the oxide layer are achieved through a three-stage cooperative processing mechanism, the pin welding qualification rate can be increased to 98.5% or above, and the temperature in the processing process is always lower than the glass-transition temperature of a plastic packaging material.

The invention provides a multilayer lutein ester liposome as well as a preparation method and application thereof, and belongs to the field of food processing. The multi-layer lutein ester liposome is prepared from the following raw materials: 30 to 50 parts of lutein ester, 40 to 60 parts of soybean phosphatidylcholine, 5 to 20 parts of cholesterol, 10 to 25 parts of starch sodium octenylsuccinate, 20 to 40 parts of trehalose, 15 to 30 parts of mannitol, 4 to 10 parts of phosphatidyl glycerol, 1 to 2 parts of vitamin E acetate and 1 to 2 parts of ascorbyl palmitate. According to the present invention, through the specific food-grade raw material composition and the accurate ratio relationship, the comprehensive delivery system is constructed for the highly hydrophobic and unstable lutein ester, and the system synchronously achieves the high encapsulation efficiency, the excellent stability, the good water dispersibility and the slow release function.

The invention relates to the technical field of materials, in particular to a graphdiynyl lanthanide series metal doped copper nano material and a preparation method and application thereof, and the preparation method comprises the following steps: preparing graphdiyne; in an inert gas atmosphere, graphdiyne, CuCl2. 5H2O, Dy (NO3) 3.5 H2O and ascorbic acid are subjected to a reaction in an aqueous solution, and the graphdiynyl lanthanide metal Dy doped copper nano material is obtained. Wherein the copper nano material is a cuprous oxide nano material. According to the prepared Dy-Cu2O / GDY, CO2 can be efficiently converted into C2H5OH through electrocatalytic reduction.

The invention relates to the technical field of immunochromatography analysis, and discloses a signal enhancer of a colloidal gold immunochromatography rapid detection card and a preparation method thereof, the signal enhancer comprises a silver ion solution, a thiourea-ascorbic acid synergistic reducing agent, a pH buffer system and a surfactant stabilizing system, the signal amplification is realized by catalyzing and depositing silver nanoparticles on the surface of colloidal gold, the operation is simple and convenient, one-time addition is realized, and the reaction is completed within 5-10 minutes; the sensitivity is improved by 5-10 times, and the specificity is higher than 98%; the stability is excellent, and the storage time is 12 months at 4 DEG C; various colloidal gold rapid detection cards are universally compatible; compared with the prior art, the colloidal gold immunochromatography rapid detection card has the advantages that the cost is controllable, the single detection is increased by 0.3-0.5 yuan, and the colloidal gold immunochromatography rapid detection card is particularly suitable for ultra-sensitive detection of small molecular substances in the field of food safety, for example, the detection limit of malachite green reaches 0.1 microgram per liter, the detection limit of fipronil reaches 0.5 microgram per liter, and the application range of the colloidal gold immunochromatography rapid detection card is obviously expanded.

The invention provides an oral thylakoid product for resisting organ failure and aging, which is prepared by the following steps: extracting thylakoid from plants including spinach, arabidopsis thaliana, lettuce, cabbage, green algae or wheat seedlings, redissolving the thylakoid into a buffer salt solution A, and carrying out ultrasonic treatment for 10-20 minutes under the ultrasonic power of 200-500W to prepare a suspension; adjusting the concentration of the suspension to 0.5-2 mg / ml, and obtaining a nano capsule-like body with the particle size of 200-500 nm by using a microfluidic technology; the buffer salt solution A is prepared from 10 to 100 mmol / L of 4-hydroxyethyl piperazine ethanesulfonic acid (HEPES), 1 to 2 mmol / L of ethylenediamine tetraacetic acid (EDTA) disodium, 0.5 to 4 mmol / L of magnesium chloride (MgCl2), 1 to 10 mmol / L of ascorbic acid and 100 to 500 mmol / L of sapoeda sodium (SNAC), and the pH value of the buffer salt solution A is adjusted to 7.5 to 8.0; and the concentration of the capsule in the buffer salt solution A is 100-400 mg / mL. According to the product, self QPRT enzyme of the thylakoid is used for efficiently catalyzing de novo synthesis of NAD + of whole body tissues and organs, so that multiple physiological processes such as energy synthesis enhancement, oxidative stress reduction and inflammatory reaction relief are finally realized, organ failure is efficiently reversed, and organ aging is relieved.

The invention provides silver powder with high crystallinity and narrow particle size distribution and a preparation method thereof, and belongs to the technical field of metal powder preparation. The preparation method comprises the following steps: preparing a silver nitrate solution, an ascorbic acid solution, a stabilizer solution, a dispersant solution, a seed crystal solution, a nitric acid solution and a surface modifier solution; adding the stabilizer solution and the nitric acid solution into the seed crystal solution, and mixing to obtain a solution A with specific PH; the dispersing agent solution is added into the silver nitrate solution for mixing, and a solution B is obtained; adding the solution B and an ascorbic acid solution into the solution A, fully reacting, and collecting a precipitate; and washing the precipitate, adding a surface modifier solution, fully stirring, drying, and dispersing to obtain the target silver powder. Different reaction mixed solutions are prepared step by step and then mixed according to a specific sequence, and the submicron silver powder with the high crystallinity and the large specific surface area is prepared through a simple and controllable method.

The invention discloses a combined drying method for maintaining color and nutrition of mango freeze-dried products, and belongs to the technical field of food processing. The preparation method comprises the following steps: cutting mangoes, performing vacuum impregnation in a composite protection solution containing maltodextrin, trehalose, L-ascorbic acid and citric acid, then performing quick-freezing treatment, and finally adopting a combined drying process combining microwave vacuum drying and vacuum freeze drying to reduce the water content of the materials to the final requirement in two stages. The method is mainly used for efficiently producing a high-quality mango freeze-dried product which can perfectly maintain the natural color, shape and nutritional ingredients of mangoes; the technical problems that the drying period is too long, the energy consumption is high, and color browning and heat-sensitive nutritional ingredient degradation are prone to occurring in the long drying process when mangoes are treated through a traditional freeze-drying technology are effectively solved.

The invention relates to a whitening and anti-aging composition which is characterized by comprising a solvent, a vitamin C derivative and an active agent, and the vitamin C derivative comprises 3-o-ethyl ascorbic acid, ascorbyl glucoside, magnesium ascorbyl phosphate, sodium ascorbyl phosphate and ascorbic acid polypeptide. By the adoption of the technical scheme, the whitening and anti-aging composition and the cosmetic containing the composition are high in stability, good in transdermal absorbability, lasting in effect, mild and capable of whitening skin and resisting aging in a synergistic mode.

The invention discloses a skin jelly preparation method capable of prolonging the shelf life through a compound technology, and relates to the technical field of food processing technologies. The method comprises the following steps: cutting an animal skin raw material, treating with a sodium carbonate solution, cleaning with a citric acid solution, boiling to extract a collagen solution, adding ascorbic acid and nisin, freezing and forming, drying in vacuum, performing irradiation sterilization and the like. According to the method, fat and impurities in the raw materials can be effectively removed, oxidation reaction and microbial reproduction can be inhibited, the moisture content can be reduced to 5% or below, and residual microorganisms can be thoroughly killed, so that the shelf life of the skin jelly can be remarkably prolonged to 12 months or above, meanwhile, good taste and nutritional value are kept, market requirements are met, and the production cost is reduced.

The invention discloses a whitening and spot-fading composition and application thereof, and belongs to the technical field of cosmetics. The whitening and spot-fading composition is prepared from the following components in percentage by mass: 0.1 to 5.0 percent of nicotinamide, 0.0001 to 3.0 percent of tranexamic acid, 0.0001 to 1.0 percent of glycyrrhiza glabra root extract, 0.0001 to 0.4 percent of phenethyl resorcinol, 0.0001 to 2.0 percent of ascorbyl tetraisopalmitate, 0 to 1.0 percent (not including 0) of radix gentianae extract, 0.15 to 4.0 percent of emulsifier, 0.1 to 2.5 percent of antioxidant and the balance of water. By matching with various whitening active ingredients, the comprehensive whitening, brightening and skin improving effects are realized in the aspects of inhibiting melanin generation, blocking melanin transfer, accelerating melanin metabolism and the like; the combination of the specific emulsifier and the thickener can effectively improve the component stability of the composition. The composition is mild in performance, free of irritation to skin and good in market value.

The invention provides a multicolor visual semi-quantitative detection method for miRNA in skin interstitial fluid, which comprises the following steps: extracting a skin interstitial fluid sample in a minimally invasive manner by combining a microneedle patch with a vacuum negative pressure technology; the method comprises the following steps: incubating a skin interstitial fluid sample and a magnetic nanoprobe of which the surface is immobilized with a hairpin probe H1, opening H1 in the presence of target miRNA, triggering a subsequent hybridization chain reaction of a hairpin probe H2 and H3, and constructing a biotin-rich DNA compound on the surface of a magnetic bead; the method comprises the following steps: carrying out enzyme labeling by using an alkaline phosphatase-streptavidin conjugate, catalyzing ascorbic acid phosphate to generate ascorbic acid to reduce potassium iodate, and generating an iodine elementary substance to etch a gold nano bipyramid, so that the color of a solution is changed, and high-sensitivity detection on target miRNA is realized. The multi-color visual detection method provided by the invention is combined with the gold nano bipyramid localized surface plasmon resonance property change, so that near-full spectrum color change can be generated, and the portability of the sensor and the accuracy of visual analysis can be improved.

The object of the present invention is to provide a novel ascorbic acid derivative with excellent stability, and its applications. [Solution] A compound (compound of general formula (1) below) is used, in which a phosphocholine group is introduced to the hydroxyl group at the 2 position of ascorbic acid via a phosphate ester bond. The ascorbic acid derivative of the present invention has excellent whitening and antioxidant properties, and is also highly stable. Therefore, the ascorbic acid derivative of the present invention can be preferably used as an active ingredient in cosmetics and topical skin preparations. TIFF2026055124000012.tif39101

A topical neurocosmetic composition comprising a first component including one or more of bakuchiol, allantoin, squalane, or Morinda citrifolia extract; a second component including one or more of hyaluronic acid, vitamin E, Zanthoxylum alatum fruit extract, Coriandrum sativum seed oil, Vitex agnus-castus extract, Helianthus annuus sprout extract, niacinamide, resveratrol, or an ascorbyl ester; and a cosmetically acceptable oil-in-water vehicle configured to deliver both lipophilic and hydrophilic actives through the skin to dermal neurons. The composition improves measurable skin parameters such as hydration and elasticity and supports psychophysiological comfort. Methods of manufacture and use are also described

The invention belongs to the technical field of talc, and provides a method for detecting fluorescent substances in talc raw ore, which comprises the following steps: S1, carrying out ball milling on the talc raw ore in a ball mill, sieving to obtain sieved powder, and adding deionized water into the sieved powder to obtain slurry; s2, adding the slurry into the mixture to enable the pH value of the slurry to be 5, stirring, and standing in a water bath for 2-3 hours to obtain a first precipitate; s3, adding a thiourea-ascorbic acid solution into the first precipitate to obtain a second precipitate; and S4, carrying out secondary ball milling on the second precipitate, and spreading the second precipitate in an enamel plate to detect whether the talc raw ore contains the fluorescent substances or not. The hydrochloric acid can dissolve quartz and mica to avoid generation of background fluorescence or quenching effect, and the nonionic surfactant polyethylene glycol can be adsorbed on the surface of the mineral to reduce interfacial tension, so that the hydrochloric acid is easier to infiltrate tiny pores, the pit defect caused by local over-corrosion is reduced, the pickling uniformity is improved, and the detection sensitivity is improved.

The invention relates to the technical field of oral preparations, in particular to an improved oral preparation based on traditional Chinese medicine prescription Yufengxiang powder and a preparation method of the oral preparation. The preparation comprises traditional Yufengxiang powder components such as mung beans, radix angelicae, Chinese wolfberry fruits, licorice roots and poria cocos. And modern functional components such as turmeric, grape seeds, low-molecular-weight hyaluronic acid, L-ascorbic acid, zinc gluconate, a pumpkin seed extract, black pepper pigment and a rice essence extract. The preparation method comprises the following steps: respectively extracting the raw materials, drying into powder, mixing all active components according to the formula, controlling the moisture content of the powder, and filling into an enteric capsule shell. Through dosage form improvement and formula optimization, the bioavailability of active ingredients is remarkably improved, multiple synergistic effects of whitening, oxidation resistance, moisturizing, nerve soothing, alopecia improvement and the like are achieved, and the technical problems that traditional Yufeng western style powder is low in external use absorption rate and single in function are solved.

The invention discloses an electroplating method of a low-porosity nanoscale bright tin layer, which comprises the following steps: placing a clean metal substrate in an activating solution containing a surface modifier, and applying high pulse current for short-time impact to form a transition layer to obtain a target substrate; a target base material is placed in the nano-composite tin plating solution, electroplating is carried out under the cooperation of a continuous ultrasonic field and target waveform pulse current, and a low-porosity nano-scale bright tin layer is formed; the nanometer composite tin plating solution comprises stannous methanesulfonate, methanesulfonic acid, nanometer silicon carbide, nanometer silicon dioxide, a grain refiner, a dispersing agent, cinnamyl aldehyde, a vinyl pyrrolidone copolymer, ascorbic acid, a wetting agent and the balance deionized water. The binding force of a plating layer without a base coat is improved, the plating layer is strengthened, compact and bright, and the process is environmentally friendly.

The invention discloses a compound microorganism freeze-drying protective agent, a preparation method of the compound microorganism freeze-drying protective agent and a use method of the compound microorganism freeze-drying protective agent. Comprising the following raw materials in parts by weight: 0.03 part of disodium ethylene diamine tetraacetate, 5 to 15 parts of trehalose, 2 to 5 parts of sorbitol, 0.5 to 2 parts of ascorbic acid, 0.05 to 0.2 part of N-acetyl-L-cysteine, 0.1 to 0.5 part of polylactic acid-glycolic acid copolymer, 0.01 to 0.05 part of alpha-tocopherol and 1 to 3 parts of bentonite. The PLGA, the alpha-tocopherol and the NAC construct a three-stage synergistic anti-oxidation system from outside to inside: the PLGA is externally blocked, so that rapid consumption of an antioxidant is avoided, and slow release is realized; the alpha-tocopherol realizes oxidative damage repair of cell membranes; nAC maintains the internal reduction environment of cells, reduces oxidative stress and can regenerate alpha-tocopherol at the same time, and reutilization of resources is achieved.

The invention relates to the technical field of titanium dioxide production, in particular to high-retention and high-weather-resistance titanium dioxide as well as a preparation method and application thereof. Comprising a titanium dioxide base material and a coating layer located on the surface of the titanium dioxide base material, and the coating layer sequentially comprises an aluminum oxide film layer, a tin oxide film layer and an ascorbyl palmitate film layer from inside to outside. The preparation method comprises the following steps: preparing titanium dioxide-based material slurry, sequentially carrying out aluminum oxide coating and tin oxide coating, then carrying out water washing, flash evaporation and steam powdering, and adding ascorbyl palmitate in the steam powdering process to obtain the high-retention and high-weather-resistance titanium dioxide. The tin coating layer and the ascorbyl palmitate coating layer are introduced to the outer side of the aluminum oxide coating layer, so that the retention rate and weather resistance of titanium dioxide in paper are remarkably improved, and the use requirements of high-end paper are met; the white water treatment pressure can be reduced, and the economic benefit is improved.